ASTM_D_3630_-_89_1993.pdf

Designation:D 3630 89(Reapproved 1993)Standard Guide forDetermining Constituents Classified as HazardousContained in Protective Coatings1This standard is issued under the fixed designation D 3630;the number immediately following the designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon(e)indicates an editorial change since the last revision or reapproval.1.Scope1.1 This guide applies to liquid protective coatings,relatedproducts,and their dried films.It is a guide for the selection ofanalytical procedures for the determination of the presence andquantity of selected materials that may present potentialphysiological hazards.1.2 Various levels of government have established laws andregulations that limit the quantity or prohibit the presence ofcertain materials classified as hazardous in protective coatings.Materials subject to such regulations are within the scope ofthis guide.1.3 A hazardous material within the scope of this guide isone that exhibits harmful physiological effects through inges-tion,inhalation,absorption,or skin or eye contact.Hazardsassociated with combustion are not within its scope.1.4 This standard does not purport to address all of thesafety concerns,if any,associated with its use.It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2.Referenced Documents2.1 ASTM Standards:D 49 Test Methods of Chemical Analysis of Red Lead2D 126 Test Methods for Analysis of Yellow,Orange,andGreen Pigments Containing Lead Chromate and Chro-mium Oxide Green2D 215 Practice for Chemical Analysis of White Linseed OilPaints3D 283 Test Methods of Chemical Analysis of CuprousOxide and Copper Pigments2D 444 Test Methods for Chemical Analysis of Zinc YellowPigment(Zinc Chromate Yellow)2D 564 Test Methods for Liquid Paint Driers3D 715 Test Methods for Analysis of Barium Sulfate Pig-ment2D 1301 Test Methods for Chemical Analysis of White LeadPigments2D 1844 Test Methods for Chemical Analysis of Basic LeadSilicochromate2D 1845 Test Methods for Chemical Analysis of StrontiumChromate Pigment2D 2348 Test Method for Arsenic in Paint3D 2349 Test Method of Qualitative Determination of Natureof Thinner in Solvent-Reducible Paints3D 2350 Test Method for Antimony Oxide in White PigmentSeparated From Solvent-Reducible Paints3D 2371 Test Method for Pigment Content of Solvent-Reducible Paints3D 2372 Practice for Separation of Vehicle From Solvent-Reducible Paints3D 2374 Test Method for Lead in Paint Driers by EDTAMethod3D 2621 Test Method for Infrared Identification of VehicleSolids From Solvent-Reducible Paints3D 2698 Test Method for Determination of the PigmentContent of Solvent-Reducible Paints by High-Speed Cen-trifuging3D 2742 Methods for Chemical Analysis of Tribasic LeadPhosphosilicate4D 3257 Test Methods for Aromatics in Mineral Spirits byGas Chromatography5D 3271 Practice for Direct Injection of Solvent-ReduciblePaints Into a Gas Chromatograph for Solvent Analysis2D 3272 Practice for Vacuum Distillation of Solvents FromSolvent-Reducible Paints For Analysis3D 3280 Test Methods forAnalysis of White Zinc Pigments2D 3329 Test Method for Purity of Methyl Isobutyl Ketoneby Gas Chromatography5D 3335 Test Method for Low Concentrations of Lead,Cadmium,and Cobalt in Paint by Atomic AbsorptionSpectroscopy3D 3432 Test Method for Free Toluene Diisocyanates inUrethane Prepolymers and Coating Solutions by GasChromatography2D 3618 Test Method for Detection of Lead in Paint andDried Paint Films31This guide is under the jurisdiction of ASTM Committee D-1 on Paint andRelated Coatings,Materials,and Applications and is the direct responsibility ofSubcommittee D01.22 on Health and Safety.Current edition approved Oct.27,1989.Published December 1989.Originallypublished as D 3630 77.Last previous edition D 3630 77(1981)e1.2Annual Book of ASTM Standards,Vol 06.03.3Annual Book of ASTM Standards,Vol 06.01.4Discontinued;see 1989 Annual Book of ASTM Standards,Vol 06.02.5Annual Book of ASTM Standards,Vol 06.04.1AMERICAN SOCIETY FOR TESTING AND MATERIALS100 Barr Harbor Dr.,West Conshohocken,PA 19428Reprinted from the Annual Book of ASTM Standards.Copyright ASTMD 3624 Test Method for Low Concentrations of Mercury inPaint by Atomic Absorption Spectroscopy3D 3717 Test Method for Low Concentrations of Antimonyin Paint by Atomic Absorption Spectroscopy3D 3718 Test Method for Low Concentrations of Chromiumin Paint by Atomic Absorption Spectroscopy3E 202 Test Methods for Analysis of Ethylene Glycols andPropylene Glycols6E 260 Practice for Packed Column Gas Chromatography72.2ANSI Standard:Z66.1 Specification for Paints and Coatings Accessible toChildren to Minimize Dry Film Toxicity82.3Federal Standards:9U.S.Federal Test Method Standard No.141:4021.1 Pigment Content(Ordinary Centrifuge)4032Vehicle Isolat