第48卷第3期2023年6月广州化学GuangzhouChemistryVol.48No.3Jun.2023DOI:10.16560/j.cnki.gzhx.20230302___________________________________________收稿日期:2022-11-01基金项目:辽宁省教育厅项目(Inzd2019-05)作者简介:王瑶瑶(1997~),女,山东临沂人,硕士研究生,主要从事低辐射镀膜研究。*通信作者:时方晓(1968~),男,辽宁鞍山人,博士,教授,主要从事低辐射镀膜研究。(Ag,Ti)复合膜层的制备及光热性能研究王瑶瑶,时方晓*,曲汝丹,覃茜语(沈阳建筑大学,辽宁沈阳110000)摘要:采用普通钠钙玻璃作为基底材料,利用磁控溅射沉积系统制备出(Ag,Ti)复合膜,通过紫外-可见光分光光度计、自制隔热木箱对膜层透光隔热性能进行分析,采用SEM对复合膜表面形貌分析,并对复合膜进行应用于室外的耐酸碱腐蚀性测试。结果表明:Ag基膜层在溅射参数为Ag靶功率为75W、溅射时间为0.2min、氩气流量20sccm、溅射压强2.1Pa时具有最高的可见光透过率;(Ag,Ti)复合膜在不改变Ag溅射参数的情况下,Ti靶溅射功率为48W、溅射时间0.2min、氩气流量20sccm、溅射压强2.1Pa时具有较好的透光隔热性能,此时可见光透过率达到70%,隔热达到4.5℃,复合膜表面相对平整。关键词:(Ag,Ti)复合膜;Low-E玻璃;磁控溅射;透光性能;隔热性能中图分类号:TQ171.72PreparationandPhotothermalPropertiesof(Ag,Ti)CompositeFilmsWANGYao-yao,SHIFang-xiao*,QURu-dan,QINXi-yu(ShenyangJianzhuUniversity,Shenyang110000,China)Abstract:Usingordinarysodalimeglassasthebasematerial,(Ag,Ti)compositefilmswerepreparedbyusingamagnetronsputteringdepositionsystem.Thelighttransmissionandheatinsulationpropertiesofthefilmwereanalyzedbyultravioletvisiblespectrophotometerandself-madeheatinsulationwoodenbox.ThesurfacemorphologyofthecompositefilmwasanalyzedbySEM.Theacidandalkalicorrosionresistanceofthecompositefilmappliedoutdoorswastested.TheresultsshowthattheAgbasedfilmlayerhasthehighestvisiblelighttransmittancewhenthesputteringparametersareAgtargetpower75W,sputteringtime0.2min,argonflowrate20sccm,andsputteringpressure2.1Pa;(Ag,Ti)compositefilmhasgoodlighttransmissionandheatinsulationperformancewhenthesputteringpowerofTitargetis48W,thesputteringtimeis0.2min,theargonflowrateis20sccm,andthesputtering...