ASTM_D_5542_-_16_rus.pdf

D554216 STANDARD TEST METHODS FOR TRACE ANIONS IN HIGH PURITY WATER BY ION CHROMATOGRAPHY 2018 ():09.07.2018:3485-18/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D5542-16 1 D554216 1 D 5542;,.()1.1.1 (/),.,.,.,:1 ASTM D19 D19.03 ,.1 2016.2016.1994.2009.D 5542-04(2009).DOI:10.1520/D5542-16.ASTM D5542-16 2 (/)()(/)A A:7-16 0-24 0.8 0-39 B 0-55 1.8 B:17-24 0-14 0.7 0-414 6.8 0-346 5.6 A ,99%-,EPRI(-),16 24.B .1.2 .1.3 A:,1 100/,3 100/,2 100/.1.4 B:,1 100/,10 200/,5 200/.1.5,.1.6 ,.,.ASTM D5542-16 3 2.2.1 ASTM:2D1066 D1129,D1192 D1193 3 D3370 D3856 ,D4210 3D4453 D5810 D5847 3.3.1:3.1.1 ,D1129.3.2 :3.2.1 (),.2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3.www.astm.org.ASTM D5542-16 4 3.2.1.1 ,.3.2.2 ,.3.2.3 ,.3.2.4 .3.2.5 ,.3.2.6 ,.3.2.7 .3.2.8 ,.3.2.9 ,.3.2.9.1 ,.ASTM D5542-16 5 :0,75 2,2 :2/:TAC-1 IonPac AG4A IonPac AS4A :AMMS 25 3/:10 :1.5/2.20/3.20/4.20/.1 A 4.4.1 ,.1/.4.2 ,.4.3 ,.,.ASTM D5542-16 6 ,pH ,.4.4 ,.,.4.5 /,.,.5.5.1 .,.45.1.1 ,.5.2 ,I D1193.,4 ,.,.,BDH Ltd.,Poole,Dorset,U.K.,and ,Inc.(USPC),Rockville,MD.ASTM D5542-16 7 I 0,22-.,.0,2 ppb()I.6.6.1 D1066,D1192,D3370 D4453,.6.2 ,.,.6.3 48 .,4C .6.4 ,.A ,7.7.1 ,.,ASTM D5542-16 8 .1.7.2 20,1.,(.).8.8.1 D4210 D5847 D3856.,.8.2 .().,.8.2.1 D5847 ,.ASTM D5542-16 9 8.2.2 ,.8.3 (),.,.(),.,.15%,.-,.8.4 (20).(15%),.,.8.5 (20)(),.ASTM D5542-16 10 ,.,.,:=x+3S(1)=x 3S(2):x-,S-,.8.5.1 ,.,.8.7 ()(20).D5810 11.11 8.6 ,().()(20),.ASTM D5542-16 11 D3856.%().8.8 ()(20).,().D5810 D3856.%().F()(.D5847,.6.3.1.1),3-8 .D5847.8.9 (),.,.1.1 .,.8.10 ,.ASTM D5542-16 12 .2 9.9.1 .2.,(,20),.,.,.,.9.1.1 ,.-ASTM D5542-16 13 ,./.9.2 .,.10.10.1 ,.(,),.10.2 ,.,.10.3 ,.80%.10.4 (/),(pH).,ASTM D5542-16 14 .11.11.1 ,.2.11.1.1 .11.1.2 ,2 5/2000 .,/.11.1.3 ,5/200 .,/.11.1.4 ,20 .11.1.5 ,.11.1.6 ,.11.1.7 ,.ASTM D5542-16 15 11.1.8 ,0 15000/.11.1.9,2 .11.1.10 ,.,.11.1.11 270 .10.1.12 ,.:AG-4A :AG-4A :AS-4A :_ A Dionex Corp.12.12.1 0,25 (0,75)0,93 (2,2)4.,.12.2 3 4 .12.3 :ASTM D5542-16 16 12.3.1 ,(1,00 =1,00 F)2,210 (NaF)1.12.3.2 ,(1,00 =1 )1,389 1.12.3.3 ,(1,00 =1 )1,511 1.12.3.4 ,(1,00 =1,00 )(NaCl)1 100C .1,648 1.12.3.5 ,(1,00 =1,00 PO4)1,433 (KH2PO412.3.6 ,(1,00 =1,00 SO)1.412.4 1000/,1,00 1.)1 105C .1,479 1.12.5 ,.,.,.5,10 25/.,5,10 25 1 ASTM D5542-16 17 .,.12.6 ,().,.13.13.1 ,.13.2 ,.12.5,:13.2.1 (,).13.2.2 (,).13.2.3 ,.13.2.4 .13.2.5 .ASTM D5542-16 18 13.2.5.1 10/0,2/10,2/.13.3 ,.13.3.1 ,.13.3.2 .13.3.3 .13.3.4 ().13.4 .14.14.1 .14.1.1 .1 30/.,ASTM D5542-16 19 ,.14.2 ,(15 20).,.14.3 ,.-/.(:,.).14.4 ,.15.15.1 /.15.2 :/=F :A-,/F-.15.3 ,.ASTM D5542-16 20 16.(A)16.1 ,-,1.5 -,2004.1 A :n-(),SoS-,tNA-.-,5 -No.(2).RP 2712 ,J.K.Rice,-,.-,3 1987.,/5%So,/St,/.ASTM D5542-16 21 B ,17.17.1 ,2000/.1.3.17.2 ,.:5 :2/:TAC-1 IonPac AG4A IonPac AS4A :AMMS :17 5/:10 :1.()2000/2.8/3.16/4.16/5.16/.3 B 17.3 20,1.,(,1%),30,.ASTM D5542-16 22 18.18.1 ,D4210 D5847 D3856.,.18.2 .().,.18.2.1 D5847 ,.18.2.2 ,.18.3 (),.ASTM D5542-16 23 ,.(),.,.15%,.-,.18.4 (20).(15%),.,.18.5 (20)(),.,.,.,=x+3S:(3)=x 3S(4)ASTM D5542-16 24 :x-,S-,.18.5.1 ,.,.18.6 .(20),.18.7 ()(20).D5810 11.11 D3856.%().18.8 ()(20).,().D5810 D3856.%ASTM D5542-16 25 .F()(.D5847,.6.3.1.1),3-8 .D5847.18.9 (),.,.1.1 .,.18.10 ,.19.19.1 .2.,(,20),.,.,.,.,.,ASTM D5542-16 26 ./.19.2 .,.20.20.1 ,.(,),.20.2,.,.,.,.20.3 ,.,.ASTM D5542-16 27 20.4 ,.20.5 (,),.30,.,.2 B :n-(),SoS-,tNA-.-,/5%So,/St,/.ASTM D5542-16 28 21.21.1 ,A(.11).22.22.1 A,.22.2 (5 )7,6 ()4.,.23.,22.1 A(.13,14 15).24.(B)24.1 ,-,2.5 -,2004.25.25.1;,.ASTM D5542-16 29 ()A1.A1.1 ,.:A1.1.1 ,A1.1.2 ,A1.1.3 pH,A1.1.4 ,A1.1.5 ,A1.1.6 .A1.2 ,.(),.,.A1.3 ,:A1.3.1 1 ,.,.-(OH).A1.3.2 1/(,).ASTM D5542-16 30 1 2 50 1/3 50 4 ,:.A1.1 A1.3.3 ,.A1.1,.A1.3.4 50 1/.A1.3.5 ,.A1.1.A1.3.6 80%.-50 50 (15 4/)ASTM D5542-16 31 ()X1.X1.1 D5542 X1.1.1 (1/)().-(2013.).,.X1 -,.X1.2,X1.2.1 A B.A -(.1)/,.,.X1.2.2 B(.3),.,.ASTM D5542-16 32 ,.,.(5),.X1.3 X1.3.1 .,.,.X1.1.X1.4 X1.4.1 -.,.,.ASTM D5542-16 33 X1.4.2 ,.X1.2 .X1.5 X1.6 X1.5.1 .,.X1.6.1 ,.X1.7 X1.7.1 .X1.1 X1.2 .ASTM D5542-16 34 .X1.1 :Thermo ScientificTM Dionex lonPac AG14,ASH,2 :10 /7,5 NaOH,0-4,65 /48,75 MaOH 4,01,65 /48,75 NaOH,4,01-8,50,10 /7,5 8,51,10 /7,5,8,51-15 :0,5/:1 :30C:,Thermo Scientific Dionex ASRS 300