ASTM_D_297_-_93_2006_rus.pdf

:D 297-93(2006.).STANDARD TEST METHODS FOR RUBBER PRODUCTS CHEMICAL ANALYSIS 2012.():1668-12/ASTM :06.06.2012 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 297-93(2006)1 :D 297-93(2006.).1 D 297;,.().1.1.1 R(.3.1).1.1.1 A .1.1.2 B ,.1.1.3 :1 ASTM D11 D11.11 .1 2006.2006.1928.2002 D 297-93(2002).ASTM D 297-93(2006)2 A.:11-13 14 15 16 17-26 27-33 34-40 41-51 B.52-58 1.2,.1.3 ,.,.31.4.5,31.6,37.4.2,38.4.2,45.1.3,53.2.3.5,54.4.2,54.6,56.5.3 57.7.3;X1.3.3 X2.4.1.6.2.2.1 ASTM:2 D 982 .3 D 1416 3 D 1418 D 1646 ,2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM 3 ASTM D 297-93(2006)3 ()D 3040 ,3 D 3156 ,D 3452 .D 3677 .D 4483 E 11 E 131,E 200 ,E 442 ,3 E 443 3 3.3.1 ,D 1418.4.4.1 .,ASTM D 297-93(2006)4,.4.,.4.2 ,.5.5.1 ,:,/3 ,HC2H3O2(99,7%)1,05 ,HCOOH 1,22 ,HCl 1,19 ,HF(49%)1,16 ,HNO3 1,42 ,H3PO4(85%)1,70 ,H2SO4 1,84 ,NH4OH 0,90 ,.5.2 ,4,.,Washington,DC.,.Analar Standards for Laboratory Chemicals,BDH Ltd.,Poole,Dorset,U.K.,and the United States Pharmacopeia and National Formulary,U.S.Pharmaceutical Convention,Inc.(USPC),Rockville,MD.ASTM D 297-93(2006)5 ,:HCl(1+9)1 HCl(1,19),9 .,.5.3 ,:0,1 Na2S2O3,CuSO4(1 3=0,001 u).5.4 ,()/3,:NaOH(10/3)10 NaOH,1 3(.1).,:(50%),50 100 .,.1 ,(,BaCl22H2O),.,.A.6.6.1 ,ASTM D 297-93(2006)6 .6.2 .,.6.3 ,.6.4 ,(11-13).(35 36),550C,.,.,.,.,550C,ASTM D 297-93(2006)7 (50),(,45)(49).6.5 ,.6.6 -,550C.7.7.1 ,.8.8.1 ,.9.9.1 ,.,.-,.,9.2-9.7.,ASTM D 297-93(2006)8,.9.2 ,.,0,5.,.-,5 14(1,40).9.3 ,14(1,40).6,7 ,.,.,.9.4 .2,21,5 E11.6 ,W.Brabender Instruments,Inc.,50 E.Wesley St.,South Hackensack,NJ 07606.7 ,-ASTM International.1,ASTM D 297-93(2006)9 .500100 (204),.,.1,0.,.,.9.5 ,1,0,1,5 .,.9.6 30C.,.9.7 ,30(600).6,.10.10.1,10.1.1-10.1.9 ,.10.1.1 ,ASTM D 297-93(2006)10 HCl,.,.-.10.1.2 0,2 0,3 35.4 36.4.10 3 HCl,.40 3,.H2S .-,50.27.3.400 3,H2S.,28.3 28.4.10.1.3 HNO3 ,.,.-.10.1.4 ,HCl,.H2SO4.,HCl,.,(32).10.1.5 ,5C ,.10.1.6 32%68%8 ASTM D 297-93(2006)11 21.1 .,(20/3).,40.10.1.7 ,NaOH(175/3).,HCl.,(22).10.1.8 HCl,.HCl,.10.1.9 ,52 58.11.11.1 ,100%.NR,IR,SBR,BR.-,.ASTM D 297-93(2006)12 12.12.1:12.1.1 ,.,.,.,SBR(.1).12.1.2 ,.12.1.3 .12.1.4 ,.1 A D /3 NR 94/97 0,94 0,91A IR 1,00 1,00 0,95B SBRC 1,00 0,92 0,94B BR 1,00 1,00 0,90B IIR 1,00 1,00 0,92B A Wood,L.A.,Values of Physical Constants of Rubber,Rubber Chemistry Technology,12,1939,.130.B Wake,W.C.,The Analysis of Rubber Rubber-Like Polymers,MacLaren and Sons,Ltd.,London,England,1958,.42 45.C 23,5%.13.13.1 :ASTM D 297-93(2006)13 ,%=(100 B)(1),%=C/D(2),%=CE/F(3),%=GE/F(4):A-,.1,-,21(19 20),22,28.2.1,34.1,38(A)39(B)40.-,%D-,.1,E-,16.1,F-,.1,G-,%14.14.1 ,14.1.1 14.1.5.14.1.1 ,:ASTM D 297-93(2006)14 ,%=A/B 100(5):A-,-.14.1.2,:,%=A/B 100(6):A-,-.14.1.3 ,18 28 15.1.14.1.4 ,.14.1.5 ,.,.15.15.1 ,1 17,;.,18 28,.ASTM D 297-93(2006)15 (1),18.1 19(2)24(3)25(4)18(5)29(6)28.2.1(7)28.2.4(8),34.1(9)38 39(10)40(11)11-13 52-58(12)11-13(13),11-13(14),11-13(15)14.1.1(16)14.1.2(17)16(18)42(19)42(20)43(21)44(22)45(23)46(24)47(25)49(26)48(27)50(28)51 16.16.1 ,.24,5 25,5C,25C.16.2 :ASTM D 297-93(2006)16 16.2.1 ,-.16.2.2 :25C /3=DCBAA9971,0(7):A-,-,-,D-(25C),/3(/3).16.3 :16.3.1 .,.16.3.2 :25C /3=CBAA9971,0(8):A-,-,-,.16.4 :16.4.1 ,.ASTM D 297-93(2006)17 16.4.2:16.4.2.1 ,-.16.4.2.2 .16.4.3 0,01.,.(,),.,.16.4.4 ,.16.4.5:16.4.5.1 ,6(.1),().,.ASTM D 297-93(2006)18 ,.,.16.4.5.2 ,.,310 0,01.16.4.5.3 (0,01)3(0,001),.16.4.6 :16.4.6.1 .40 120 3;100 3.14.4.6.2 ,16.1(.25 0,5C).16.4.7:16.4.7.1 ,600 (87 .)(.1,.2 3).2 600 (87 .).1 18,9,7389 (1072 .).1,ASTM D 297-93(2006)19 ,.1-,2-3-4-5-6-/7-()8-.1 3 .,L-4 100 0,5C 8 10 50 47.5.4 25 3 1 3 HCl,2 3 AlCl3,5 3 MgCl2,10 3 NH4F,1 .NH4OH,0,5 3 NH4OH.,30,.10 3 ,60 3 5 .,5 3 2,4-.-,47.5.3.ASTM D 297-93(2006)79 47.5.5 25 3.2 3 AlCl3,10 3 NH4F,.NH4OH,-,1,0 3 HCl,.NH4OH,47.5.4,.47.6:47.6.1:=W/(V 40)(39)47.6.2:ZnO,%=(V C 100 100)/(S A)(40):-,ZnO/3,W-,V-,3,S-,A-,3.47.7:21 47.7.1 6 7 .1 27%ZnO.(2S%,D2S%).47.7.2 (),3,0%(2S%).,4,2%(D2S%)21 -ASTM International RR:D11-1009.ASTM D 297-93(2006)80 .47.7.3 (),4,4%(2S%).,6,2%(D2S%).48.48.1:48.1.1 (H2S).48.1.2 (Na2CO3),.48.1.3 (50 Na2CO3/3).48.1.4 (NaNO3).48.2 (35.4.2 36.4),50-3,:5 Na2CO3 NaNO3.,400-3 125 3,.Na2CO3.,HCl,.NH4OH(2+3)HCl(1+1),4 5 3 HCl(1+1)/100 3,.Na2CO3.