ASTM_D_4047_-_13_rus.pdf

:D 4047-13:149/93 STANDARD TEST METHOD FOR PHOSPHORUS IN LUBRICATING OILS AND ADDITIVES BY QUINOLINE PHOSPHOMOLYBDATE METHOD ():2919-16/ASTM :20.06.2016 2016 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 4047-13 :D 4047-13 :149/93 1 D 4047;,.().1.*1.1 0,005 10,0%.,.1 ASTM D02 ,D02.03 .15 2013.2013.1981.2011.D4047-00(2011).DOI:10.1520/D4047-13.1ASTM D 4047-13 1.2 ,.1 IP 149 IP 148,IP 149 .1.3 ,.1.4,18,3,5,.1.5,.1.6 ,.,.6.9.2.2.1 ASTM:2 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.2ASTM D 4047-13 D 1193 D 6299 2.2 IP:IP 148 3 3.3.1 .3.2 ,.4.4.1 ,.3 ,61 New Cavendish St.,WIG 7AR,http:/www.energyinst.org.uk.3ASTM D 4047-13 5.5.1 ,40 40.5.2 ,700C .5.3 ,25.5.4 ,500,.5.5 ,35 -20.5.6 ,20.6.6.1 .,4,.,.6.2 ,4 ,DC.,.,BDH Ltd.,Poole,Dorset,U.K.,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.4ASTM D 4047-13 II III D 1193.6.3 ,1 N.6.4 (36%)(HCl).6.5 ,(0,1 N)(HCl).6.6 2 .6.7 ,(1/95%-).6.8 (KBrO3),.6.9 (),.232 238C.6.10 20 800 ,25 (HCl);,1 .1.6.11 (0,1 M)(NaOH).6.12 10 NaOH 18 200 .5ASTM D 4047-13 2 ,.6.13 (1/)95%-.6.14 (ZnO),.6.15 .6.16 1/,95%-.6.17 ,0,005%.7.7.1 0,3%,0,1 0,3%.7.2 ,10 ,:A=2/P(1):P-,A-,10 .7.3 ,10 ,:=10 A(2):-,.7.4 A 0,01 25.7.5 B .6ASTM D 4047-13 7.6 ,50C.8.8.1 1 ,7.6.8.2 3 ,3 .1.1.,%,NaOH 0,1 M P,%0,005 0,10 3 0,005 1,3 0,010 2,5 0,05 13 0,10 25 0,10 0,30 0,10 8 0,20 17 0,30 25 8.3 8 ,.(Meker),.700C .8.4 600 (.3),.50 (HCl).7ASTM D 4047-13 ,23.8.5 ,().,30 50 KbrO3 ,().3 .,.8.6 150 ,30 30 ,.8.7 ,2 .2 ,24.15 ,.8.8 (.4),.8ASTM D 4047-13 20 1 M HCl.25 30 .,.,0,1 N NaOH.4 20,.8.9 ,500.CO2 .,;.CO2 ,120.8.10 ,.,NaOH.8.11 0,1 M NaOH,.0,1 M NaOH ,5.1 .0,1 M NaOH(V1).6 9ASTM D 4047-13 0,1 M HCl ,-.0,1 M HCl(V2).8.12 ,.5,0 0,1 M NaOH 0,1 M HCl(V3).9.9.1 :,%(3):A-10 ,-10 ,W-,V1-0,1 M NaOH,V2-0,1 M HCl,V3-0,1 M HCl,.9.2 :,%=(4):W-,V1-0,1 M NaOH,V2-0,1 M HCl,V3-0,1 M HCl,.10ASTM D 4047-13 10.10.1 D 4047 IP 148.11.11.1 ,.11.1.1 /.11.1.2 /,X1.12.12.1 ,5:12.1.1 ,x=:5 .11ASTM D 4047-13 (x)0,005 0,079%0,08 10%0,0318x0,992 0,032(x+0,04)12.1.2 ,x=:(x)0,005 0,079%0,08 10%0,118x0,992 0,074(x+0,04)12.2 ,.2,x.1979.2.,x 0,007 0,001 0,003 0,01 0,001 0,003 0,02 0,002 0,004 0,04 0,002 0,006 0,07 0,003 0,008 0,1 0,003 0,012 0,2 0,006 0,024 0,4 0,013 0,047 0,7 0,022 0,083 1,0 0,032 0,118 2,0 0,063 0,234 4,0 0,126 0,467 7,0 0,219 0,813 10,0 0,312 1,153 12.3 ,.12ASTM D 4047-13 13.13.1;()X1.X1.1 (QC).X1.2 QC(.D 6299 ASTM MNL 7).6 X1.3 QC (.D 6299 ASTM MNL 7).X1.4 ,QC ,.QC .QC ,QC .QC ,6 ASTM MNL 7,6-.,-ASTM.13ASTM D 4047-13 ASTM.X1.5,QC,.QC,.X1.6 .D 6299 ASTM MNL 7.D02.03 (D4047-00(2011),.(1)1.3,1.4,5.4,5.5,5.6,6.15,6.16,6.17 ,IP 149.14ASTM D 4047-13 15ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).ASTM(www.astm.org/COPYRIGHT/).