TM_D_5159_
_04_2014_rus_scan
MEXTOCYAAPCTBEHHbIM COBET No CTAHAAPTM3ALN,METPONor CEPTOKALM(MrC)INTERSTATE COUNCIL FOR STANDARDIZATION,METROLOGY AND CERTIFICATION(ISC)FOCTMETOCYAAPCTBEHHbI33583-CTAHAAPT2015yrOb AKTBPOBAHHbINPAHYJIPOBAHHbIMCTaHAapTHbIn MeToA onpegeneH nbineo6pa3oBaHnAnp CTpaHM3AaHne onnanbHoeMocKBaGnCTaHAapTHopM2016FOCT 33583-2015ME KTOC YA APC TBEHHbIMC TAHAAPTyOb AKTMBMPOBAHHbIM PAHYMPOBAHHbIMCTaHAaptHLI MetoA onpeAeneHA nLineo6pa3oBaHnA npn nctupaHnnGranular activated carbon.Standard method for determination of dusting attritionAaTa BBeAeHn-2017-04-011 06nacTb npMeHeHA1.1 Hactogwn cTaHAapt ycTaHaBnnBaet npouegypy oueHkn conpoTuBneHnA(cTokoctu)rpaHynupo-BaHHbIX aKTBnpoBaHHbix yrne k nbineo6pa3oBaHnio np ncTpaHn.B HacToeM cTaHAapTe Ko3中nun-eHt nbineoopa3oBaHng npu nctupaHnn,DA,onpegengeTcA Kak Macca(unn paccynTaHHbI o6beM)nbInn BeqnHnLy BpeMeHn,co6paHHo ha npeABapnTenbHO B3BeweHHOM 中NLtpe,no otHoweHnio K Macce eAHbIyrng,noMeweHHon B ycTaHoBneHHoe(onpegeneHHoe)Bn6panOHHoe ycTpoicTBo Ha onpegeneHHoe BpeMA.Take MokeT 6bITL onpegeneHo nepBoHa4anbHoe cogepxaHe nbinn B npo6e.An HacTouero cnbiTaHngrpaHynupoBaHhbi aktuBupoBaHhbi yronb gonkeH cogepxatb He MeHee 90%4actny,pa3Mep koTopbix 6onb-we 80 Mew(0,18 MM)(cM.ASTM D 2867).1.2 EAnHbi n3MepeHng,npuBeAeHHble B cncTeMe CN,cunTalotcA ctaHAapTHbIM.EAnHNLbi N3Mepe-hu(AoMbi n 中ytbi),yka3ahhble B cko6kax,npuBegeHbi Ang nHopmaynn.1.3 B HacToAueM cTaHgapte He npeAycMoTpeHo paccMOTpeHe Bcex BonpocoB o6ecne4eHnA 6e3onac-HOCTM,cBA3aHHbIX c ero cnonb3oBaHeM.onb3oBaTenb cTaHgapTa HeceT OTBeTCTBeHHOCtb 3a o6ecne4e-HMe cooTBeTCTByHOWMX Mep 6e3onacHocT n oxpaHbI 3AopoBbA u onpegenget yenecoo6pa3HOcTbnpMeHeHn 3aoHoaTenbHbx orpaH4eH nepeg ero cnonb3oBaHeM.2 HopMaTBHble ccbInKnAng npuMeHeHng Hactoguero ctaHgapta Heo6xoguMbi chegyiouwne ccbino4Hble gokyMeHtbi.An Hega-TpoBaHHbIX ccbInoK npMeHoT nocneHee n3gaHe ccbino4Horo gokyMeHTa(Bknio4ag Bce ero n3MeHeHng).2.1 CTaHAapTbI ASTM1)ASTM D 2854 Test Method for Apparent Density of Activated Carbon(MeTog onpegeneHn HacbInHoinnoTHOCT aKTBpoBaHHoro yrng)ASTM D 2867 Test Methods for Moisture in Activated Carbon(MeTogbi onpegeneHn Bnarn B aKTBnpo-BaHHOM yrne)ASTME 11 Specification for Woven Wire Test Sieve Cloth and Test Sieves(CTaHgapTHa cneunpnKaunaHa npoBono4Hy cToTKaHb cnbITaTenbHble cTa)ASTM E 300 Practice for Sampling Industrial Chemicals(paKTuKa or6opa npo6 npoMbIWneHHbIX XnMM-yecknx npoAykToB)1)YTO4HNTb CCbUKn Ha cTaHgapTbi ASTM MOHO Ha cavite ASTM:www.astm.org nnu B cny6e noggepxkn KnneH-ToB ASTM:serviceastm.org.B nHpopMaunoHHoM ToMe exerogHoro c6opHnKa cTaHgapToB(Annual Book of ASTMStandards)cnegyer o6pauaTbc K cBogke cTaHgapToB exerogHoro c6opHnKa cTaHgapToB Ha cTpaHnue caviTa.M3aHne onunanbHoe0CT33583-20153 CywHocTb MeToAa3.1 OnpeneneHHbln o6beM onpeneneHHoN Maccbl rpaHynnpoBaHHoro aKTNBNpoBaHHoro yrna noMewa-HOT B npobonepatenb,KoTopbin nonBepraoT BNopauln c nocTOAHHbIM yckopeHneM(g)B TeueHve onpeneneH-Horo BpeMeHn.IbInb nepeHOCNTCA Bo3nyWHbIM noTOKOM,npoXonAwM yepe3 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MeTonoB NcnblTaHwn,npouenypa wcnblTaHwN,ycTaHoBneHHaa HacTog-WNM CTaHnapToM,no3BonaeT N3MepNTb neNcTBNe cNnbl TpeHNA,BO3HWKalowen Mexkny BN6pnpyiowNMN MMenneHHO ABnraOwNMNCA yacTnuaMN Bo BpeMa NcnblTaHna,N Mano 3aBNCNT OT pa3Mepa,opMbl n nnoTHOC-TN 4aCTNU5 O6opynoBaHne n Tpe6oBaHna K HeMy5.1 Bn6paunoHHa ycTaHoBKa2),cnoco6Has o6ecneyNTb RMS(cpeAHekBanpaTnyHoe 3HayeHne)ycko-peHne 40 M/c2(4g).5.2 VcnblTaTenbHaa ayenka(KaMepa),CM.pwcyHOK 1,N3roToBneHHaa N3 anoMNHnA wnM Apyroro 3neK-TponpoBonawero MeTanna.5.3 nbe3o3neKTpnuecknN akcenepoMeTp3)cnoco6HbIN N3MepNTb RMS yckopeHne,BblopaHHoe nonb30-BaTeneM.nonxonawa ycTaHoBKa n 3HayeHna 40 M/c2(4g)noka3aHa Ha pncyHKax 1 n 2.5.4 npeo6pa3oBaTenb cnrHana4),na B3anMonencTBna akcenepoMeTpa c MnnnnBonbTMeTpoM AC,cnoco6HbIn npoN3BOANTb BbIXO Hoe nMHeNHoe HanpaxkeHne OT 0 no 1 B,nponopunoHanbhoe yckopeHno.5.5 BonbTMeTp5)nepeMeHHoro ToKa OT 0 Ao 1 B.5.6 AMnepMeTp nepeMeHHoro Toka oT Oo 1000 MA c norpewHoCTblo N3MepeHna no 1 MA.5.7 PerynupyeMbin TpaHcdpopMaTop oT 0 Ao 120 B.5.8 TanMep oT 0 no 120 MMH.5.9 Pe3WHoBaa Bn6pon3onAuNoHHaa npoknanka.PekoMeHnyeTca Ncnonb3oBaTb npoknanky N3 Heonpe-HOBoN pe3MHbI TBep oCTblo 45 ycn.en.5.10 PacxonoMep c perynnpylowM knanaHoM,cnoco6HbIN KOHTponnpoBaTb TOK Bo3Ayxa npn cKopoc-TN,BblopaHHon nonb3oBaTeneM HacTogwero cTaHnapTa.noToK npNMepHo 7 n/MNH CYWTaHOT nonxonAWNM npMNcnonb3oBaHnn o6opynoBaHna,noka3aHHoro Ha pncyHKax 1 W 2.5.11 nnbTp nna ynaBnnBaHna yacTnu,nonxonawero pa3Mepa Ang coeAnHeHna c ncnblTaTenbHonAyeNkon(KaMepon),cnoco6Hbin ynaBnnBaTb yronbHyio nbinb.wnbTpbl N3 CTeknoBonoKHa CuNTalOTca nonxo-WNMN.Takke 3pobeKTNBHbIMN B Ncnonb3oBaHnN ABNAHOTCA NnbTpbl ynaBnnBaHna TBepnblx yacTNU,npe Ha3HayeHHble n 3aWNTbl opraHoB bixaHNA npn okpacke pacnbineHneM wnN npyrx onacHOCTAX,BO3HN-KarowNx npl pacnbineHNN.5.12 TpagyupoBaHHbin unnNHap BMeCTNMOCTbIo 100 Mn.5.13 AHanTMyeckne Becbl c norpewHoCTblO N3MepeHNA no 0,1 Mr.2)HanpnMep MOXHo ncnonb30BaTb Bn6paunoHHyo ycTaHoBKy KoMnaHnn Buffalo Dental Manufacturing Co.,(Underhill Blvd.,Syosset,NY 11791),Mogenb Ne 1,40 BT npn 115 B,60 Tu,a Takoke BM6pocTanKnBaTenb,Mogenb SyntronM J-1A,30 BT npn 115 B,60 Tu,wnm nx aHanor.3)HanpnMep MOXHo ncnonb3oBaTb akcenepoMeTp KoMnaHnn Endevco,Mogenb Ne 2251,nnn aHanoryHbin.4)HanpnMep MOXHo ncnonb30BaTb npeo6pa3oBaTenb CnrHana KoMnaHnn Endevco,MoAenb Ne 4416,pa6oTaownnnoapo MynTMeT Keithley 179 oM Keithley Instruments(AurorRd.,Cleveland,OH 44139).2OCT 33583-2015CTABalowa wnnba(4)Tpe6.10,32 UNF 5 Lq.(yHnupoBaHHa MenKa pe3b6a)Tanka 6apawek(4)Tpe6.10,32 UNFO-o6pa3Hoe ynnoTHnTenbHoe Konbuo(4)Tpe6.(6,4 MM)WecTrpaHHa ranka(8)Tpe6.10,32 UNFpKpbBaoa nnacTHa(cM.pcyHoK 3)Pe3MHoBa npoknaAKa(CM.npMe4aHe 1)McnbTaTenbHa 4eka(cM.pcyHoK 3)Pe3MHoBa npoknaka(cM.npMe4aHe 1)MeTannneckoe cTo(cM.npMe4aHMe 2)Pe3HoBa npoknaKa(cM.npMe4aHe 1)Pa3enTenbHa ce(CM.pcyHoK 3)TepnoHoBa npoknaka(cM.npnMeaHne 1)中nbTPTenoHoBa npoknaka(cM.npMe4aHne 1)eppoppoBaHHa nnacTnHa(cM.npMe4aHe 3)Pe3HoBa nponaKa(cM.npMe4aHe 1)BbTHa CeKM(CM.PCyHOK 3)BuHt c nnocko unHApuecko ronoBko(2)Tpe6oBane8,32 UNC Lq.CTonopHa wa6a(2)Tpe6oBaHe An 8 6onToBWecTrpaHHa ranka(2)Tpe6oBaHne 8,32 UNCBepXHAA KpeneHa nnTa B6paOHHO ycTaHOBKn(CM.pMcyHoK 3)WbpeBo naroBb coeHTenAn NPT-(1)门pume4aHue 1-BHytpeHHn qnametp-2 3/4 goiMa(69,9 MM),Hapyxhbi Anametp-3 AoMa(76,2 MM),TonwHa 1/16 AoMa(1,6 MM).门puMe4aHne 2-poBono4HaA tKaHb 250 MKM 3 HepxaBeowen cTann AuaMeTpoM 3 AonMa(76,2 MM)no ASTM E 11.门puMe4aHne 3-lnactnHa c nponycKHLIM ce4eHneM 37%,n3roToBneHHaR n3 24 HepKaBelowencrann,Anamerpom 0,45 qoMa(11,4 MM),c orBepcrugmn 0,066 oiMa(1,68 MM)B yeHTpe,kBaApaTHaRceTka AaMeTpoM 3 AoMa(76,2 MM).PcyHoK 1-cnbiTaTenbHa 4eka An oTceBa nin6 logroToBka npo6bi,06pa3ybi n 06pa3ybi An cnbitahn6.1 OT6npalot npo6bi rpaHynnpoBaHHoro aKTnBnpoBaHHoro yrng B cooTBeTcTBnn c ASTM E 300(CM.Taloke 8.1).3