ASTM_D_2036_-_09_2015_rus.pdf

:D2036-09(2015.)STANDARD TEST METHODS FOR CYANIDES IN WATER 2017 ():20.11.2017:3324-17/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D2036-09(2015)1 :D2036-09(2015.)1 D2036;,.().1.1.1 .:A 12-18 B 2 19-25 C 26-32 D ()33-39 1.2 .1 ASTM D19 ,D19.06 .15 2015.2015.1964.2009.D2036-09.DOI:10.1520/D2036-09R15.2 .Lancy,L.E.Zabban,W.,ASTM STP 337,1962,.32-45.ASTM D2036-09(2015)2 1 ,-.CNCl ,A1.1.3 .,.2 ,.1.4 ,.D6994.1.5 ,.1.6 .1.7,.1.8 ,.,.ASTM D2036-09(2015)3 5.1,8.8,8.18,9,11.3 16.1.9.2.2.1 ASTM:3 D1129,D1193 D2777 ,D19 D5788 D5847 D6696 D6888 ,D6994 ,-D7284 ,D7365 E60 ,3 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D2036-09(2015)4 E275 3.3.1:3.1.1 ,.D1129 D6696.3.2:3.2.1 FIA 3.2.2 HPLC 3.2.3 IC 3.2.4 PAD 4.4.1 (HCN).,D6888,.4.2 A ,1-.4.3 B ASTM D2036-09(2015)5 .4.3.1 ,.4.4 C ,1-.4.5 D .4.6 ,0,005/,D6888 0,002/,0,4/0,05/.,.4.7 :0,03/;1,0/0,03/.D6888 0,002/.5.5.1 .,(X1).5.2 D ASTM D2036-09(2015)6 .,B .5.3 ,A1,.6.6.1 ,.6.2 ,.D7365 .7.7.1 1-,.8,6.Allihn.,.1.,100 4%.ASTM D2036-09(2015)7 .1 7.1.1 50-MIDI 6-MicroDist(),D7284,40.,.,500-;.7.2 ,578,1,0-,2,0-,5,0-10,0-.,E60.E275.7.3 ,-,.7.4,.7.5 ,2-5-,0,01.Allihn ASTM D2036-09(2015)8 7.6 ,10-.7.7 ,Dionex IonPac AS7,4 250,().8.8.1 .,.4 ,.8.2 ,I II,D1193.8.3 (1+9)1 9 .8.4 410 (NaC2H3O23H2O)500 .,pH=4,5,500.8.5 .4 ,DC.,.,BDH Ltd.,Inc.(USPC),MD.ASTM D2036-09(2015)9 8.6 (50/)5 (Ca(OCl)2)100 .8.7 -T(10/)1,0 -T 100 .8.8 (1 =250 CN)0,6258 (KCN)40 (40/).1 .(.16.2).(KCN ,(.9).,.8.8.1 I(1 =25 CN)(100)KCN 1 NaOH(1,6/).8.8.2 II(1 =2,5 CN)100 I 1 NaOH(1,6/).8.8.3 III(1 =0,25 CN)100 II 1 NaOH(1,6/).8.8.4 IV(1 =0,025 CN)100 III 1 NaOH(1,6/).8.9 ,3%10 30%-(H2O2)100.8.10,(ASTM D2036-09(2015)10).8.11 (PbCO3),(Pb(C2H3O2)23H2O)(Pb(NO3)2),50/.8.12 (Ca(OH)2),.8.13 510 (MgCl26H2O)1.8.14 -.8.15 -15 250-,.75 .15 (.1,19),.6,.;.8.16 (0,2/)0,02 -100 .8.17 (0,01 N)1,6987 (AgNO3)1.,.8.18 (20/)2 NaAsO2 100 .(ASTM D2036-09(2015)11 .)8.19 (40/)40 (NaOH)1 .8.20 (1,6/)40 NaOH(40/)1.8.21 (133/)133 1.8.22 (500/)785 (Na2S2O35H2O)1.8.23 (1+1)1 (H2SO4,.1,84)1 ,.8.24 (100/)120 Zn(C2H3O2)22H2 500 .1.8.25 ,(75 ,250 0,05%(.)8.25.1 20,50 NaOAc 500-600 18-.980 18-.0,2-.5,97 (3,9)NaOH(50%)0,4495 (0,50).1015 (1,0)18-.,.0,25/(2)1,00/(4).8.26.8.27 (50%.).50%(.).ASTM D2036-09(2015)12 .8.28 .9.9.1 -.(HCN).,.9.2 ,.9.3 ,.10.10.1 D7365.11.11.1.D7365 .11.2 ,ASTM D2036-09(2015)13 .11.3 ,.(1+9)pH 6-7(,).,(),20%.HCN ,pH.pH 12 12,5 NaOH.11.4 ,.,pH.D7365.11.5 ,pH .11.6 ,.,50 0,4 (40/)500 ,ASTM D2036-09(2015)14 3 .11.7 .,.,.,-T .-T,-,.,-T ,.11.7.1 ,(16.5).,50/,D6888.11.7.2 ,.,D6888.0,6/;24.11.7.3 (.16.5 )A ,ASTM D2036-09(2015)15 .11.8 .D ,.11.9,D.A 12.12.1 ,().12.2 ,.,.12.3 ,D6888.12.4 ,-.12.5 /ASTM D2036-09(2015)16 ,.,.13.13.1 6 .13.2 10 11.14.14.1 .1.14.2 .7.15.15.1.8.16.16.1 :16.1.1 ,.1.16.1.2 10,0 1 M NaOH .,.225 .16.1.3 .16.1.4 500 .,ASTM D2036-09(2015)17 10/,5 ,500 .A1 .,500 .16.1.5 .16.1.6 1 ,.16.1.7 20 (8.13).,15 (8.21).16.1.8 3.16.1.9 50 H2SO4(1+1).(,.)16.1.10 .,.16.1.11 ,16.1.6.16.1.12 1.16.1.13 ,15.16.1.14 500-250-.ASTM D2036-09(2015)18 16.1.15 .16.1.16 (16.2),(16.3),(16.4),(16.5),D6888(16.6).4.6 4.7 .16.2 :16.2.1 100 ,100 NaOH(1,6/),.16.2.2 0,5 .16.2.3 (8.17),-.16.2.4 100 NaOH(1,6/)(8.20).16.2.5 1(17.1).16.3 :16.3.1:16.3.1.1 (.1).50-.16.3.1.2 16.3.2.2 16.3.2.6.16.3.1.3 (17.2.1).16.3.2:16.3.2.1 ,50-ASTM D2036-09(2015)19 .1.,CN/,50 1,0 5,0 10,0 IV 5,0 0,0025 X IV 10,0 0,0050 X X IV 15,0 0,0075 X X IV 20,0 0,0100 X X IV 25,0 0,0125 X X IV 30,0 0,0150 X X IV 40,0 0,0200 X III 5,0 0,0250 X X III 10,0 0,0500 X III 15,0 0,0750 X III 20,0 0,1000 X III 25,0 0,1250 X III 30,0 0,1500 X 0,0()X X X 16.3.2.2 40 NaOH,.16.3.2.3 40 NaOH,.().16.3.2.4 1 -T 1 ,2.16.3.2.5 5 -,8 .16.3.2.6 578.(A).ASTM D2036-09(2015)20 16.3.2.7 (CN/),17.2.16.4 :16.4.1:16.4.1.1 100-I,II,III IV 250-.16.4.1.2 16.4.2.2 16.4.2.3.16.4.1.3 10-50-IV 250-100 NaOH(1,6/).16.4.1.4 16.4.2.2 16.4.2.3,.16.4.1.5 ,.16.4.2:16.4.2.1 100 (,100 NaOH(1,6/)250-.3 .,PbCO3,Pb(C2H3O2)2.16.4.2.2 ,.16.4.2.3 -ASTM D2036-09(2015)21 .16.4.2.4 ,5(17.3).16.5 :16.5.1:16.5.1.1 2 I,II,III IV HPLC ,.16.5.1.2 16.5.2.1 16.5.2.4 10 .4 10-.,10-.16.5.1.3 .16.5.1.4 .16.5.2:16.5.2.1 ,:():1,0/.(b),ASTM D2036-09(2015)22 ,0,05 Ag/AgCl,.,.(c),Dionex IonPac