_MNL_44-2007.pdf

Guide to ASTM Test Methodsfor the Analysis of PetroleumProducts and Lubricants2nd EditionR.A.Kishore NadkarniASTM Stock No.MNL442ndASTM International100 Barr Harbor DrivePO Box C700West Conshohocken,PA 19428-2959e-mail:serviceastm.orgwebsite:http:/www.astm.orgPrinted in U.S.A.Library of Congress Cataloging-in-Publication DataNadkarni,R.A.Guide to ASTM test methods for the analysis of petroleum products and lubricants/R.A.Kishore Nadkarni2nd ed.p.cm.?ASTM manual series;no.mnl44-2nd?Includes bibliographical references and index.ISBN 978-0-8031-4274-91.Petroleum productsTestingStandards.2.Lubrication and lubricantsTestingStandards.I.Title.TP691.N33 2007665.5380287-dc222007022845Copyright 2007 ASTM International,West Conshohocken,PA.All rights reserved.This material may not be reproducedor copied,in whole or in part,in any printed,mechanical,electronic,film,or other distribution and storage media,without the written consent of the publisher.Photocopy RightsAuthorization to photocopy item for internal,personal,or educational classroom use,or the internal,personal,oreducational classroom use of specific clients,is granted by ASTM International ASTM provided that theappropriate fee is paid to the Copyright Clearance Center,222 Rosewood Drive,Danvers,MA 01923;Tel:978-750-8400;online:http:/ in City,StateMonth 2007How To Use This ManualTable Ilists the test methods with their equivalent IP,ISO,DIN,JIS,and AFNOR designations.The top of each pagelisting the test summary also refers to these equivalent standards.If you are considering using any standard that hasequivalent standards you should refer to them to determine the full scope of each standard and any differencesbetween.Although these standards are listed as equivalent they will not be exactly the same in many cases.Table IIlists the ASTM test methods alphanumerically by ASTM designation.If you know the ASTM designation,this isthe easiest way to find what you need.The top of each page listing the test summary also refers to these equivalentstandards.ForewordTHE PUBLICATION,Guide to ASTM Test Methods for the Analysis of Petroleum Products and Lubricants:2nd Edition,wassponsored by ASTM Committee D02 on Petroleum Products and Lubricants and edited by R.A.Kishore Nadkarni,Millennium Analytics,Inc.,East Brunswick,NJ.This is Manual 442nd of ASTMs manual series.This manual originally published in 2000 has proved to be a useful reference book to technologists and others in thePetroleum Products and Lubricants industry.This enlarged second edition is updated to include ASTM D02 Committeetest methods published through the end of 2006.The manual contains descriptions of a total of 585 test methods?anincrease of 222 test methods from 363 methods in the first edition?describing a total of about 229 chemical and physicaltests used to analyze petroleum products and lubricants?an increase of about 69 properties from about 160 propertiesdescribed in the first edition?.The author and the publisher hope that this second edition will prove as useful as the first one to the oil industryresearchers,analysts,and marketers.CONTENTSIntroduction1Explanation of Terms2Table ITest Method Equivalence3Table IIAlphanumeric Index of Standards6Reference ASTMAnalysisStandardACID NUMBERby color indicator titrationsee also Base number,p.37D 97417by potentiometric titrationD 66417by semi-micro color indicator titrationD 333919by semi-quantitative micro determination of acid number of lube oils duringoxidation testingD 577019ACIDITYin aviation turbine fuelD 324220of hydrocarbon liquids and their distillation residuesD 109320ACTIVE SULFURin cutting oilsD 166221in fuels and solvents?doctor test?D 495221ADHESION OF SOLID FILM LUBRICANTSD 251021AIR RELEASE PROPERTIES OF OILSD 342722ALKYL NITRATE IN DIESEL FUELSD 404622AMYL NITRATE IN DIESEL FUELSD 183923ANALYSIS OF LPG AND PROPANE CONCENTRATES BY GCD 216323ANILINE AND MIXED ANILINE POINTD 61124APPARENT VISCOSITY GENERAL25Borderline pumping temperature of engine oilssee p.47D 3829Apparent viscosity by capillary viscometer at high temperature high shearD 462425HTHs by tapered bearing simulatorD 468325HTHs by tapered plug viscometerD 474126using cold cranking simulatorD 529326at high temperature high shear by multicell capillary viscometerD 548126of lubricating greasesD 109227yield stress and apparent viscosity at low temperatureD 468427APPLIED COATING WAX IN CORRUGATED BOARD FACINGD 352228AROMATICSand polynuclear aromatics in diesel and aviation turbine fuels by SFCD 518628in finished gasoline by gas chromatographyD 442029in finished gasoline by GCD 558030in finished gasoline by GC-FTIRD 598630in gasolines by gas chromatography-mass spectrometry?GC-MS?D 576931in hydrocarbon oils by high resolution nuclear magnetic resonance?HR-NMR?D 529232ASHin coal tar and pitchD 241532in petroleum cokeD 442233from petroleum productsD 48233sulfated ash from lubricating oils and additivesD 87434ASPHALTENES?HEPTANE INSOLUBLES?IN CRUDE PETROLEUM ANDPRODUCTSD 656034BASE NUMBE