ASTM_D_3906_-_03_2008_rus.pdf

D 3906 03(2008),STANDARD TEST METHOD FOR DETERMINATION OF RELATIVE X-RAY DIFFRACTION INTENSITIES OF-TYPE-CONTAINING MATERIALS :1217-10/ASTM :31.05.2010 2010 (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FGU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FGU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.-,.9,-49,-1,119991.:(495)236-54-49:(499)230-13-72 E-mail:interstgost.ruhttp:/www.interstandart.ru ASTM D 3906-03(2008)D 3906 03(2008),1 D 3906;,.()1.1.1 ,Y X,Y.24,2-25,0 (2,42-2,50).A1.2 ,.1.3 1 ASTM D32 D32.05 s.1 2008.2008.1980.2003 D 3906-03.1ASTM D 3906-03(2008)(XRD)-,.1.4 ,NaY.(Y X,REY .),%XRD /NaY.1.5 .:1.5.1 ,.1.5.2 .1.6 ,.,.2.2.1 ASTM:2E 177 ASTM E 456 .E 691 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.2ASTM D 3906-03(2008)3.3.1 ,(NaY),.,%XRD /NaY.,(533)(23,5 Cu K),%XRD /NaY(533)4.4.1 Y X,.,.Y (FCC),X ,.4.2 Y X ,.,.Y X .,.3ASTM D 3906-03(2008)H2O .,Y X .4.3.1-,4.3,.(2).1 ASTM NaY;4ASTM D 3906-03(2008)4.4 ,.,.5.5.1 ,-.5.2 ,110C.5.3 (),35%,CaCl26H2O.Y Na (2).2 NaY 5.4 5ASTM D 3906-03(2008).6.6.1 NaY RE Y .3 7.7.1 ,.7.2 ,.1 ,.8.8.1 ,8.2-8.5,NaY.8.2 3-5 110C 1.35%,16.2 ,.8.3 ,.8.4 ,14 35 2 1/3 (NIST),100 Bureau Dr.,Stop 3460,Gaithersburg,MD 20899-3460.6ASTM D 3906-03(2008),.8.4.1 ,10/.()NaY,(533)23,6 50 100%.(),.,(533),10%.1 NaY ,.8.5 ,.(.2 NaY.)8.6 ,1/4/.3 ,.,0,02 2/1 NaY,10-20 .8.6.1 22,5 25 2,(533).3 NaY.,(,):14,0 17,0,(331)19.0 22,0,(440)25,5 28,0,(642)7ASTM D 3906-03(2008)4 8.6 ,.,24,2-25,0 (2,42-2,50)A.X1 .(2).3 NaY ASTM 9.9.1 8ASTM D 3906-03(2008)()8.4,:9.1.1 (9.2 ),9.1.2 (9.3 ,),9.1.3 ,(9.4 ).9.2 :9.2.1 ,SFC-,SFX,SFR.,SFC=SFX/SFR.,.9.2.2 (533),8.6.,.,WF,WX,NaY,WR.,WF=WX/WR.5 .:,0,2;,.9.2.3 ,%XRD /NaY .(9ASTM D 3906-03(2008),8.4.,SFC,9.2.1,WF,9.2.2.1:6 2,1 24,2-25,0 (2,42-2,50).A 7 ,NaY.1 2 hkl Peak 2 hkl 1 15,7 0,2 331 2 18,7 0,2 511,333 3 20,4 0,3 440 4 23,7 0,4 533 5 27,1 0,5 642 6 30,8 0,5 822,660 7 31,5 0,5 555,751 8 34,2 0,6 664 9.2.4 :%XRD /NaY=SFX WF (SX/SR)100(1):SX-SR-NaY.:,(533),.10ASTM D 3906-03(2008),.,.9.3 :9.3.1%XRD/NaY,(),8.4(.7).:%XRD /NaY=100RXSS(2):S-,SR-NaY.9.4 :9.4.1%XRD/NaY,(),8.4(.7).:%XRD /NaY=100rxSS(2):Sx-,Sr-NaY.9.5 XRD ,.,(533).11ASTM D 3906-03(2008),.,8.6.(533)()8.6 ,NaY :9.5.1 ,8.6;9.5.2 ;9.5.3 .9.5.4 .,.3,(622),0,25 (533),.,.%/NaY(533)=100 (CX/CR)(4):CX-,CR-NaY.%XRD /NaY(533)=100 SFC (AX/AR)(5):AX-AR-,NaY.%XRD /NaY(533)=100 SFC WF (HX/HR)(6):HX-HR-NaY.12ASTM D 3906-03(2008)-,(533)8.6,(331),(440),(642),(533).9.6 ,9.2,9.3 9.4:%XRD /NaY NaY,NaX 90 105 NH4Y 100 115 REY 25 50 Y 80 95 9.7 ,.9.8,9.2-9.4 ,.,9.2-9.4,1/2 2 9.5.,%XRD /NaY%XRD /NaY(533).9.9 9.2.2.,.10.10.1 :10.1.1 XRD /NaY.,REY,XRD /REY.13ASTM D 3906-03(2008)10.1.2 ,.(.9.1-9.4)(533)(.9.5).11.4 11.1 ,.E 691,.11.2 ,2,772 S,2,772 S 95%,S .E 456 E 177.()95%()95%()A 25,4 1,3%(5,2%)5,9%(23%)12,3 0,9%(7,3%)8,7%(71%)12,8 1,1%(8,6%)4,4%(34%)8 ,.11.3 .4 ASTM ,Report RR:D32-1010.14ASTM D 3906-03(2008)12.12.1;()X1.X1.1 15ASTM D 3906-03(2008)ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).16