ASTM_D_1007_-_11.pdf

Designation:D100711Standard Specification forsec-Butyl Alcohol1,2This standard is issued under the fixed designation D1007;the number immediately following the designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon()indicates an editorial change since the last revision or reapproval.1.Scope*1.1 This specification covers sec-butyl alcohol for use inpaint,varnish,lacquer,and related products.1.2 The values stated in SI units are to be regarded asstandard.No other units of measurement are included in thisstandard.1.3 The following applies to all specified limits in thisstandard;for purposes of determining conformance with thisstandard,an observed value or a calculated value shall berounded off“to the nearest unit”in the last right-hand digitused in expressing the specification limit,in accordance withthe rounding-off method of Practice E29.1.4 For hazard information and guidance,see the suppliersMaterial Safety Data Sheet.2.Referenced Documents2.1 ASTM Standards:3D268 Guide for Sampling and Testing Volatile Solvents andChemical Intermediates for Use in Paint and RelatedCoatings and MaterialD1078 Test Method for Distillation Range of Volatile Or-ganic LiquidsD1209 Test Method for Color of Clear Liquids(Platinum-Cobalt Scale)D1353 Test Method for Nonvolatile Matter in Volatile Sol-vents for Use in Paint,Varnish,Lacquer,and RelatedProductsD1364 Test Method for Water in Volatile Solvents(KarlFischer Reagent Titration Method)D1613 Test Method for Acidity in Volatile Solvents andChemical Intermediates Used in Paint,Varnish,Lacquer,and Related ProductsD4052 Test Method for Density,Relative Density,and APIGravity of Liquids by Digital Density MeterD5386 Test Method for Color of Liquids Using TristimulusColorimetryE29 Practice for Using Significant Digits in Test Data toDetermine Conformance with SpecificationsE300 Practice for Sampling Industrial Chemicals2.2 U.S.Federal Specification:PPP-C-2020 Chemicals,Liquid,Dry,and Paste:Packagingof43.Properties3.1 sec-Butyl alcohol shall conform to the following re-quirements:Apparent specific gravity:20/20C0.807 to 0.809or25/25C0.804 to 0.806Color,Pt-Co scale,maxA10Distillation range,760 mmHg,C as:Initial boiling point,min98.0Dry point,max101.0Nonvolatile matter,max,mg/100 mL5Water,max,weight%0.5Acidity,as acetic acid,max,weight%0.002BAInstrumental Pt-Co color determined by Test Method D5386 have been shown tohave no statistically significant difference from Pt-Co color determined by TestMethod D1209.However,it is not known whether sec-butyl alcohol was part of thesample set included in the interlaboratory study.BEquivalent to 0.019 mg of KOH per gram of sample.4.Sampling4.1 The material shall be sampled in accordance withPractice E300.5.Test Methods5.1 The properties enumerated in this specification shall bedetermined in accordance with the following ASTM methods:5.1.1 Apparent Specific GravityDetermine the apparentspecific gravity at 20 or 25C by a convenient method that isaccurate to the third decimal place.See Guide D268 or TestMethod D4052.1This specification is under the jurisdiction of ASTM Committee D01 on Paintand Related Coatings,Materials,and Applications and is the direct responsibilityD01.35 on Solvents,Plasticizers,and Chemical Intermediates.Current edition approved Nov.1,2011.Published November 2011.Originallyapproved in 1949.Last previous edition approved in 2005 as D1007 05.DOI:10.1520/D1007-11.2This compound is also known under the names 2-butanol and secondarybutanol.3For referenced ASTM standards,visit the ASTM website,www.astm.org,orcontact ASTM Customer Service at serviceastm.org.For Annual Book of ASTMStandards volume information,refer to the standards Document Summary page onthe ASTM website.4Available from Standardization Documents Order Desk,DODSSP,Bldg.4,SectionD,700RobbinsAve.,Philadelphia,PA19111-5098,http:/dodssp.daps.dla.mil.*A Summary of Changes section appears at the end of this standardCopyright ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959.United States1 5.1.2 ColorTest Method D1209(see Note A in 3.1).5.1.3 Distillation RangeTest Method D1078 using a tem-perature measuring device having a range of 72 to 126C anda resolution of 0.1C.5.1.4 Nonvolatile MatterTest Method D1353.5.1.5 WaterTest Methods D1364.5.1.6 AcidityTest Method D1613.6.Packaging and Package Marking6.1 Package size shall be agreed upon between the pur-chaser and the supplier.6.2 Packaging shall conform to applicable carrier rules andregulations or when specified shall conform to Fed.Spec.PPP-C-2020.7.Keywords7.1 methylethylcarbinol;sec-butylalcohol;2hydroxybutaneSUMMARY OF CHANGESCommittee D01 has identified the location of selected changes to this standard since the last issue(D1007-05)that may impact the use of this standard.(Approved November 1,2011.)(1)Revised 5.1.3.(2)Removed Specification E1 from 2.1.ASTM