Designation:F3139−15StandardTestMethodforAnalysisofTin-BasedSolderAlloysforMinorandTraceElementsUsingInductivelyCoupledPlasmaAtomicEmissionSpectrometry1ThisstandardisissuedunderthefixeddesignationF3139;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginaladoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperscriptepsilon(´)indicatesaneditorialchangesincethelastrevisionorreapproval.1.Scope1.1Thistestmethodcoversproceduresfortheanalysisoftin-basedsolderalloysforminorandtraceelementsusinginductively-coupledplasmaatomicemissionspectrometry(ICP-AES)instrumentation.1.2Thesetestprocedureswerevalidatedfortheanalytesandmassfractionslistedbelow.ElementValidatedMassFractionRange,mg/kgLead115to965Cadmium25to60Mercury5to530Antimony85to1330Bismuth80to210Arsenic95to360Silver4000to42100Cobalt0.5to60Iron15to115Chromium0.5to1.5Copper3000to30600Indium25to115Nickel5to150Phosphorus10to110Selenium1to30Zinc2to160Aluminum1to31.3Theproceduresappearinthefollowingorder:ProcedureSectionInternalStandardization8CalibrationSolutionPreparations9PreparationofSampleandValidationSolutions10Calibration11AnalysisProcedure121.4ThevaluesstatedinSIunitsaretoberegardedasthestandard.Anyothervaluesareforinformationonly.1.5Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappro-priatesafetyandhealthpracticesanddeterminetheapplica-bilityofregulatorylimitationspriortouse.2.ReferencedDocuments2.1ASTMStandards:2D1129TerminologyRelatingtoWaterE177PracticeforUseoftheTermsPrecisionandBiasinASTMTestMethodsE416PracticeforPlanningandSafeOperationofaSpec-trochemicalLaboratory(Withdrawn2005)3E691PracticeforConductinganInterlaboratoryStudytoDeterminethePrecisionofaTestMethodE1479PracticeforDescribingandSpecifyingInductively-CoupledPlasmaAtomicEmissionSpectrometers3.Terminology3.1Definitions—Fordefinitionsofothertermsusedinthistestmethod,refertoTerminology...
