ASTM_D_1783_-_01_2012e1_rus.pdf

D 1783-01(2012.)1 STANDARD TEST METHODS FOR PHENOLIC COMPOUNDS IN WATER ():2619-15/ASTM :12.05.2015 2015 (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.-,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/ASTM D 1783-01(2012)1 D 1783-01(2012.)1 1 D 1783;,.().1 2015.1.1.1 .(C6H5OH)4-,.ASTM D19 ,D19.06 .15 2012.2012.1960.2007.D1783-01R07.DOI:10.1520/D1783-01R1201.1ASTM D 1783-01(2012)1 ,.1.2 -4-,-,4-.1.3 ,:A 0 100/11 17 B 0,1/(100/)18 24 1.4 .1.5 ,.,.6.3.2 8.6.2.2.1 ASTM:2 D 1129,2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.2ASTM D 1783-01(2012)1 D 1192 (2003.)3 D 1193 D 1293 pH D 2777 ,D19 D 3370 D 5789 (2003.)3 D 5810 D 5847 3.3.1 ,.D 1129.3.2 ,:3.2.1 .4.4.1 A B ,4-.4.2 A B 3 .www.astm.org.3ASTM D 1783-01(2012)1,20-.4.3 ().,.,.5.5.1 .5.2 ,.6.6.1 ,.,.6.2 ,4ASTM D 1783-01(2012)1.,(),.6.3 .8 .6.3.1 ,.().,.6.3.2 ,o(H2S)(SO2),.(H2SO4)(HCl),(CuSO4)-,(CuS).H2S SO2 CuSO4,.(CO2),SO2,H2S ,5ASTM D 1783-01(2012)1.,).6.3.3 ,.CuSO4 .12 12,5 (NaOH).(CCl4).,.CCl4 .1 CuSO4,NaOH (Cu(OH)2),.7.7.1 .,5 .7.2 ,460 (A),510 (B),1,0 10.1,0,.7.3 1,6ASTM D 1783-01(2012)1 ,.7.4 pH-D1293.8.8.1 .,4.,.8.2 ,I,II,III IV D 1193.,.,20.8.3 (20/)2,0 4-100.2 4-108,0 109,5C.8.4 (20/)20 4 ,.,Analar Standards for Laboratory Chemicals,BDH Ltd.,Poole,Dorset,U.K.United States Pharmacopeia and National Formulary,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD().7ASTM D 1783-01(2012)1 (NH4Cl)1.8.5 (NH4OH)(0,90)(NH4OH).8.6 (CCl4).,.,.8.7 (CHCl3).8.8 (HCl)(1,19)(HCl).8.9 ,(1 =10 )1,00 (C6H5OH)1000 .30.8.10 ,(C6H5OH)(1 =10 )10,0 1000 .8.11 ,(C6H5OH)(1 =1,0 )50 500 .2 .8.12 -(K3Fe(CN)6)(80/)8,0 (K3Fe(CN)6)100.-.8.13 (NaHSO4).8.14 (Na2SO4),.8.15 (H2SO4)(1,84)8ASTM D 1783-01(2012)1 (H2SO4).8.16 (H2SO4)(1+9).9.9.1 D 1192 D 3370.9.2 4C .4.,10 .10.10.1 ,.4 .0,5 2,0 H3PO4,HCl,H2SO4 NaHSO4.10.2 ,2C 4C.,28 .9ASTM D 1783-01(2012)1 A 11.11.1 ,100/(0,1/).,.11.2 ,.11.3 (),.12.12.1 4-pH,10,0 0,2,K3Fe(CN)6.()460./(C6H5OH).13.13.1 500 10ASTM D 1783-01(2012)1 0,5,10,20,30,40 50 C6H5OH(1 =1,0 C6H5OH).13.2 -,14 15.13.3 460 ,.().3 .14.14.1 500 .pH pH 0,5 4 H2SO4(1+9).-.10.1,.500.14.2 450 .50 .14.3 ,.H2SO4(1+9).,.11ASTM D 1783-01(2012)1 .15.15.1 500 ,500,50 .,500 .15.2 25 NH4Cl .H 9,8 10,2 NH4OH.1.3,0 4-(20/),3,0 K3Fe(CN)6 .3.4 -,.15.3 25,0 (1,0 5,0).10 50,0 .,.15.4 ,5 12ASTM D 1783-01(2012)1 Na2SO4 ,.15.5 ,460.(.13),.16.16.1 /:/=W 100/V:W-,500,V-500,4-,.5 ,(C6H5OH).,.,.13ASTM D 1783-01(2012)1 17.5 17.1 .C6H5OH ,.,.,/,/.1.()17.2 ,:(2),(3),(1),(1),5 -ASTM International RR:D19-1132.ASTM Customer Service serviceastm.org.14ASTM D 1783-01(2012)1 (1).,.,.,.17.3 D 2777.,.1.A 6,460/34,780/67,900/2,840/32,840/66,260/n 23 23 23 24 24 23 S 3,384 4,190 8,923 2,494 3,957 8,147 So 2,718 5,320 7,300 2,528 3,243 5,850 So:C.V.A 38%10,8%11,8%46,6%9,9%1,8%A (So-),100.17.4 .1,:ST-,SO-.,.15ASTM D 1783-01(2012)1 ,/,/.2.()17.5 ,.2 .1 2.2.A ,/,/,/,%7,154 6,460-0,693-9,7 35,768 34,780-0,990-2,8 71,535 67,900-3,631-5,1 ,/,/,/,%7,154 5,430-1,729-24,0 35,768 32,840-2,930-8,2 71,535 66,260-5,274-7,4 16ASTM D 1783-01(2012)1 B 18.18.1 ,0,1/.6 0,005/10.18.2 ,.18.3 (),.19.19.1 4-pH,10,0 0,2,K3Fe(CN)6.510./(C6H5OH).20.20.1 100 0,5,10,20,30,40 50 C6H5OH(1 =0,01 ).17ASTM D 1783-01(2012)1 20.2 ,22.20.3 ()510 ,.(.3).21.21.1.14.7 100 (100 ),1/5 .,.22.22.1 100 ,100,0,5 .,100 .22.2 5 NH4Cl .H 9,8 10,2 NH4OH.2,0 4-(20/),2,0 K3Fe(CN)6 .22.3 15 510.18ASTM D 1783-01(2012)1 (.20),.23.23.1 /:/=W 1000/V:W-,100,V-100,4-,.24.5 24.1 .C6H5OH ,.,.24.2 ,:(1),(1),(3),(1),(1),(1),(1).19ASTM D 1783-01(2012)1,-.,.24.3 D 2777.,.24.4 .3,:ST-,SO-.ST SO ():ST=-0,056+0,039X r2=100,0%SO=-0,094+0,036X r2=98,2%:X ,.3.B 6,930/34,430/68,780/6,960/34,240/68,940/n 27 27 26 26 26 26 S 0,228 1,274 2,653 1,11 1,113 3,152 So 0,226 1,035 2,460 0,337 1,080 2,460 So:C.V.A 3,3%3,0%3,5%4,7%3,1%3,5%A (So-),100.20ASTM D 1783-01(2012)1 ,/,/.3.(-)4.B ,/,/,/,%7,154 6,930-0,224-3,1 35,768 34,430-1,338-3,7 71,535 68,777-2,758-3,9 ,/,/,/,%7,154 6,958-0,196-2,7 35,768 34,242-1,526-4,3 71,535 68,942-2,593-3,6 21ASTM D 1783-01(2012)1 ,/,/.4.()24.5 ,.4 .3 4.25.25.1 ,:25.2 :25.2.1:25.2.1.1 .25.2.1.2 ,22ASTM D 1783-01(2012)1 .25.2.1.3 ,.25.3 :25.3.1 ,-,.,.25.3.2 (),(IRM),C6H5OH 30/()30/().,.,.25.3.3 ,.5.25.3.2,D 5789 D 5847.23ASTM D 1783-01(2012)1 5.LCS LCS 30/(A)1