ASTM_D_3242_-_11_rus.pdf

:D 3242-11:354/98 STANDARD TEST METHOD FOR ACIDITY IN AVIATION TURBINE FUEL 2011 ():1520-11/ASTM :11.10.2011 -,.9,-49,-1,119991.:(499)236-54-49,236-43-83:(499)230-13-72 E-mail:interstgost.ru Web:www.interstandart.ru (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FGU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FGU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 3242-11 1 :D 3242-11:354/98 1 D 3242;,.().1.1.1 0,000 0,100 /.1.2,.1.3 ,.1 ASTM D02 D02.06 .1 2011.2011.1973.2008.D 3242-08.DOI:10.1520/D3242-11.-.ASTM D 3242-11 2 ,.2.2.1 ASTM:2 D 664 D 1193 3.3.1:3.1.1 ,.3.1.1.1 ,-,/-.4.4.1 ,.2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM ASTM D 3242-11 3 ,()-.5.5.1 ,.,.,.5.2 .6.6.1 25,0,1,10,0,05.1 ,0,05 ,.7.7.1 .,ASTM D 3242-11 4 ,.3 ,.2 ,7.1.7.2 ,III D 1193.7.3 -4,5 -,1.-10 0,01/.7.4,.(.)7.5 ,(0,01)0,6 (,.)1 (.,.)(0,9%)2-.10-15,.0,2 (Ba(OH)2)(.3“Reagent Chemicals,American Chemical Society Specifications”,Am.Chemical Soc.,Washington,DC.,.”Annual Standards for Laboratory Chemicals,”BDH Ltd.,Poole,Dorset,U.K.,the United States Pharmacopeia,and National Formulary,U.S.Pharmacopeial Convention,Inc.,(USPC),Rockville,MD.4 ,2006.,-,Kodak,Baker(Mallinkrodt),Fluka Aldrich 1.,Kodak .5 -ASTM International RR:D02-1626.ASTM D 3242-11 5,.)5-10.,;(2).,.3 ,.7.5.1 ,0,0002N.0,1 0,02 ,1 110 1 40 1 ,2.:(1),;(2),6 .,.:=bpVVW100023,204 (1):Wp-,ASTM D 3242-11 6 204,23-,V-,Vb-,(),.7.5.2 0,1 0,01 50 ,2,50 .7.6 500 (.,.)5 495 .8.8.1 100 5 ,0,5 500-.(.1.)100 0,1 .6 8 5 600-800/.3 30 .8.1.1,.8.2 30.0,01 N .,()0,01-0,05 ().,ASTM D 3242-11 7 15 .4 .8.3 100 0,1 ,.1.9.9.1 QC().QC,.()QC .6 QC ,.,.QC ,6 MNL 7,Manual on Presentation of Data Control Chart Analysis,3:,6-.,ASTM,ASTM International,W.Conshohocken,1990.ASTM D 3242-11 8.QC ,QC ,.QC ASTM,.5 QC,QC.10.10.1 :,/=(A B)N 56,1/W (2):-,(8.2),-,(8.3),N-,W-,.11.11.1 0,001 /(D 3242)=().12.7 12.1 :7 -ASTM International RR:D02-1010.ASTM D 3242-11 9 12.1.1 ,(.1).12.1.2 ,(.1).6 .,.1.:=0,0132a =0,0406a:=12.2 ,ASTM D 3242-11 10.14.14.1;()1.-1.1 1.1.1 .1.1.2 0,5%.1.1.3 1 .1.1.4 0,1000 250 .(.)100 12.1,20 650-DU (Beckman),1-.1.1.5 :1.1.5.1 -=11 0,5 r-2.1.1.5.2 0,5 0,01 ,-.ASTM D 3242-11 11 1.1.5.3 1,0 0,01 ,.1.1.5.4 r ,.1.1.5.5 50 0,05 26,9 0,1 .2.pHr -2.1 2.1.1 -D 3242 r.2.2 2.2.1 ,:2.2.1.1 r ,-,.r ,r 4 pHr 11.r ,.2.3 2.3.1 ,r.ASTM D 3242-11 12 2.4 2.4.1 ,D 664 IP 177.A2.5 2.5.1 .,.4 ,.2.5.2 .2.5.3 (r=4,0):A2.5.3.1 2,4,6 ()(CH3)3C5H2N)(121,18).(2,4,6-(),.)(,.,.):168 170C ,nD20 1,4982 0,0005 A2.5.3.2 .A2.5.3.3 A (ASTM D 3242-11 13.)(2,4,6-(),.)(,.,.)24,2 0,1 2,4,6-(-),1-,100 -2-.1-,150/C 5 0,2/HCl(C HCl ).-2-1000,.A2.5.3.4,10 A 100 .1.2.5.4 (r=11,0):A2.5.4.1-(NO2C6H4OH)(139,11).(-,.,.,.):96 97C -A2.5.4.2 .A2.5.4.3 B (.)(-ASTM D 3242-11 14,.,.,.)27,8 0,1 -1-,100 -2-.250-,50/C2 1 0,2-/KOH(C2 KOH ).-2-1000 .A2.5.4.4,10 B 100 .1.2.5.5 ,(0,2)D 664-IP 177.2.5.6 -7.3.2.5.7 (KCl).2.5.8 ,(0,2).(.)(.).12-13 (KOH)1 -2-.10 .,().,(CO2),ASTM D 3242-11 15 ,.,0,0005 ,CO2.2.5.9 500 5 495 .2.6 A2.6.1 (.A2.1)(),.(.),KCl .,KCl.,.,.,.A2.1 8,8 ,.Lykken,L.,Porter,P.,Ruliffson,H.D.,Tuemmler,F.D.,“Potentiometric-Determination of Acidity in Highly Colored Oils,”Industrial Engineering Chemistry,Analytical Edition,IENAA,16,1944,.219234.ASTM D 3242-11 16,.,.A2.6.2 .,.,.(.),.5 ,.A2.6.3 -,100 1,0-1,5 0,1-/KOH.-,480 ,(.A2.2).A2.2 ,590 ,.,8.3.ASTM D 3242-11 17 2.7 2.7.1 ,25 2 .-,-4,0.2.7.2 ,.,25 2.-,.0,2 11,0,r,.0,2 11,0,.2.1.-,r.2.8 2.8.1 100 0,01 ,-r 13 14.2.8.2 0,5 0,01 ,13 14.ASTM D 3242-11 18 .2.1.-r 2.8.3 r -r.2.3 ,:-2.8.4 ,.2.9 2.9.1 ,r,r 10 pHr 12.ASTM D 3242-11 19 D02.06 (D3242-08),.(1)3.1.1.ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428-2959,USA.()ASTM 610-832-9585,610-832-9555 serviceastm.org (www.astm.org).ASTM(www.astm.org/COPYRIGHT/).