ASTM_D_3264_-_97.pdf

Designation:D 3264 97Standard Specification forIndustrial Grade Aniline1This standard is issued under the fixed designation D 3264;the number immediately following the designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon(e)indicates an editorial change since the last revision or reapproval.1.Scope1.1 This specification covers industrial grade aniline.1.2 The following applies to all specified limits in thisspecification:for purposes of determining conformance withthis specification,an observed value or a calculated value shallbe rounded off“to the nearest unit”in the last right-hand digitused in expressing the specification limit in accordance withthe rounding-off method of Practice E 29.1.3 Consult current OSHA regulations,suppliers MaterialSafety Data Sheets,and local regulations for all materials usedin this specification.NOTE1The properties included in this specification are those re-quired to characterize the above material.If additions are deemednecessary,these will be added when their inclusion becomes desirable andthe necessary methods become available.2.Referenced Documents2.1 ASTM Standards:D 1078 Test Method for Distillation Range of VolatileOrganic Liquids2D 1209 Test Method for Color of Clear Liquids(Platinum-Cobalt Scale)2D 1493 Test Method for Solidification Point of IndustrialOrganic Chemicals2D 3436 Practice for Sampling and Handling Aniline2D 3505 Test Method for Density or Relative Density ofPure Liquid Chemicals2D 4589 Test Method for Nitrobenzene in Aniline2E 29 Practice for Using Significant Digit in Test Data toDetermine Conformance with Specifications3E 203 Test Method for Water Using Karl Fischer Reagent42.2Other Document:OSHA Regulations,29 CFR,paragraphs 1910.1000 and1920.120053.Properties3.1 Industrial grade aniline shall conform to the followingrequirements:PropertySpecificationASTMTestMethodNitrobenzene,max,weight%0.0002D 4589Water,max,weight%0.05E 203AppearanceAColor,max,PT/Co scale100D 1209Distillation range,including the temperature,184.2C,at 101.3 kPa(760 mm Hg)pressure,max CTotal1.0D 107895%(2.0 mL to 97.0 mL)0.5Relative density,20/4C1.020 to 1.024D 3505Solidification point,anhydrous basis,min,C6.20D 1493_AClear liquid free of sediment and haze when observed at 18.3 to 25.6C(65 to78F).NOTE2Aniline is light sensitive and will darken on exposure to lightand air.4.Sampling4.1 Sample the material in accordance with PracticeD 3436.5.Keywords5.1 aminobenzene;aniline;aniline oil;benzenamine;indus-trial grade;phenylamine1This specification is under the jurisdiction of ASTM Committee D16 onAromatic Hydrocarbons and Related Chemicals and is the direct responsibility ofSubcommittee D16.03 on Organic Nitrogen Compounds.Current edition approved Dec.10,1997.Published August 1998.Originallypublished as D 3264 73 T.Last previous edition D 3264 92.2Annual Book of ASTM Standards,Vol 06.04.3Annual Book of ASTM Standards,Vol 14.02.4Annual Book of ASTM Standards,Vol 15.05.5Available from Superintendent of Documents,U.S.Government PrintingOffice,Washington,D.C.20402.1Copyright ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.NOTICE:This standard has either been superceded and replaced by a new version or discontinued.Contact ASTM International(www.astm.org)for the latest information.ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard.Users of this standard are expressly advised that determination of the validity of any such patent rights,and the riskof infringement of such rights,are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised,either reapproved or withdrawn.Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters.Your comments will receive careful consideration at a meeting of theresponsible technical committee,which you may attend.If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards,at the address shown below.This standard is copyrighted by ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.Individual reprints(single or multiple copies)of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585(phone),610-832-9555(fax),or serviceastm.org(e-mail);or through the ASTM website(www.astm.org).D 32642NOTICE:This standard has either been superceded and replaced by a new version or discontinued.Contact ASTM International(www.astm.org)for the latest information.