ASTM_D_3171_-_11_rus_scan.pdf

ELEPANbHOE ArEHTCTBOnO TEXHNYECKOMy PErYnNPOBAHNIO M METPONOrVMTOCT PHAUNOHANbHbINCTAHAAPT56682-POCCNNCKONEAEPA4MM2015KOMnO3NTbI nOnNMEPHbIEN METANYECKNEMeTon onpeneneHna o6bema Matpnubl,apMnpyoweroHanonHNTenA N nycTOTM3 naHwe o中nunanbHoeMocKBaCTaHAapTMH中opM2016FOCTP 56682-2015peAncnoBne1 NOAOTOBNEH O6enHeHnem opnAn4ecknx nny Coo3 npon3BAnTene KoMno3TOBCOBMeCTHO C OTKpbITbIM aKyOHePHbIM 06eCTBOM HO CTeKnonnacTnK ABTOHOMHOHeKoMMep4ecko opraHn3ayne LeHTp HOpMpoBaHnA,cTaHAapTn3ayn n Knacc中nKayn KoMno3TOBHa ocHoBe ooManHoro nepeBoga Ha pyccKn 3bIK aHrncKo Bepc yKa3aHHoro B nyHKTe 4cTahgapta,kotopbi BbinonheH TK 497KomN03nTbi,KOHcTpykynn n n3gennA n3 Hnx2 BHECEH TeXHn4eCKnM KOMnTeToM no cTaHAapTn3aynn TK 497 KoMnO3TbI,KOHCTpyKunn n3en3 HX3 YTBEPKAEH BBEAEH B AENCTBME NpKa3oM PeAepanbHoro areHTCTBa no TexHM4ecKoMyperynupoBaHnio n MeTponornn oT 30 oKT6p 2015 r.N2 1681-cT4 HacToq cTaHAapT ABngeTcA MoAnOypoBaHHbIM no OTHOweHnO K cTaHAapTyACTM 3171-11 CTaHgapTHbn MeTog onpegeneHnA cogepaHA cocTaBHbIX yacTen B KOMnO3MTHbIXMarepnanax(ASTM D3171-11 Standard Test Method for Constituent Content of Composite Materials,MOD)nyTem 3MeHeHnA cogepxaHnA oTAenbHbix cTpyKTypHbix 3neMeHTOB,KOTopble BbiAeneHbIBeptKanbHon nnHen,pacnonoxeHHon Ha nongx 3Toro TeKcTa.OpMrHanbHbI TeKCT 3TX CTpyKTypHbIXanemeHToB npnMeHeHHoro cTaHgapTa ACTM npBegeH B gononHTenbHoM npnnokeHnn AA.OTAenbHbleCTpyKTypHble 3neMeHTbI 3MeHeHb B enAx coonogeHA HOpM pyccKoro A3biKa M TexHn4ecKoro cTnA3nokeHng,a takke B cooTBeTcTBnn c Tpe6oBaHnAM TOCT P 1.5.pM 3TOM OcObeHHOCT pOcccKo HauoHanbHOM cTaHgapT3ay yTeHbi B gononHTenbHOMnogpa3gene 7.4,kotopbi BbigeneH nyTem 3akno4eHA B paMKn 3 TOHKnx nnH.AononHnTenbHoenonokeHme npBegeHo An ycTaHoBneHMA TpeoBaHn K onpegeneHo nnoTHOCT MaTpMbI apMpyowero HanonHTeng.AononHnTenbHbie ccbinkn,Bknio4eHHbie B teKct cTaHAapta An yueTa ocobeHHocTen poccnckonHaOHanbHo cTaHAapT3au,BbeneHb KypCBOM.B HacTOAw cTaHAapt He Bkno4eHbi pa3geni 5,6,9,11,16,nopa3genti 3.2,3.3,nyHKTbi 3.1.1-3.1.5 n cCbInK Ha ASTM E12,ASTM E177,ASTM E1309 3 npnMeHeHHoro cTaHAapTa ACTM,KOTopbleHeLenecoopa3Ho npMMeHATb B poccncKon HaLOHanbHO cTaHAapT3aMM B CBA3M C TeM,4TO OHMMeoT peKoMeHgatenbHbi,nocHw n cnpaBoHbin xapakTep.yka3aHHble pa3genbl,He BknioeHHble B ocHOBHyio acTb HacToero cTaHapta,npnBeAeHbi BAononHTenbHoM npnoeH 6.B HacTOALeM cTaHAapTe BMeCTo CCbino4HbIX CTaHAapToB ACTM nCnOnb3OBaHbI COOTBeTCTByIOMeMexrocyapcTBeHHble cTaHAapTbI.CpaBHeHMe cTpyKTypLI HacToAuero cTaHAapTa co cTpyKTypo yKa3aHHoro cTaHAapTa ASTMnpBeeHo B AononHTenbHOM npnoeH AB.门pm npnMeHeHM HacTowero cTaHAapTa peKoMeHAyeTcA nCnOnb3OBaTb BMeCTO CCbINO4HbIXcTaHapTOB cOOTBeTCTByouMe M HaMOHanbHbIe MexrocyAapcTBeHHble cTaHapTbI,cBeAeHnA OKOTOpbIx npBeeHbI B npnoeH.5 BBEAEH BNEPBbIEpaeuna npuMeHeHuR HacmoRue3o cmaHdapma ycmaHoeneHbi e OCT P 1.0-2012(pa3den 8).VHpopMauuRo6 u3MeHeHuRx K HacmoRueMy cmaHdapmy ny6nukyemcR e exe2odHoM(no cocmoRHuKo Ha 1 sHeaps mekyeso aoda)uHpopMauoHHoM yxa3amene HauuoHanbHbIe cmaHoapmbi,a opuquanbHbIu meKcm u3MeHeHuu u nonpaeok eexeMeCR4HOM uHPopMaLuOHHoM yKa3amene HauuoHanbHble cmaHdapmbi.B chyuae nepecMompa(3aMeHbi)unuomMeHbI Hacmoueao cmaHdapma coomeemcmeyouwee yeedoMneHue 6ydem ony6.nukoeaHo e 6nuxauweM ebinyckeexeMecR4Ho30 uHpopMauOHHo2o ya3ameng HauuoHanbHble cmaHdapmbi.CoomeemcmeylowaR uHpopMauuR,yeedoMneHue u mekcmbi pa3Mewalomc makke e uHpopMauOHHOu cucmeMe ooweso nonb3oeaHuR HaopuuuanbHoM caume PedepanbHo2o aeHmcmea no mexHu4eckoMy peynupoeaHuio u Memponoauu e cemuHmepHem(www.gost.ru)CTaHAapTHopM,2016HacToA cTaHAapt He MOxeT 6bITb nOnHOCTbHO n yacTM4HO BOcnpoM3BeAeH,TpaxmpOBaH MpacnpocTpaHeH B ka4ecTBe opMymanbHoro 3AaHMA 6e3 pa3peweHnA 中egepanbHoro areHTCTBa noTexHMeckoMy perynpoBaHo MeTponornFOCTP 56682-2015HAUOHAnbHb CTAHAAPT POCCCKO 中EAEPAUKOMNO3TbI nOMEPHbIE METAECKEMeToAbi onpegeneHng o6bema Matpubi,apmnpyowero HanonHnTeng n nycToTPolymer and metal composites.Method for determination the volume of matrix,reinforce filler and voidsAaTa BBeAeH-2017-01-011 06nacTb npMeHeHHacrou craHgapT pacnpocTpaHgeTcA Ha KOMnO3MTHble MaTepnani c nonMMepHOM nMMeTannneckon Matpnuen,apMpoBaHHon BonoKHoM(ganee-KoMno3Tbi)n ycTaHaBnBaeT ABa MeToaonpegeneHng cogepaHng Matpbi,apMnpyoero HanonHnTeng n nycToT.MeTog I npMeHoT An onpegeneHn cogepaHn MaTpnybi,apMpyiowero HanonHnTeng n nycToT.MeTog ll npumeHAoT tonbo An onpegeneHng cogepxaHng matpybi n apmnpyowero HanonHntengnaMMHaToB.2 HopMaTnBHble ccbIKnB HacToAeM cTaHgapte ncnonb3oBaHbI HOpMaTBHble ccbinkn Ha cneAyioune cTaHAapTbi:OCT 166-89(MCO 3599-76)WmaH2eHuupkynu.TexHu4eckue ycnoeuaOCT 177-88 Bodopoda nepekucb.TexHueckue ycnoeuaOCT 2768-84 AuemoH mexHu4eckuu.TexHueckue ycnoeugOCT 3118-77 Peakmuebi.Kucnoma congHa.TexHueckue ycnoeuaOCT 4204-77 Peakmuebi.Kucnoma cepHa.TexHueckue ychoeuaOCT 4328-77 Peakmuebi.Hampua 2uopookucb.TexHu4eckue ychoeugOCT 6709-72 Boda ducmunnupoeaHHa.TexHu4eckue ycnoeuOCT 11125-84 Kucnoma a3omHa oco6o 4ucmombi.TexHu4eckue ycnoBuaOCT 15139-69 nacmMaccbi.Memodbi onpedeneHu nnomHocmu(06LeMHO Maccbi)(ASTM D792-13 CmaHdapmHbi Memod onpedeneHu nnomHocmu u ydenbHo2o eeca(omHocumenbHonnomHocmu)nnacmukoebix Macc no 06beMy bimecHeHHO xudkocmu,NEQ,ASTM D1505-10 Memo0ucnimaHu on onpedeneHu nnomHocmu nnacmMacc npu nomouu Memoda apadueHmHo mpy6bi,NEQ)OCT 19710-83 3muneH2nukonb.TexHueckue ycnoeuaOCT 20289-74 Peakmuebi.AumemunpopMamud.TexHu4eckue ycnoeuaOCT 24363-80 Peakmuebi.Kanug 2udpookucb.TexHu4eckue ycnoeuaOCT 25336-82 locyda u o6opydoeaHue na6opamopHble cmeknAHHble.TuNbl,OCHOBHblenapaMempbi u pa3MepblOCT 29227-91(MCO 835-1-81)locya na6opamopHa cmeknHHaR.lunemku apadyupoeaHHbIe.Yacmb 1.06uue mpe6oeaHuOCT 32794-2014 KoMno3umbi nonuMepHbIe.TepMuHbi u onpedeneHu(ASTM D883-12 TepMuHbIu onpedeneHu,omHocauyueca k nnacmMaccaM,NEQ,ASTM D3878-07(2013)TepMuHbi u onpedeneHu,omHOCauec K KoMnO3umHbIM MamepuanaM,NEQ)OCT P 56762-2015 KoMno3umbi nonuMepHbie.Memod onpedeneHuA ena2ono2noweHug upaeHoBeCH020 cocmoHu(ASTMD5229/D5229M-12 Memod ucnLimaHu On onpedeneHuno2noweHu enazu u ceoucmea u cocmoRHue paHoeecu KoMno3umHbIx Mamepuanoe c nonuMepHouMampuueu,MOD)M3aHne oanbHoe10CTP56682-2015门pMMe4aHMe一冂on nonb3 OBaHNN HacTo山MM CTaHnapToM yenecoo6pa3HonpoBepMTb nencTBMeCCbinoyHblX CTaHnapToB B WH中opMa4 NOHHON CNCTeMe o6山ero nonb3 oBaHN9一Hao中MuNanbHOM caNTeenepanbHoroareHTCTBa no TexHMyecKoMy perynupoBaHnlo n MeTponornn B ceTn MHTepHeT wnn no exeroHoMy NHdopMaynoHHOMyyKa3aTeno HayNoHanbHble cTaHnapTbl,KoTopbin ony6nnKoBaH no CoCTOAHNIO Ha 1 AHBap9 Tekywero rona,w noBbinyckaM exeMecAyHoro WHopMaynoHHoro yKa3aten HayMoHanbHble cTaHnapTbl3a Tekywwn ron.Ecnn 3aMeHeHcCbinoyHbln cTaHnapT,Ha KoTopbin naHa HenatnpoBaHHag ccbinka,To peKoMeHnyeTca ncnonb3oBaTb eMcTByowyoBepCNiO 3Toro CTaHnapta c yueTOM Bcex BHeceHHbIX B aHHylO BepcNiO N3MeHeHNN.Ecnn 3aMeHeH CCbInoyHbINcTaHnapT,Ha KoTopbin naHa naTnpoBaHHaA ccbinka,To peKoMeHnyeTcA Ncnonb3oBaTb BepcNio 3Toro cTaHnapTa cyKa3aHHbIM Bblwe ronoM yTBepxneHn(npWHATNA).Ecnn nocne yTBepxneHn HacToawero cTaHnapTa B cCblnoyHblNCTaHnapT,Ha KoTopbin naHa aTnpoBaHHa ccbinka,BHeceHo N3MeHeHNe,3atparBarowee nonoxeHne,Ha KoTopoenaHa ccbinka,To 3To nonoxeHne peKoMeHnyeTca npMMeHATb 6e3 yueTa naHHoro N3MeHeHNA.Ecnw ccblnoyHblNCTaHnapT OTMeHeH 6e3 3aMeHbl,To nonoxeHne,B KOTopOM aHa ccbinka Ha Hero,pekoMeHayeTca npNMeHATb B uacTw,He 3aTparwBalowen 3Ty ccblnky.3 TepMNHbI n onpeneneHnaB HacToaweM cTaHnapre npuMeHeHbl TepMMHbl no TOCT 32794.4 CywHocTb MeTOAOB4.1 MeTon IMeTon 3akniouaeTc B pacTBopeHnn B pa3nnyHbIX XnMnyeCKnx coeAnHeHnax nnn CKnraHnn MaTpnublKOMnO3NTa:-cnoco6 A(CM.7.2.3.1)npnMeHAIOT Ana pacTBopeHna MaTpny M3 3nOKCMAHon CMonbl,CTanm,Meanwnn Apyrnx MaTepnanoB,pacTBopNMbIX B a30THoM KncnoTe;cnoco6 B(CM.7.2.3.2)npnMeHAIOT pacTBopeHNA MaTpnubl N3 3nOKCnHbIx,ceHonbHblx,nonMaMN HbIX.TepMonnacTNYHbIX CMon NnM pyrnx MatepnanoB,pacTBopNMbIX B cepHON KNCnoTe;cnoco6 C(CM.7.2.3.3)npMeHAIOT n pacTBopeHna Matpnubl N3 OTBepxkneHHbix aHrnapnaoM3nOKCMAHbIX CMOn,apMnpoBaHHON CTeKnAHHbIMN NnM yrnepoHbIMN HanonHNTenAMN;cnoco6 D(CM.7.2.3.4)npnMeHAIOT n pacTBopeHna MaTpnubl n3 anIOMMHNA,6poH3bl nnn ApyrnxMatepnanoB,pacTBopNMbIX B rapokcnne HaTpnA;cnoco6 E(CM.7.2.3.5)npMMeHAIOT n pacTBopeHnA MaTpNubl N3 CTanM,TWTaHa,Menn,aniOMNHNAnnn pyrMx MaTepnanoB,pacTBopNMbIX B conAHON KNcnoTe;-cnoco6 F(CM.7.2.3.6)npuMeHAIOT Ang pacTBopeHn MaTpny M3 3nOKCnAHoN CMONbI,CTann,MeAnwnw ApyrMx MatepnanoB,pacTBopMMbIX B a30THoN KNcnoTe,c cnonb3oBaHneM HarpeBaMNKpOBONHOBON neyn;-cnoco6 G(CM.7.2.3.7)npnMeHAIOT cxKMraHNA MaTpnubl,apMnpoBaHHon CTeKnAHHbIM nnMKepaMNyeCKNM HanonHNTenAMN.Cnoco6 HenpnMeHNM K MaTpnuaM,KOTopble He nonHOCTblo cropaoT npn NcnblTatenbHONreMnepaType,n MaTpnuaM,conepxkawnM apMnpyiouneHanonHnTenn,KOTopble pa3pywaloTca npnTeMnepaTypax Hnke MMHNManbHoN TeMnepaTypbl cKnraHNA.4.2 MeTon llMeTon 3aknioyaeTCA B N3MepeHNN TonWNHbl naMWHata.npN 3TOM OKHa 6bITb N3BeCTHa MaccoBaAAonA Ha enNHnuy nnowann M KonnyecTBo cnoeB apMnpylowero HanonHnTena.5 O6opynoBaHne n Matepnanbl5.1 06opynoBaHne5.1.1 MeToa I5.1.1.1 Becbl c norpewHoCTbO B3BewnBaHna He 6onee 0,0001 r.5.1.1.2 3kcMkaTop no OCT 25336.5.1.1.3 ycTpoNcTBO HarpeBarowee,cnoco6Hoe nonnepxnBaTb nocToaHHyo TeMnepaTypy no 610 C.5.1.1.4 neyb nabopaTopHas MnkpoBonHOBa co BCTpoeHHoN 3aWMToN OT BO3HMKHOBeHMAN36bITOYHorO naBneHNA,cnocooHaa nonepKnBaTb noCTOAHHyIO MOWHOCTb.5.1.1.5 Lkad cyunnbHbin,o6ecneynBarowni noCToHHylo TeMnepaTypy(100+3)C.5.1.1.6 neyb MydpenbHa,o6ecneynBarowaa nonnepxkaHne TeMnepaTypbl He MeHee(600+30)C.5.1.1.7 Hacoc BakyyMHbIM.5.1.1.8 ycTaHoBKa dnnbTpoBanbHa BakyyMHa,CoCToAa N3 Kon6bl ByH3eHa,BopOHKM BIOXHepa WnopncToro cTeKnAHHoro downbTpa.2T0CTP56682-20155.1.1.9 HenTpann3aTop cTaTnyeckoro 3nekTpnyecTBa Ana ycTpaHeHnA 3neKTpocTaTwuecknx 3apAAoBHa CTeHKax CTeKnAHHON eMKOCTN.5.1.1.10 XononnnbHNK 06paTHbin no TOCT 25336.5.1.1.11 EMKOCTb CTeKnAHHaa o6beMOM He MeHee 50 CM3.5.1.1.12 Turnn nnaTnHOBble wnn capopopoBble.5.1.1.13 Kon6bl CTeknaHHble.5.1.1.14 nwneTkM rpanyupoBaHHbie no/OCT 29227.5.1.1.15 ABToKnaB aHanMTnyecknn c peaKuMOHHbIMM CTakaHaMn.5.1.2 MeTon ll5.1.2.1 MnkpomeTp c ueHon neneHna 0,001 MM.5.1.2.1 LUTaHreHunpkynb no TOCT 166.5.2 MaTepnanbl5.2.1 KncnoTa a30THaa no OCT 111255.2.2 nepekncb Bonopona no OCT 1775.2.3 KucnoTa cepHaa no OCT 4204.5.2.4 AnMeTundpopMaMna no FOCT 202895.2.5 3TwneHrnnkonb no OCT 19710.5.2.6Mnp0 KCN Kanna noOCT243635.2.7 TMapokcna HaTpna no FOCT 4328.5.2.8 ConaHaa kncnoTa no OCT 3118.5.2.9 AueTOH no FOCT 2768.5.2.10 Bona AncTnnnmpoBaHHas no TOCT 6709.6 nonroToBKa K npoBeneHno NcnbITaHnN6.1 nonroToBka o6pa3uoB6.1.1 MeTonI6.1.1.1 na NcnbITaHnn wcnonb3yIOT o6pa3ubl B KonMyeCTBe,yCTaHoBneHHOM B HopMaTNBHbIX AoKyMeHTaxWnN TeXHNyeckon noKyMeHTauNN Ha N3nenMe.IpN OTCyTCTBNN Taknx yka3aHnN NcnbITblBalOT npoN3BonbHoeKonnyeCTBO oopa3LOB,HO He MeHee Tpex.6.1.1.2 O6pa3ubl ncnbITaHnn,Bblpe3aHHble n3 nccneAyeMoro KOMnO3NTHorO MaTepnana,AOKHblNMeTb Maccy,yCTaHoBneHHyIO B HOpMaTNBHbIX DOKyMeHTax NnN TeXHNyeCKoN noKyMeHTauNN.IpN OTCyTCTBNNTaknx yka3aHnN N3rOTOBNAIOT oopa3ubl nA NcnbITaHNN C Maccon 1 r.6.1.1.3 O6pa3ubl n ncnblTaHnn AonKHbl NMeTb poBHyo,cnnowHylo noBepxHOCTb 6e3 nyCTOT WTpewNH yMeHbweHN BO3MOXKHOCTN 3axBata wnn BKnioyeHNA BO3yWHbIX ny3blpbKoB.6.1.2 MeTon ll6.1.2.1 na NcnbITaHnM wcnonb3yIOT o6pa3ubl B KonMyeCTBe,yCTaHoBneHHOM B HOpMaTNBHbIX oKyMeHTaxnnn TeXHNyeckon oKyMeHTayMn Ha n3nenne.npn OTCyTCTBNN Taknx yKa3aHnn ncnbITblIBaIOT npon3BoNbHoeKonMyeCTBO oopa3LOB.6.1.2.2 O6pa3ubl ncnblTaHnn AonKHbl NMeTb dopMy ynnnHApa nnn Ky6a n nnowanb noBepxHOCTn HeMeHee 625 MM.6.1.2.3 Ha noBepxHOCTN 06pa3ya n ncnbITaHnn He AOnKHo 6bITb Macna,rp93n n Apyrnx noCTopoHHNXBewleCTB.6.2 Cywka o6pa3uoBnepen ncnblTaHneM o6pa3ubl cywaT B COoTBeTCTBMM C TOCT P 56762(MeToA D).7 npoBeneHne ncnblTaHnn7.1O6叫e nonoxkeHNVcnblTaHna npoBOnAT npn TeMnepatype(23+3)C N OTHOCNTenbHoN BnaxKHOCTN Bo3nyxa(5010)%.7.2 MeTOA I7.2.1 B3BewnBaoT o6pa3ey ana ncnblTaHnn C TOYHOCTbIO Ao 0,0001 r.7.2.2 OnpenenoT nnoTHOCTb 06pa3ua na ncnblTaHnn MeTOAoM rnApocTaTnueckoro B3BewnBaHnano FOCT 15139(pa3nen 3)wnn MeTonoM rpanweHTHoN KonoHKM no TOCT 15139(pa3nen 6).7.2.3 ynanaoT MaTpnuy 06pa3ua ana ncnblTaHnn OnHMM n3 cnoco60B no 7.2.3.1-7.2.3.7.Bbl6paHHbin cnoco6 onkeH no3BONATb npon3BOANTb ynaneHne Matepnana MaTpnubl,He oKa3blBanpN 3TOM Bo3neNCTBNe Ha MaTepnan apMnpyiowero HanonHNTenA.3