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TM_D_5854_
_19a
Designation:D585419aManual of Petroleum Measurement Standards(MPMS),Chapter 8.3Standard Practice forMixing and Handling of Liquid Samples of Petroleum andPetroleum Products1This standard is issued under the fixed designation D5854;the number immediately following the designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon()indicates an editorial change since the last revision or reapproval.1.Scope*1.1 This practice covers handling,mixing,and conditioningprocedures that are required to ensure that a representativesample of the liquid petroleum or petroleum product isdelivered from the primary sample container or container orboth into the analytical apparatus or into intermediate contain-ers.1.2 Appendix X1 details the background information on thedevelopment of Table 1 used in performance testing.AppendixX2 provides guidance in the acceptance testing for water incrude oil.Appendix X3 provides a guide for materials ofsample containers.Appendix X4 provides a summary ofrecommended mixing procedures.Appendix X5 provides aflow chart for sample container/mixing system acceptance test.1.3 For sampling procedures,refer to Practices D4057(APIMPMS Chapter 8.1)and D4177(API MPMS Chapter 8.2).Practice D5842(API MPMS Chapter 8.4)covers sampling andhandling of light fuels for volatility measurement,and D8009(API MPMS Chapter 8.5).1.4 It is recommended that the users of this practice performthe tests in Practice D4177(API MPMS Chapter 8.2)beforeperforming the test in this practice.1.5 This standard does not purport to address all of thesafety concerns,if any,associated with its use.It is theresponsibility of the user of this standard to establish appro-priate safety,health,and environmental practices and deter-mine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accor-dance with internationally recognized principles on standard-ization established in the Decision on Principles for theDevelopment of International Standards,Guides and Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade(TBT)Committee.2.Referenced Documents2.1 ASTM Standards:2D3700 Practice for Obtaining LPG Samples Using a Float-ing Piston CylinderD4057 Practice for Manual Sampling of Petroleum andPetroleum ProductsD4177 Practice for Automatic Sampling of Petroleum andPetroleum ProductsD4306 Practice for Aviation Fuel Sample Containers forTests Affected by Trace ContaminationD5842 Practice for Sampling and Handling of Fuels forVolatility MeasurementD8009 Practice for Manual Piston Cylinder Sampling forVolatile Crude Oils,Condensates,and Liquid PetroleumProducts2.2 API Documents:3Manual of Petroleum Measurement Standards,Chapter 10,Sediment and Water(all sections)Publication 2003,Protection Against Ignitions Arising Outof Static,Lighting,and Stray CurrentsPublication 2026,Safe Descent onto Floating Roofs ofStorage Tanks in Petroleum ServicePublication 2217,Guideline for Confined Space Work in thePetroleum Industry2.3 Department of Transportation:4Code of Federal Regulations,Title 49,Section 1732.4 Occupational Safety and Health Standards:429 Code of Federal Regulations,Subpart Z,“Toxic andHazardous Substances,”Part 1910.1000 and following1This practice is under the jurisdiction of ASTM Committee D02 on PetroleumProducts,Liquid Fuels,and Lubricants and the API Committee on PetroleumMeasurement,and is the direct responsibility of Subcommittee D02.02 the jointASTM-API committee on Hydrocarbon Measurement for Custody Transfer(JointASTM-API).This practice has been approved by the sponsoring committees andaccepted by the Cooperating Societies in accordance with established procedures.Current edition approved May 1,2019.Published July 2019.Originally approvedin 1996.Last previous edition approved in 2019 as D5854 19.DOI:10.1520/D5854-19A.2For referenced ASTM standards,visit the ASTM website,www.astm.org,orcontact ASTM Customer Service at serviceastm.org.For Annual Book of ASTMStandards volume information,refer to the standards Document Summary page onthe ASTM website.3Available from American Petroleum Institute(API),1220 L.St.,NW,Washington,DC 20005-4070,http:/www.api.org.4Available from the Superintendent of Documents,U.S.Government PrintingOffice,Washington,DC 20402.*A Summary of Changes section appears at the end of this standard Jointly copyrighted by ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,USA and the American Petroleum Institute(API),1220 L Street NW,Washington DC 20005,USAThis international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards,Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade(TBT)Committee.1 3.Terminology3.1 D