Designation:D5865−13StandardTestMethodforGrossCalorificValueofCoalandCoke1ThisstandardisissuedunderthefixeddesignationD5865;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginaladoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperscriptepsilon(´)indicatesaneditorialchangesincethelastrevisionorreapproval.1.Scope*1.1Thistestmethodpertainstothedeterminationofthegrosscalorificvalueofcoalandcokebyeitheranisoperiboloradiabaticbombcalorimeter.1.2ThevaluesstatedinSIunitsaretoberegardedasstandard.Nootherunitsofmeasurementareincludedinthisstandard.1.3Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappro-priatesafetyandhealthpracticesanddeterminetheapplica-bilityofregulatorylimitationspriortouse.SpecifichazardstatementsaregiveninSection8.2.ReferencedDocuments2.1ASTMStandards:2D121TerminologyofCoalandCokeD346PracticeforCollectionandPreparationofCokeSamplesforLaboratoryAnalysisD388ClassificationofCoalsbyRankD1193SpecificationforReagentWaterD2013PracticeforPreparingCoalSamplesforAnalysisD3173TestMethodforMoistureintheAnalysisSampleofCoalandCokeD3177TestMethodsforTotalSulfurintheAnalysisSampleofCoalandCoke(Withdrawn2012)3D3180PracticeforCalculatingCoalandCokeAnalysesfromAs-DeterminedtoDifferentBasesD4239TestMethodforSulfurintheAnalysisSampleofCoalandCokeUsingHigh-TemperatureTubeFurnaceCombustionD7582TestMethodsforProximateAnalysisofCoalandCokebyMacroThermogravimetricAnalysisE144PracticeforSafeUseofOxygenCombustionVesselsE178PracticeforDealingWithOutlyingObservationsE882GuideforAccountabilityandQualityControlintheChemicalAnalysisLaboratoryE2251SpecificationforLiquid-in-GlassASTMThermom-eterswithLow-HazardPrecisionLiquids3.Terminology3.1Foradditionaldefinitionsoftermsusedinthistestmethod,refertoTerminologyD121.3.2Definitions:3.2.1adiabaticcalorimeter—acalorimeterthatoperatesintheadiabaticmodeandmayormaynotuseamic...
