ASTM_D_3942_-_03_2008_rus.pdf

D 3942 03(2008)STANDARD TEST METHOD FOR DETERMINATION OF THE UNIT CELL DIMENSION OF A FAUJASITE-TYPE ZEOLITE :1216-10/ASTM :31.05.2010 2010 (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FGU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FGU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.-,.9,-49,-1,119991.:(495)236-54-49,236-43-83:(499)230-13-72 E-mail:interstgost.ru Web:www.interstandart.ruASTM D 3942-03(2008)D 3942 03(2008)1 D 3942;,.()1.1.1 ,Y X,Y.24,2-25,0 (2,42-2,50 o).1.2 ,.5%,.1.3 1 ASTM D32 D32.05 Zeolites.1 2008.2008.1980.2003.D 3942-03.1ASTM D 3942-03(2008),.,.2.2.1 ASTM:2E 691 3.3.1 Y X,.,.4.4.1 Y X,.,.Y (FCC),X ,.2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.2ASTM D 3942-03(2008)4.2 ,X Y.,Y-,.4.3 ,.,.,.3 ,;.4.4 ,-.,.5.5.1 ,0,25 2/.2 ,.1 ,3 -:Breck,D.W.and Flanigen,E.M.in Molecular Sieves,Society of Chemical Industry,London,1968,p.47,Wright A.C.,Rupert,J.P.and Granquist W.T.Amer.Mineral.,Vol 53,1968,p.1293;Dempsy,E.,Kuehl,G.H.,and Olson,D.H.,Journal of the Physical Chemistry,Vol 73,1968,p.387.3ASTM D 3942-03(2008)0,25 2/,.5.2 ,110C.5.3,35%,CaCl26H2O 23C 3C.6.6.1 ,5,.()(SMR 640),.7.7.1 1,5 110C 1.2 .,.7.2 1 0,05 .,16.7.3 .7.4 50 60 2.4ASTM D 3942-03(2008)3 .4 53,4 57,8 2 .,20 32 2.Cu K u 1 Cu K2.Cu K ,.,Cu K1,Cu K.5 Cu K2,(20 32).7.5 53,4 57,8 2 56,1 ,.,-Cu K1 Cu K2 ,(Cu K1)3/4.6 ,23,5,26,9 31,2 28,5 2(Cu K).8.8.1 ,().Cu K1,56,123 2;Cu K,56,173 2.5ASTM D 3942-03(2008)7 ,28,443 2(Cu K1)28,467 2(Cu K).8.2 d-,:(1):dhkl-,hkl,(10),o-,1,54178 o(0,154178)Cu K 1,54060 (0,154060)Cu Ko1.,2,.4 8.3 ,a,:(2)(h2+k2+l2):5 (h2+k2+l2)57,8 2 243 53,4 211 31,2 75 26,9 56 23,5 43 4 ,d.,.Fang,J.H.and Bloss,F D.,X-Ray Diffraction Tables,Southern Illinois University Press,Carbondale,IL.1966.5 hkl 5 55 2.Broussard,L.and Shoemaker,D.P.,Journal of the American Chemical Society,Vol 82,1960,p.1041.6ASTM D 3942-03(2008)8 .,26,9.,.8.4 a .8.5 NaY,.1.Cu K1()Cu K2(),Cu K1.:2 (h2+k2+l2)(a,)o58,197 58,215 243 24,683 56,105 56,123 53,872 53,890 211 24,691 24,687 56,123(Si)56,105()=0,018 .d Cu K1(8.2),a,8.3.9.9.1 .9.1.1 ,a,.(10 =1.)9.1.2,.7ASTM D 3942-03(2008).1 NaY 10.610.1 ,.E 691 .10.2 :10.2.1 ,0,02(0,002).o10.2.2 ,0,04 (0,004).o10.3 6 ASTM ,RR:D321002.8ASTM D 3942-03(2008),.11.11.1;.ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).9