ASTM_D_1068_-_15_rus.pdf

D 1068-15 STANDARD TEST METHODS FOR IRON IN WATER 2016 ():2976-16/ASTM :01.09.2016 -,.9,-49,-1,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 1068-15 1 D 1068-15 1 D 1068;,.().1.*1.1 .,.:A -0,1 5,0/7-16 1 ASTM D19 ,D19.05 .1 2015.2015.1949.2010.D1068-10.DOI:10.1520/D1068-15.ASTM D 1068-15 2 -5 100/17-26 C ,/40 1000/27-38 1.2 .1.3 /.2.1.4,.-,.1.5 ,.,.4,11.7.1 X1.1.2.2.2.1 ASTM:2 D 858 D 1066 D 1129,2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 1068-15 3 D 1193 D 1687 D 1688 D 1691 D 1886 D 2777 ,D19 D 3370 D 3558 D 3559 D 3919 -D 4841 ,D5673 -D 5810 D 5847 E 60 ,E 275 ,3.3.1:3.1.1 ,.ASTM D 1068-15 4 D 1129.3.2 ,:3.2.1 ,4.4.1 -,.-0,3/.5.5.1 .,.3 ,.5.2 ,3 ,DC.,.Analar Standards for Laboratory Chemicals,BDH Ltd.,Poole,Dorset,United States Pharmacopeia and National Formulary,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.ASTM D 1068-15 5 ,I D 1193.,.II.,.6.6.1 D 1066 D 3370,.6.2 HNO3 HCl(1,42)pH 2 .0,45.D 4841.1 ,pH ,14.,24 ,.,.6.3 .6.4 33.1.ASTM D 1068-15 6 A -7.7.1 .7.2 0,1 5,0/.7.3 ,.8.8.1 -,/,.(D 1886),(D 1687),(D 3558),(D 1688),(D 3559),(D 858)(D 1691).ASTM D 1068-15 7 9.9.1,(5000/),(100/).9.2 (/).2 .10.10.1-,248,3.3 .,248,3,.10.1.1 ,.10.2 ,.11.11.1 (1,19)(HCl).4 ,HCl ASTM D 1068-15 8 ,.(HCl (6 N HCl),HCl,.)11.2 (1,42)(HNO3).5 ,HNO3 ,.11.3 (1+499)1 HNO3(1,42)499 .11.4 (1 =1,0 )1,000 100 HCL(1+1).1.,.11.5 (1 =0,1 )100,0 1.11.6:11.6.1,.11.7:11.7.1 ,.,.345 (50 .).(,ASTM D 1068-15 9 ).11.8 .0,45-.:,.,.12.12.1 100 ,HNO3(1+499).D 4841.12.2 0,5 HNO3(1,42),13.1-13.5.6,13.1.12.3 ,.HNO3(1+499).12.4 .,.ASTM D 1068-15 10 13.13.1 100,0 125.6 13.5.13.2 5 HCl(1,19).13.3 ,20 15,.7 ,.8 ,.,.(65C 85C).,0,5%.,.13.4 (11.8)(,)100.-.13.5 13.4 248,3.HNO3(1+499).ASTM D 1068-15 11 14.14.1 ,12.4.15.4 15.1 ,10 16 ,:,II:ST=0,047 X+0,053 So=0,030 X+0,037 :ST=0,050 X+0,114 So=0,024 X+0,078:ST-,So-,X-,/.15.2 .1.15.3 ,.4 -ASTM International RR:D19-1035.ASTM Customer Service serviceastm.org.ASTM D 1068-15 12 1.-,II:-,%(95%-),/,/,/0,2 0,2 0,0 0,0 2,4 2,4 0,0 0,0 4,4 4,3 0,1 2,3 :-,%(95%-),/,/,/0,2 0,2 0,0 0 2,4 2,3 0,1 4,17 4,4 4,2 0,2 4,55 15.4 ,D 2777-77,.,1.4 D 2777-13,D19 .16.16.1 ,QC.16.2 :16.2.1 ASTM D 1068-15 13 ,.0,990.16.2.2 ,.,15%.16.2.3 .16.2.4 (CCB)(CCV)10%.15%.16.3 :16.3.1 ,.,.16.3.2 ,.,.ASTM D 1068-15 14 16.3.3 ,.1.,.1.,.D 5847 F-t-.16.4 (LCS):16.4.1 ,LCS,(20).,LCS.LCS ,.,LCS,15%.16.4.2 ,.16.5 :16.5.1 .,ASTM D 1068-15 15.,.16.6 (MS):16.6.1 -.16.6.2 .,2-5 ,10-50 ,.16.6.3 (P):P=100 A(Vs+V)BVs/CV(3):A-(/),-(/),-(/),Vs-(),V-().ASTM D 1068-15 16 16.6.4 ,.1 D 5810.,.:,.9 .D 5810.16.7 :16.7.1 .,(MSD).16.7.2 ,F-.F-.6.4.4 D 5847.16.7.3 ,.16.8 (IRM):16.8.1 ,(IRM),ASTM D 1068-15 17 .IRM ,.,.B -17.17.1 .17.2 5 100/20.,-(A).-(ICP-MS),.D 5673.17.3 ,.17.4-D 3919 ASTM D 1068-15 18-.18.18.1 -.,(),.,.D 3919.18.2 .18.3 .,.19.19.1 ,D 3919.20.20.1-,248,3.ASTM D 1068-15 19 10 ,248,3,.,.11 .20.2 ,.20.3 ,.20.4 ,.20.5,1 100,.20.6 ,(,.).0,2.20.7 .12 ,-,.ASTM D 1068-15 20 20.8 .11.8.21.21.1 (1 =1000 Fe).11.4.21.2 (1,0 =10 Fe)10,0 (21.1)1 HNO3(1,42)1.21.3 (1,0 =0,2 Fe)20,0 (21.2)1 HNO3(1,42)1.21.4 (1,42)(HNO3)(.5).21.5,.,.22.22.1 ,D 3919.23.23.1 ,HNO3(1+1),.23.2 100,0 ASTM D 1068-15 21 125.HNO3(1,42)5/,23.4 23.6.23.3 0,45-,23.6.(.11.8)23.4 95 ,20 15,(.7 8).23.5 (11.8)(,)100.-(.13).0,5%HNO3.13 .100.23.6 ,.D 3919.24.24.1 D 3919.25.5 25.1 13 5 -ASTM International RR:D19-1102.ASTM Customer Service serviceastm.org.ASTM D 1068-15 22 ,7 ,.,.2.2.-:,/,/ST-,/-,%8,0 11,3 6,18+3,3+41,3 20 21,1 12,35+1,1+5,5 68 67,1 30,62 0,9 1,3 :,/,/ST-,/-,%8,0 6,9 3,17 1,1 13,8 20 19,0 8,33 1,0 5,0 68 70,1 21,63+2,1+3,1 25.2 ,.25.3 ,D 2777-77,ASTM D 1068-15 23 .,1.4 D 2777-13,D19.26.26.1 ,QC.26.2 :26.2.1 ,.0,990.26.2.2 ,.,15%.26.2.3 .26.2.4 (CCB)(CCV)10%.15%.26.3 :ASTM D 1068-15 24 26.3.1 ,.,.26.3.2 ,.,.26.3.3 ,.2.,.2.,.D 5847 F-t-.26.4 (LCS):26.4.1 ,LCS,(20).,LCS.LCS ,.,LCS,ASTM D 1068-15 25 15%.26.4.2 ,.26.5 :26.5.1 .,.,.26.6 (MS):26.6.1 -.26.6.2 .,2 5 ,10 50 ,.ASTM D 1068-15 26 26.6.3 (P):P=100 A(Vs+V)BVs/CV(2):A-(/),-(/),-(/),Vs-(),V-().26.6.4 ,.2 D 5810.,.:,.14 .D 5810.26.7 :26.7.1 .ASTM D 1068-15 27,(MSD).26.7.2 ,F-.F-.6.4.4 D 5847.26.7.3 ,.26.8 (IRM):26.8.1 ,(IRM),.IRM ,.,.C 27.27.1 :(BPA-)(4,7-1,10-),ASTM D 1068-15 2