ASTM_D_4005_-_92_2022.pdf

Designation:D400592(Reapproved 2022)Standard Test Method forPlastic-Coated FabricsCompleteness of Fusion of PVCDispersion Coatings1This standard is issued under the fixed designation D4005;the number immediately following the designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon()indicates an editorial change since the last revision or reapproval.1.Scope1.1 This test method describes a simple procedure to deter-mine the completeness of fusion of poly(vinyl chloride)(PVC)dispersion coatings on fabric.This test applies primarily tocoatings with a mechanical bond and does not include tiecoating.1.2 This standard does not purport to address all of thesafety concerns,if any,associated with its use.It is theresponsibility of the user of this standard to establish appro-priate safety,health,and environmental practices and deter-mine the applicability of regulatory limitations prior to use.1.3 This international standard was developed in accor-dance with internationally recognized principles on standard-ization established in the Decision on Principles for theDevelopment of International Standards,Guides and Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade(TBT)Committee.2.Summary of Test Method2.1 Specimens of the PVC-coated fabric are examined forsurface cracks or breaks,followed by immersion in acetone.Subequent appearance of additional cracking indicates thatfusion is incomplete.3.Significance and Use3.1 Poly(vinyl chloride)(PVC)is applied to coated fabricsas a dispersion of PVC particles in a liquid vehicle.During theprocessing of the fabric the PVC is fused or melted to producea uniform film on the fabric.This test measures whether thePVC is converted,fused,or melted to produce a homogeneousfilm.3.2 This conversion process is a melting of the crystallitestructures in the polymer particles followed by solution of themolten polymer in the plasticizing vehicle.Fusion is importantin the production of PVC-coated fabrics.4.Apparatus and Reagents4.1 Glass Beaker,500-mL.4.2 Acetone.4.3 Glass Rods,5-mm diameter.4.4 Metal Clips.5.Sampling5.1 Select a sample of coated fabric to adequately representthe roll or lot under consideration.5.2 Cut three 20 by 40-mm test specimens to be tested,onein the middle and the others from the sides at least 200 mmfrom the edges of the roll of fabric.5.3 Remove the PVC coating from the fabric of the testspecimens by peeling carefully.6.Procedure6.1 Carefully examine each specimen for cracks on thesurface or breaks(cracks completely through the film)andrecord size,frequency,and location.6.2 Wrap each specimen around a glass rod with the coatingunder test outward.Secure the assembly with a metal clamp.6.3 Immerse the test specimens in acetone at 23 6 2 C for15 min.Remove and examine visually.Determine whethercracks or breaks have appeared.7.Report7.1 Report the following information:7.1.1 Description of the material and date manufactured,7.1.2 Date tested,7.1.3 If any cracks or breaks have appeared,report thatfusion is incomplete,and7.1.4 Report the observation of each test specimen sepa-rately.8.Precision and Bias8.1 This test is essentially a“pass-fail”test and does notassess a quantitatively measured test characteristic.Due to thisno precision and bias data are reported.1This test method is under the jurisdiction of ASTM Committee D11 on Rubberand Rubber-like Materials and is the direct responsibility of Subcommittee D11.37on Coated Fabrics,Rubber Threads and Seals.Current edition approved Oct.1,2022.Published November 2022.Originallyapproved in 1981.Last previous edition approved in 2015 as D4005 92(2015).DOI:10.1520/D4005-92R22.Copyright ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959.United StatesThis international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards,Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade(TBT)Committee.19.Keywords9.1 coated fabrics;fusion;PVCASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard.Users of this standard are expressly advised that determination of the validity of any such patent rights,and the riskof infringement of such rights,are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised,either reapproved or withdrawn.Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters.Your comments will receive careful consideration at a meeting of theresponsible technical committee