ASTM_D_1886_-_14_rus.pdf

D 1886-14 STANDARD TEST METHODS FOR NICKEL IN WATER ():2753-15/ASTM :29.10.2015 2015 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 1886-14 1 D 1886-14 1 D 1886;,.()1.*1.1 2,3,4 .:A ,0,1 10/7-16 B ,-10 1000/17-26 C ,5 100/27-36 1.2 A,B C 1 ASTM D19 D19.05 .1 2008.2008.1961.2003.D1886-03.DOI:10.1520/D1886-08.2 Chilton,J.M.,25,1953,.1274-1275.3 Platte,J.A.Marcy,V.M.,1965.4 Brown,E.,Skougstad,M.W.Fishman,M.J.,.,5,1970,.115.ASTM D 1886-14 2 .C ,.1.3,.,.1.4 ,.,.5,.11.8.1,21.11,23.7 23.10.1.5 .X1.2.2.1 ASTM:5 D 858 D 1066 D 1068 D 1129,D 1193 D 1687 5 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 1886-14 3 D 1688 D 1691 D 2777 ,D19 D 3370 D 3557 D 3558 D 3559 D 3919 -D 4841 ,D5673 -D 5810 D 5847 3.3.1:3.1.1 ,.D 1129.3.2 ,:3.2.1 ,.ASTM D 1886-14 4 4.4.1 ,.A,B C .4.2 .6 ,pH,.4.3 -,.5.5.1 .,.7 ,.6 .EPA-570/9-76-003 1976.1980.,401 M ST.,S.W.,DC 20406.7 ,DC.,.,BDH Ltd.,Poole,Inc.(USPC),MD.ASTM D 1886-14 5 5.2 ,D 1193,I.,.II.6.6.1 D 1066 D 3370 .6.2 HNO3(.1,42)pH 2 ,2/.,0,45-.D 4841.1 ,pH ,14.,24 ,.,.A ,7.7.1 ,.7.2 ASTM D 1886-14 6 0,1 10/.8.8.1 -.(D 3557),(D 1687),(D 3558),(D 1688),(D 1068),(D 3559),(D 858)(D 1691).9.9.1,(9000/),(4000/),(2000/),(10/).2 ,-.10.10.1-,232,0.3 ASTM D 1886-14 7 .232,0,.10.2 .10.3 ,.11.11.1 .0,45-.:,.,.11.2 (.1,19)(HCl).4 ,HCl .5 HCl ,(6 N HCl).,HCl,HCl.11.3 (.1,42)(HNO3).6 ,HNO3 .11.4 (1+499)1 HNO3(.1,42)ASTM D 1886-14 8 499 .11.5 (1,0 =1,0 Ni)4,953 Ni(NO3)26H2O 10 HNO3(.1,42)100 .1 .11.6 (1 =0,1 Ni)100,0 1 of HNO3 1.11.7:11.7.1,.11.8:11.8.1 ,.,.345 (50 .).(,).12.12.1 ,HNO3(1+499),11.6.(100),.12.2 0,5 HNO3(.1,42),13.2 13.4.ASTM D 1886-14 9 13.5.12.3 ,.HNO3(1+499).12.4 ,.13.13.1 100,0 125-.7 ,13.5.13.2 5 HCl(.1,19)(11.2).13.3 ,15 20,.8 .9 ,.,.(65C 85C).,ASTM D 1886-14 10 0,5%.,.13.4 (11.1),100-.13.5 .HNO3(1+499).14.14.1 ,12.4.15.8 15.1 ,.1;.2.15.2 .8 -ASTM International RR:D19-1038.ASTM Customer Service serviceastm.org.ASTM D 1886-14 11 1 ,(A):(X),/7,74 0,84 3,93 ST 0,502 0,102 0,383 SO 0,261 0,045 0,324 :(X),/7,74 0,84 3,87 ST 0,629 0,108 0,401 SO 0,420 0,067 0,192 15.3 D 2777-77,.,1.4 D 2777-13,D19.2 ,(A),/,/-,/-,%(95%-):8,0 7,74 0,26 3 0,8 0,84+0,04+5 4,0 3,93 0,07 2 :8,0 7,74 0,26 3 0,8 0,84+0,04+5 4,0 3,87 0,13 3 16.16.1 ,ASTM D 1886-14 12 ,.16.2 :16.2.1 ,(.12.3).0,990.16.2.2 .15%.16.2.3 ,.16.2.4 (CCB)(CCV)10%.15%.16.3 :16.3.1 ,.,.16.3.2 ,.,ASTM D 1886-14 13 .,.16.3.3 .2.,.1.,D 5847 F t .16.4 (LCS):16.4.1 ,LCS ().LCS ,.,LCS,15%.16.4.2 ,.16.5 :16.5.1 .,0,5 .,ASTM D 1886-14 14,.16.6 (S):16.6.1 ,S .16.6.2 .,2-5 ,10-50 ,.16.6.3 (P),:P=100 A(Vs+V)BVs/CV :A-(/),-(/),-(/),Vs-(),V-().16.6.4 ,D 5810,.1.ASTM D 1886-14 15,.:;,;.10 .D 5810.16.7 :16.7.1 ,.,(MSD).16.7.2 ,F.F .6.4.4 D 5847.16.7.3 ,.16.8 (IRM):16.8.1 ,(IRM),().IRM .ASTM D 1886-14 16 ,.B ,-17.17.1 ,NaCl.17.2 10 1000/.18.18.1 -.,.,.-.,8.1,.-(D 3557),(D 3558),(D 1688),(D 1068),(D 3559)(D 1691).ASTM D 1886-14 17 19.19.1.9.1.20.20.1 ,10.21.21.1 ()(1/)0,1 100 50%-.21.2 (CS2).21.3 (CHCl3).21.4 .11.1.21.5 (.1,19)(HCl)(.4 .5).21.6 (1+2)1 (HCl),.1,19,2 .21.7 (1+49)1 (HCl),.1,19,49 .21.8 (1,0 =200 Ni)0,9906 (Ni(NO3)26H2O),1 HNO3(.1,42),1.21.9 (1,0 =2,0 Ni)10,0 1 HNO3(.1,42)1.21.10 (.1,42)ASTM D 1886-14 18 (HNO3)(.6).21.11 -36 1 CHCl3.30 CS2 ,.2 (CHCl3).,.(.).21.12 (100/)100 (NaOH)1.().21.13 .11.7.21.14 .11.8.22.22.1 ,0,0 100 0,0 50,0-100 (21.9).,.22.2 125-,0,5 HNO3(.1,42)(21.10)23.2 23.15.250-23.5 23.15.ASTM D 1886-14 19 22.3 ,.23.23.1 (100),100 ,125-100 .11 ,(100),10,0 ,250-23.5.23.2 5 HCl(.1,19)(21.5).23.3 ,15 20,.9.12 .23.4 (21.4),250-.100.23.5 2 (21.1).23.6 pH NaOH(100/)(21.12).HCl(1+49)(21.7);2,5 HCl(1+49).pH 2.3.13 pH 23.6 pH-.ASTM D 1886-14 20 23.7 10 -(21.11)2.(.).23.8 ,CHCl3 100-.23.9 10 CHCl3(21.3)CHCl3 .14 -CHCl3,CHCl3 .23.10 ,.().9.23.11 45 2 HNO3(.1,42)(21.10),.(,).23.12 ,.9.23.13 2 HCl(1+2)(21.6),1.15 (1+2)ASTM D 1886-14 21 ,-(21.11).23.14 10-.23.15 .24.24.1 ,22.3.,:,/=(1000/A)B:1000=1000/A-,-,.25.5 25.1 ,.3;.4.ASTM D 1886-14 22 3 ,-(B):(X),/784,2 56,8 398,5 ST 146,4 15,2 35,1 SO 41,02 9,18 22,97 :(X),/794,4 53,6 399,4 ST 133,9 11,2 37,7 SO 70,9 12,6 11,1 25.2 .4 ,-(B),/,/-,/-,%(95%-):900 784,2-115,8-12,9 50 56,8+6,8+13,6 400 398,5-1,5-0,4 :900 794,4-105,6-11,7 50 53,6+3,