ASTM_D_1688_-_12_rus.pdf

D 168812 STANDARD TEST METHODS FOR COPPER IN WATER 2014.():2259-14/ASTM :03.02.2014 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 1688-12 1 D 168812 1 D 1688;,.().1.*1.1 -.:A ,0,05 5/7-15 ,-50 500/16-24 ,5 100/25-33 1.2 .0,45 (325).1 ASTM D19 D19.05 .1 2012.2012.1959.2007.D 1688-07.DOI:10.1520/D1688-12.ASTM D 1688-12 2 .1.3,-,.,;.1.4 ,.,.4,.6,.10 .16.1.5 .X1.2.2.1 ASTM:2 D 858 D 1066 D 1068 D 1129,D 1193 D 1687 D 1691 D 1886 2 ASTM,-ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 1688-12 3 D 2777 ,D19 D 3370 D 3557 D 3558 D 3559 D 3919 -D 4841 ,D 5810 D 5847 3.3.1:,.D 1129.4.4.1 ,.0,01%,(CuFeS2).,.4.2 ,ASTM D 1688-12 4 .,.,.4.3 ,.5.5.1 .,3.,.5.2 ,I,D1193.-,.II 3 ,American Chemical Society Washington DC.,(Analar Standards for Laboratory Chemicals),BDH Ltd.,Poole,Dorset,U.K.(United States Pharmacopeia and National Formulary),U.S.Pharmaceutical Convention,Inc.(USPC),Rockville,MD.ASTM D 1688-12 5 .6.6.1 D1066 D3370 ,.6.2 (HNO3,.1,42)pH 2 ,2/.,(325)0,45.D4841.1 ,pH ,14.,.A ,7.7.1 .7.2 0,05 5/.5/.7.3 ,.,.ASTM D 1688-12 6 8.8.1 -./.(D3557),(D1687),(D3558),(D1068),(D3559),(D858),(D1886)(D1691).9.9.1,(8000/),(5000/),(2000/),(1000/),(10/).9.2 -(.B).2 .10.10.1-,324,7.3 .,324,7,.ASTM D 1688-12 7 10.1.1 (),.10.2 .11.8.10.3 .11.9.10.4 ,.11.11.1 ,(1,0 =1,0 Cu)1,000 ,250 15 HNO3(.1,42)15 .4 H2SO4(1+1)SO3.,1.11.2 ,(1,0 =0,1 Cu)100,0 1.11.3 (.1,19)(HCl).4 ,HCl ,.HCl (6 N HCl).,HCl ,HCl .11.4 (.1,42)(HNO3).5 ,NO3 ,.ASTM D 1688-12 8 11.5 (1+499)1 HNO3(.1,42)499 .11.6 (H2SO4).11.7 (1+1),1 (H2SO4,.1,84)1 .11.8:11.8.1,.11.9:11.9.1 .,.50 .(345).6 :,(),.12.12.1 100 ,(11.2)HNO3(1+499).,.12.2 0,5 HNO3(.1,42)(11.4),13.2 13.4.13.5.ASTM D 1688-12 9 12.3 .HNO3(1+499)(11.5).12.4 .,.13.13.1 100,0 125.7 ,13.5.13.2 5 HCl(.1,19)(11.3).13.3 ,15-20,.8 ,-.9 ,.,.0,5%.13.4 ,100.ASTM D 1688-12 10 .13.5 324,7.HNO3(1+499)(11.5).14.14.1 ,(.12.4).15.4 15.1 ,.15 ,270.15.2 ,.,.15.3 D2777-77,.,1.4 D 2777-08,D 19.ASTM D 1688-12 11 15.4 :,II:S=0,020X+0,035 ST=0,052X+0,123 :S=0,016X+0,033 ST=0,060X+0,039:S-,S-,X-,/.15.5 ,.1.1 A ,Cu/,Cu/,%,95%4,0 4,11+2,75 2,0 2,06+3,0 0,4 0,46+15,0 4,0 4,03+0,75 2,0 2,02+1,0 0,4 0,41+2,5 4 -ASTM International.RR:D19-1037.ASTM D 1688-12 12 B ,-16.16.1 .16.2 50 500/.500/.16.3 ,50%NaCl(50000/).,.17.17.1 -.,.,.,8.1,.-(D 3557),(D 3558),(D 1068),(D 3559),(D 1886)(D 1691).ASTM D 1688-12 13 18.18.1.9.19.19.1 ,10.20.20.1 (1/)0,1 100 50%.20.2 (CHC13).20.3 ,(1,0 =1,0 Cu)1,000 ,250,15 HNO3(.1,42)15 .4 H2SO4(1+1)SO3.,1.20.4 ,(1,0 =10 Cu)10,0 1 HNO3(.1,42)1.20.5 ,(1,0 =1,0 Cu)10,0 100.20.6 (.1,19)(HCl)(.5).20.7 (1+2)1 HCl(.1,19)2 .20.8 (1+49)1 HCl(.1,19)49 .ASTM D 1688-12 14 20.9 (.1,42)(HNO3)(.5).20.10 -36 1 CHC13.30 CS2 ,.2 CHC13.10 :.20.11 (100/)100 (NaOH)1.20.12 (H2SO4).20.13 (1+1),1 (H2SO4,.1,84)1 .20.14 .11.8.20.15 .11.9.21.21.1 ,0,0 50,0 ,0,0 50,0 (20.5)100.21.2 125,0,5 HNO3(.1,42)(20.9),22.2 22.15.,22.5 22.15.21.3 ASTM D 1688-12 15 .22.22.1 ,50,0 (100),125 100.11 ,50,0 (100),250 22.5.22.2 5 HCl(.1,19)(20.6).22.3 ,15-20,.12 ,-.13 ,.,.0,5%.22.4 ,250.100.ASTM D 1688-12 16 22.5 2 (20.1).22.6 pH NaOH(100/)(20.11),.HCl(1+49)(20.8),;2,5 HCl(1+49)(20.8).pH 2.3.14 22.6 pH pH-.22.7 10 -2.(.10.)22.8 ,CHC13 100.22.9 10 CHCl3(20.2)CHC13 .15 CHC13 ,CHC13 .22.10 ,.16 :.17 ,.,.ASTM D 1688-12 17 0,5%.22.11 45 2 HNO3(.1,42)(20.9),.22.11.1 ,.22.12 ,.22.13 2 HCl(1+2)(22.7)1.22.14,10 .22.15 324,7.23.23.1 ,10.(.21.3.).,1:,/AB1000(1):ASTM D 1688-12 18 1000=1000/A ,.24.4 24.1 ,.120.24.2 ,50%NaCl(50000/).,.24.3 3 D 2777-77,.,1.4 D 2777-08,D 19.24.4 :,II:S=0,119X+9 ST=0,247X+47 :S=27 ST=0,270X+42:ASTM D 1688-12 19 S ,/,ST ,/X ,/.24.5 ,.2.2 ,Cu/,Cu/,%95%300 290-3,3 100 112+12,0 20 65+225 300 234-22,0 100 93-7,0 20 49+145 C ,25.25.1 .25.2 5 100/.,-(.A).25.3 ,ASTM D 1688-12 20 ,.26.26.1 -.,().,.D 3919.26.2 .26.3 .,.,.27.27.1 D3919.ASTM D 1688-12 21 28.28.1-,324,7 .18 ,324,7,.19 .28.2 (),.28.3 ,.28.4 ,.28.5,.1 100.28.6 ,(,.).28.7 .29.29.1 ,(1,0 =1,0 Cu).20.3.29.2 ,(1,0 =10 Cu).20.4.29.3 ,(1,0 =0,10 Cu)10,0 (29.2)1 HNO3(.1,42)1.ASTM D 1688-12 22 .29.4 (.1,42)(HNO3).(.6.)29.5,.30.30.1 .,D 3919.31.31.1 ,/,HNO3(1+1),.,HNO3(1+1).31.2 100,0 125.31.3 HNO3(.1,42)5/,31.4,31.5 31.6.,0,45,HNO3(.1,42)5/31.6.31.4 95C