Designation:D4326−13StandardTestMethodforMajorandMinorElementsinCoalandCokeAshByX-RayFluorescence1ThisstandardisissuedunderthefixeddesignationD4326;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginaladoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperscriptepsilon(´)indicatesaneditorialchangesincethelastrevisionorreapproval.1.Scope1.1ThistestmethodcoverstheanalysisofthecommonlydeterminedmajorandminorelementsinashfromcoalorcokeusingX-rayfluorescence(XRF)techniques.NOTE1—TestMethodD5016isusedfordeterminationofsulfur.NOTE2—Althoughnotincludedinthepresentmethod,thedetermina-tionofbarium,strontium,andmanganesemayberequiredtoyieldadequatetotals.1.2ThevaluesstatedinSIunitsaretoberegardedasstandard.Nootherunitsofmeasurementareincludedinthisstandard.1.3Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappro-priatesafetyandhealthpracticesanddeterminetheapplica-bilityofregulatorylimitationspriortouse.2.ReferencedDocuments2.1ASTMStandards:2D121TerminologyofCoalandCokeD346PracticeforCollectionandPreparationofCokeSamplesforLaboratoryAnalysisD2013PracticeforPreparingCoalSamplesforAnalysisD3173TestMethodforMoistureintheAnalysisSampleofCoalandCokeD3174TestMethodforAshintheAnalysisSampleofCoalandCokefromCoalD5016TestMethodforTotalSulfurinCoalandCokeCombustionResiduesUsingaHigh-TemperatureTubeFurnaceCombustionMethodwithInfraredAbsorptionD7348TestMethodsforLossonIgnition(LOI)ofSolidCombustionResiduesD7582TestMethodsforProximateAnalysisofCoalandCokebyMacroThermogravimetricAnalysisE2MethodsofPreparationofMicrographsofMetalsandAlloys(IncludingRecommendedPracticeforPhotogra-phyAsAppliedtoMetallography);ReplacedbyE883(Withdrawn1983)3E11SpecificationforWovenWireTestSieveClothandTestSieves3.Terminology3.1Definitions—DefinitionsapplicabletothistestmethodarelistedinD121,TerminologyofCoalandCoke.4.SummaryofTestMethod4.1The...