ASTM_D_1796_-_11_rus.pdf

,()INTERSTATE COUNCIL FOR STANDARDIZATION,METROLOGY AND CERTIFICATION(ISC)317342012,1.092 .1.22009.,-.,-,1-(),-160 ,42 3 ,(-1 2012.51-):(3166)00497 (3166)00497 AZAMBYKGMDRUTJ -4 ASTM D 1796-11 Standard test method for water andsedimentinfueloilsbythecentrifugemethod(laboratoryprocedure)().D02.02 -ASTMD02API-(ASTM).ASTM,-,ASTM,-.-1.52001(3.6).ASTM.(en).(IDT)5 15 2012.893-317342012-1 2014.6 -,-.().,-,2013-,II 3173420121 .12 .13 .24 .25 .36 .57 .68 .69 .810 .811 .8.1().10III 317342012 Fuel oils.Method for determination of water and sediment by centrifuge method 201407011 1.1 0%30%().1 ,-,-.ASTM D 95(API MPMS,-10.5)ASTM D 473(API MPMS,10.1).2 API MPMS,10.6(ASTM D 1796)API MPMS,10.3(ASTM D 4007)API 2548.1.2,.,.1.3,-.,-.6.1.2 .-().2.1 ASTM1):ASTM D 446-07 Test method for water in petroleum products and bituminous materials by distillation()ASTM D 473-07 Test method for sediment in crude oils and fuel oils by the extraction method()ASTM D 4007-11 Test method for water and sediment in crude oil by the centrifuge method(laboratoryprocedure)(-)ASTM D 4057-06(2011)Practice for manual sampling of petroleum and petroleum products(-)ASTMD4177-95(2010)Practiceforautomaticsamplingofpetroleumandpetroleumproducts(-)1)ASTM ASTM website,www.astm.org ASTM serviceastro.org,ASTM(Website standsrds Document Summary).1 317342012ASTM D 5854-96(2010)Practice for mixing and handling of liquid samples of petroleum and petroleumproducts()ASTM D 6304-07 Test method for determination of water in petroleum products,lubricating oils,andadditivesbycoulometricKarlFischertitration(,-)ASTM 542-01(2007)Practice for calibration of laboratory volumetric apparatus()2.2 API2):API MPMS Chapter 8.1(R2006)Practice for manual sampling of petroleum and petroleum products(ASTM D 4057)()API MPMS Chapter 8.2(R2010)Practice for automatic sampling of petroleum and petroleum products(ASTM D 4177)()API MPMS Chapter 8.3(R2010)Practice for mixing and handling of liquid samples of petroleum andpetroleum products(ASTM D 5854)()API MPMS Chapter 10.1(2007)Test method for sediment in crude oils by the extraction method(ASTM D 473)()APIMPMSChapter10.3(2008)Testmethodforwaterandsedimentincrudeoilbythecentrifugemethod(laboratoryprocedure)(ASTM D 4007)()APIMPMSChapter10.5(R2010)Testmethodforwaterinpetroleumproductsandbituminousmaterialsby distillation(ASTM D 95)2.3 IP3):Methods Book,appendix B.Specification for methylbenzenes(toluenes),-.()2.4 ISO4):ISO5272:1979 Tolueneforindustrialuse Specifications(.)3 3.1 .4 4.1 ,.-,-.4.2 ,.,-ASTM D 6304.2 3173420122).,1220 L.St.,N.W.,Washington,DC 20005.3),61 New Cavendish St.,London,WIG 7AR,U.K.4)(ANSI),25 W.43rdSt.,4thFloor,New York,NY10036,http:/www.ansi.org.5 5.1 5.1.1 ,()-203 (8),(rcf)500 800(5.1.6).5.1.2 ,-,-,.-().5.1.3 -.-(60?1)(140,0?1,8)F.-.5.1.4 .3 -,.5.1.5 ,(r/min),r/min=1335 rcf d,(1)rcf ;d ,;r/min=265 rcf d,(2)rcf ;d ,.5.1.6,-(r/min),rcf=dr min13352?,(3)d ,;rcf=dr min2652?,(4)d ,.5.2 5.2.1,1.,1,.-,3 317342012 .1 ,20(68 F).4 3173420121 ;2 ;3 10;4 1;5 1 203 (8)1 203 (8-),0 0,10,05?0,02 0 0,30,05?0,03 0 0,50,05?0,05 0 1,00,10?0,05 1,0 2,00,10?0,10 2,0 3,00,20?0,10 3,0 5,00,50?0,20 5,0 101,00?0,50 10 255,00?1,00 25 10025,00?1,005.2.2 ASTM542,(NIST)5)-.0,5;1,1,5,2,50 100.,-1,.5.3,-100.(60?1)(140,0?1,8)F(4).4 ,-60(140F).(),60,-.-(.1).6 6.1,IP ()ISO5272.(.,.-.-.)6.1.1 :C6H5CH392,14()10 ()2,0 (3,6 F)0,001%,H2SO4 ACS()0,003%)110,6.5 3173420125)(NIST),100 Bureau Dr.,Stop 3460,Gaithersburg,MD 20899-3460.5 -.6.1.2 (60?1)(140,0?1,8)F,.-.1.6.2 6.2.1 -,-.6.2.2()-.-.7 7.1 ,.7.2 ,ASTM D 4057(API MPMS,8.1)ASTM D 4177(API MPMS,8.2).7.3 ASTM D 5854(API MPMS,8.3).ASTMD5854(API MPMS,8.3).8 8.1 (5.2)50 .50 (6.1).50100.100 10 (60?1)(140,0?1,8)F.8.2 ,-.(60 (140 F),40 (104 F).,.)8.3 ,.10,5.1.6,(rcf)500800(2-,).-(60?1)(140,0?1,8)F(4).2 ,)500 rcf 800 rcf3051217102170330131650201035614159020006 317342012 2 )500 rcf 800 rcf3811515301930406161490187043217144018204571814001770483191360172050820133016805332113001640559221270160058423124015606102412101530),-.rcf .8.4 -(-,-)0,050,1 1 0,1 1.0,1 0,025(.2).0,025,0,025.-0,000.,10.8.5 -,-.,-.8.6-,(.-1),0,0025 0,10,7 317342012 2 -ASTM 100(5),9.-,0,025 0,10,.,8.1.9 9.1 .9.2 V,%.,V=V1+V2,(5)V1 50,;V2 50,.9.3,-.10 10.1 V,%.,3.3 ,1 ,2 ,%.0,00 0,0250,0250,0250,0250,050,0250,050,0750,050,050,100,050,0750,1250,0750,0750,150,0750,100,1750,100,100,200,100,150,2010.2 ,.10.2.1 2,0%.0,1%.10.2.2 0,20%.2,0%.0,05%.10.2.3 0,20%.,3.10.3 ,(5).-(6.2),.-,60 (140 F)(4).11 11.1(95%)-,11.1.1 11.1.2.8 31734201211.1.1,-,3.11.1.2 ,-3.11.2 -.11.3 11.3.1 (.-XIASTMD4007/APIMPMS,10.6),.0,06,-0,10.,-.11.3.2 ASTMD95(APIMPMS,10.5)-:0,08 0,1 0,11 0,2.0,1%1%.11.3.3 ,;-0,12,0,28.9 3173420121 ;2 3 .1().1.1 .1.1.1,.1.2 .1.2.1 .1.1 .0,03%-21(70F)0,17%70(158F).-,.-.-.1.3.1.3.1,IP ()ISO 5272.1.3.2 .1.4.1.4.1,1.(60?1)(140,0?1,8)F.10 317342012.1.1 .1.4.2 1 .1.5.1.5.1,.-?1.1.5.2 700800.(2,25),.30.1.5.3 30.,30.(60(140F),40(104F).,.).1.5.4,.1.5.3,.1.5.5 48.-,.,48(),-,.,.1.5.6 .-,.11 317342012 665.6.033:006.354 75.140IDT:,317342012 .03.12.2013.09.12.2013.60?