ASTM_D_2030_-_97.pdf

Designation:D 2030 97Standard Test Method forWater Solubility of Refined Pyridine1This standard is issued under the fixed designation D 2030;the number immediately following the designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon(e)indicates an editorial change since the last revision or reapproval.1.Scope1.1 This test method covers the determination of the solu-bility of refined pyridine in water.1.2 This standard does not purport to address all of thesafety concerns,if any,associated with its use.It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.For a specifichazard statement,see Section 6.2.Referenced Documents2.1 ASTM Standards:D 1193 Specification for Reagent Water2D 3437 Practice for Sampling and Handling Liquid CyclicProducts32.2Other Document:4OSHA Regulations,29,CFR,paragraphs 1910.1000 and1910.12003.Summary of Test Method3.1 Specific volumes of pyridine and water are mixed,allowed to stand for 30 min at room temperature,and theclarity of the solution noted.4.Significance and Use4.1 Water solubility is a qualitative detection of oil contami-nants in pyridine.5.Reagents5.1 Purity of WaterUnless otherwise indicated,referencesto water shall be understood to mean reagent water conformingto Types I to IV of Specification D 1193.6.Hazards6.1 Consult current OSHA regulations,suppliers MaterialSafety Data Sheets,and local regulations for all materials usedin this test method.7.Sampling and Handling7.1 Sample the material in accordance with PracticeD 3437.8.Procedure8.1 Measure 10 mL of pyridine specimen in a 100-mLmixing cylinder and dilute to 100 mL with water.Stopper andmix thoroughly by shaking.Let stand for 30 min at roomtemperature.8.2 Fill another cylinder with 100 mL of water and comparethe clarity of the specimen solution with that of the water.9.Report9.1 Report the appearance of the specimen solution as“clear,”“very slightly cloudy,”“slightly cloudy,”or“cloudy.”NOTE1If clear the specimen“passes”;if other than clear thespecimen“fails.”10.Precision and Bias10.1 This test method for measuring water solubility ofpyridine has no precision nor bias because the value of watersolubility of pyridine is defined only in terms of this testmethod.11.Keywords11.1 pyridine;solubility;water solubilityASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard.Users of this standard are expressly advised that determination of the validity of any such patent rights,and the riskof infringement of such rights,are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised,either reapproved or withdrawn.Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters.Your comments will receive careful consideration at a meeting of theresponsible technical committee,which you may attend.If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards,at the address shown below.1This test method is under the jurisdiction of ASTM Committee D16 onAromatic Hydrocarbons and Related Chemicals and is the direct responsibility ofSubcommittee D16.03 on Organic Nitrogen Compounds.Current edition approved Dec.10,1997.Published August 1998.Originallypublished as D 2030 64 T.Last previous edition D 2030 93.2Annual Book of ASTM Standards,Vol 11.01.3Annual Book of ASTM Standards,Vol 06.04.4Available from Superintendent of Documents,U.S.Government PrintingOffice,Washington,DC 20402.1Copyright ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.NOTICE:This standard has either been superceded and replaced by a new version or discontinued.Contact ASTM International(www.astm.org)for the latest information.This standard is copyrighted by ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.Individual reprints(single or multiple copies)of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585(phone),610-832-9555(fax),or serviceastm.org(e-mail);or through the ASTM website(www.astm.org).D 20302NOTICE:This standard has either been superceded and replaced by a new version or discontinued.Contact ASTM International(www.astm.org)for the latest information.