ASTM_D_4124_-_09_rus.pdf

,()INTERSTATE COUNCIL FOR STANDARDIZATION,METROLOGY AND CERTIFICATION(ISC)32269 2013 2014 322692013 II ,-1.092 .1.22009 .,.,1 160 -,-,-()-,4 2 3 ,(28 2013.58-):(3166)00497 (3166)00497 AM BY KZ KG MD-RU TJ UZ 4 ASTM D 412409 Standard test method for separa-tion of asphalt into four fractions(-).ASTM D02 -D02.05 ,.(en).-1.52001(3.6).ASTM,-,ASTM,-.(IDT)5 28-2013.751-322692013 1 2015.6 322692013 III -,.()-.,.,2014 -,-322692013 _ 1 Petroleum bitumens.Method of separation into four fractions _ 20150101 1 1.1 -:,-,.,-,-.1.2 .1.3 ,.-,-.1.4 ,.-.2 .(-)1).ASTM D 140 Standard practice for sampling bituminous materials()Manual on Hydrocarbon Analysis()2)3 -:3.1 (asphaltenes or alkane insolubles):,-().3.2 (naphthens):CnH2n,.1)ASTM ASTM website,www.astm.org ASTM serviceastm.org.ASTM ASTM Website standards Document Summary.2)ASTM PCN 03-332030-12.322692013 2 3.3 (naphthene aromatics):,-CG-20 -.3.4 ()petrolenes(maltenes):1),-()5 10,-;2),-,-.3.5 ()polar aromatics(resins):,-(50:50)-CG-20 -.3.6 (saturates):,CG-20 .4 4.1 ,-,.CG-20 ,-.-.3.5 5.1 -.1,2.,-,.6 6.1 /,-1(.6.1.1)322692013 3 -;b-,;-29/42;d 29/42 24/40;-24/40 1 /6.1.1 (1):-;b-,-;-29/42;d 29/42 24/40;24/40.6.2 ,2(.6.2.1 6.2.5).322692013 4 -25 3 -;b-;-LC-:c1-,c2-;3-;4-;5-/-;d-(:200-500;:0,1);-2 -6.2.1 LC-(2):25 3 ;b -;-LC-,:c1 ,c2 ,3 ,4 -,5 /;d -(:200-500,:0,1);.6.2.2-(2)-,-,-(),.6.2.3-(2),-,.0,1 5,0 3/0,1 3/.6.2.4 LC-70,1,5 (124 3).LC-,-,6,35 (1/4).6.2.5/,0 C 100 C 0,1 C,LC-,-15,9 (5/8)322692013 5 6.3 6.3.1 ,-,-(),.6.3.2 25 500 3 .6.3.3 .6.3.4 .6.3.5 60 100 3 (-10 15 ASTM).6.3.6 1 2 3.6.3.7 0,5 3.6.3.8 c 250,0,0001.6.3.9 .6.3.10 25 50 3,.6.3.11 .6.3.12 .6.3.13 24/40 29/42.6.3.14 15,9 (5/8).6.3.15 ,-1,59 (1/16)3,17 (1/8).6.3.16 6,35 (1/4)3,17 (1/8)3,17 (1/8).7 7.1 1)CG-20,425 -16,3 5.7.2 -.,-2).,-.7.3 7.3.1 (2,2,4-)0,01%.7.3.2-0,01%.7.3.3 0,01%.7.3.4 0,001%.7.3.5 0,02%,86,5 C 87,5 C.1)EMD Chemicals,Inc.,P.O.Box 70,480 Democrat Road,Gibbstown,NJ 08027(Prod-uct Code AX0612),CAS Number:1344-28-1,2.5 kg Chromatographic Grade Alumina(Al2O3)80-200 mesh CAS 1344-28-1,Cat#EM-AXO612-3.2)(-,).,.-,BDH,Inc(USPC),.322692013 6 8 8.1 ,-.MSDS .,.,.9 ()9.1 ,ASTM D 140.50 ,100 C.9.2 2,000 0,001 -500 3 M.,-,100 3 1 .500 3 (200,0 0,1)3 .9.3 ,1.500 3 -.500 3 -.(-1).-15,9 (5/8).1-.9.4 .(99).500 3 1 2 .1 (2).2-2 .-3.9.5 2 3 -,.2 ,-,2 (3).3 1020 3,.9.6 (60 3,-1015 ASTM)1 3 .-.9.7 ,9.2-9.5,-.9.8 ,1 3,(,).322692013 7 1 3 .-.9.9 100 3.500 3 ,30 -.1 2.,-,.500 3 ,.9.15.9.10 -,.4-,.-.9.11 ,-,.9.12 -1 3,(9.7 9.8).10 15 3.-50 3 .-,35 24 48.9.13 (22 .120 C 30 1).-M.-.9.14 ,9.9-9.11,1 3.,80.2 3 -.M,.-25 3 .-,M().9.15 50 3 -.10 20 3 500 3,9.9,.50 3 .,(-35)24 48 .(22 .120 C 30 1)-.,M().-.322692013 8 10 ()-10.1 LC-(2),-.10.2 (2),2.LC-,-.-(0,1 10,0 3/)-/,LC-,LC-30,5 (12),1,59 (1/16)3,17 (1/8),6,35 (1/4).30,5 (12)6,35 (1/4).30,5 (12)LC-6,35 (1/4).10.3-(2)-LC-()(),-,-LC-.10.4 -()LC-LC-(),15,9 (5/8);.11 (),-11.1 (),(1,0000 0,0001),9,-25 3 (5).(10,0 0,1)3-,-3 5 25 C.,40 50 30 40.5-,(),.11.2 70 1,5 (7.1),-.-.124 3 110 ,0,90/3.11.3 1 ),-,1,0%-(.-).322692013 9 1 /-),3 ,3)-150 33 183 67/50/50 75 142 150,-150)-.,1,0,1%(100).,.,.-,.)-,.11.4 -.-(70 3 )10 3.3,0 3/,.-10 3 -100 3 ./-(-).-/25 C(77 F)-.11.5 ,(11.1)25 3,(-).(6).-,5 10 3-.100 3 -500 3 ,.-,-.6-30.,.11.6 -(7)350 400 (3).7-,-.322692013 10 3 ,-11.7 -50 3,(-)(.)-500 3.,-,(.-,),.,-500 3,-,.,-500 3 ,.,-183 3 (150 3-33 3).-500 3 500 3 ,150 3 .-500 3,500 3.,33 3.,.,1.-,.11.8 ,150 3-33 3 .-(,),366,.322692013 11 ()-.,500 3.11.9.8.5,08 ,-.100 3 75 3 50:50 -.250 3.11.10.8.,-,.,-,-,.-,.,-,.-250 3.8 -,-.3,350,400.-.11.11 ,-1 3,-.,10 15 3 -.-25 3 .,-,35 24 48.,(22 .-120 30 1).,:S ,MNA ,MPA .322692013 12 12 12.1 ,%.,-,M :;)()(M=+(1);)(100100=+(2)(100100100ANAS=+;(3),100100100100ANAS=+(4)M(),;M(),;M ,;M ,;M ,;MS ,;NA ,;MPA ,.12.2 0,1%.13 13.1 .2 ,(),-,2 AC-30,SHRP 64-22 .2 (),(AC30,SHRP 64-22 ),%-23,7 25,0 76,2 72,5 ,%99,9 97,5 10,0 10,3 31,0 30,1 54,0 57,3 ,%96,6 97,8 13.2 ,-.,-.322692013 13 1 Corbett,L.W.,Composition of Asphalt Based on Generic Fractionation,Using Solvent Deasphal-tening,Elution-Adsorption Chromatography,and Densimetric Characterization,Analytical Chemistry,Vol.41,No.4,1969,pp.576579 2 Corbett,L.W.and Petrossi,U.,Differences in Distillation and Solvent Separated Asphalt Re-sidua,Ind.Eng.Chem.Prod.Res.Dev.,Vol.17,No.4,1978,pp.342346 322692013 14 ()-.1 -ASTM D 14009 -IDT 322682013 -.:IDT .322692013 15 665.775.5:006.354 75.140IDT :,01.04.2014.60 x841/8.2,33.31.1704.,123995,.,4.www.gostinfo.ruinfogostinfo.ru