ASTM_D_5185_-_18_rus.pdf

D5185-18 -(-)STANDARD TEST METHOD FOR MULTIELEMENT DETERMINATION OF USED AND UNUSED LUBRICATING OILS AND BASE OILS BY INDUCTIVELY COUPLED PLASMA ATOMIC EMISSION SPECTROMETRY(ICP-AES)2018 ():14.06.2018:3466-18/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D5185-18 1 D5185-18 -(-)1 D5185;,.().,.1 ASTM D02 ,D02.03 .1 2018.2018.1991.2013.D5185-13 1.DOI:10.1520/D5185-18.ASTM D5185-18 2 ,D4628,D4927 D4951.1.*1.1 ,-(-).1.1.2 ,.1,.1.3 -,190,.,.1.4 .2.1.5,.1.6 ,*2,K.,.,.,.,.,56,1984.ASTM D5185-18 3 .2 3,.,.1.A ,308,22;396,15;309,27 233,53;455,40;493,41 249,77 315,89;317,93;364,44;422,67 205,55;267,72 324,75 259,94;238,20 220,35 279,08;279,55;285,21 257,61;293,31;293,93 202,03;281,62 231,60;227,02;221,65 177,51;178.29;213,62;214,91;253,40 766,49 589,59 288,16;251,61 328,07 180,73;182,04;182,62 189,99;242,95 337,28;350,50;334,94 292,40;309,31;310,23;311,07 202,55;206,20;213,86;334,58;481,05 A ,.1.7,.1.8 ,.,ASTM D5185-18 4 ,.6.1,8.2 8.4.1.9 -,(TBT).2.2.1 ASTM:3 1109 -D1552 (IR)(TCD)D4057 D4177 D4307 D4628 ,D4927 ,3 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D5185-18 5 D4951 -D7260 ,-(ICP-AES)E135,3.3.1:3.1.1 .E135.3.2 ,:3.2.1 ,.3.2.2 ,.3.2.3 ,.3.2.4 ,.3.2.5 ,.3.2.6 ,.ASTM D5185-18 6 2.,/,/6-40 0,71 X0,41 0,5-4 0,24 X0,66 4-30 0,26 X 40-9000 0,0020 X1,4 1-40 0,17 X0,75 2-160 0,12 X0,91 2-140 0,13 X0,80 10-160 1,6 X0,32 5-1700 0,16 X0,86 5-700 0,010 X1,3 5-200 0,29 X0,70 5-40 0,52 X0,49 10-1000 1,3 X0,58 40-1200 3,8 X0,33 8-50 1,3 X0,26 0,5-50 0,15 X0,83 7-70 0,49 X0,66 900-6000 0,49 X0,81 10-40 2,4 X0,17 5-40 0,54 X0,37 1-50 0,061 X 60-1600 0,15 X0,88 A:X=,/.3.2.7 ,(,).3.2.8 (),.3.2.9 ,.3.2.10 ,ASTM D5185-18 7 ,.3.2.11 ()(3 -300).3.2.12 ,.3.,/,/6-40 3,8 X0,26 0,5-4 0,59 X0,92 4-30 13 X0,01 40-9000 0,015 X1,3 1-40 0,81 X0,61 2-160 0,24 X 2-140 0,52 X0,80 10-160 3,0 X0,36 5-1700 0,72 X0,77 5-700 0,13 X1,2 5-200 0,64 X0,71 5-40 1,5 X0,50 10-1000 4,3 X0,50 40-1200 6,6 X0,29 8-50 2,9 X0,39 0,5-50 0,35 X 7-70 1,1 X0,71 900-6000 1,2 X0,75 10-40 2,1 X0,62 5-40 2,5 X0,47 1-50 0,28 X1,1 60-1600 0,083 X1,1 A:X=,/.4.4.1 ,.ASTM D5185-18 8 ,.,.4.2 ,-,D7260.5.5.1 -22 ,.,/.,.,.5.2 ,.,.,.,ASTM D5185-18 9 .5.2.1 .4.5.3 .,.4.();,;-,.ASTM D5185-18 10 6.6.1 ,.1.,.,.1.(,).6.1.1 ,.,.C1109,.4 ,.,.6.1.2 .4,.,-,1976,31B,.147-152.ASTM D5185-18 11 ,.,.6.1.3 ,Kia,:a,:Ca=Ia/Ha(1):Ca-a,Ia-(.,)a,Ha-6.1.3.1,i :Ci=Ii/Hi(2):Ii-a.6.1.3.2 ,Kia,:Kia=Hi/Ha=Ii/(Ci Ha)(3)6.1.3.3 Ii/Ha,Ci,.Ci Kia.:ASTM D5185-18 12 Ca,=(Ia+Ii)/Ha(4)Ca,=Ca+Ii/Ha(5)Ca=Ca,Ii/Ha(6)Ca=Ca,Kia*Ci(7):Ca=Ca,K1a C1 K2a C2 (8)6.1.4 ,i .Kia ,.6.2 .,.,.6.3 ,.,.ASTM D5185-18 13 7.7.1,0,001 0,0001,.7.2-,-,.1 .180.7.3 5,6 .7.4 ,().0,5 3/.6 .,.7.5 ,(),.7.6 ,5,.,1973,.102.6,.,M.,49,1977.ASTM D5185-18 14.7.7 ,().7.8,().8.8.1 .,.7 ,.8.2 U.S.P.,.(.).8.3 ,(-).8.4 ,7 ,DC.,.Analar Standards for Laboratory Chemicals,BDH Ltd.,Poole,Dorset,United States Pharmacopeia and National Formulary,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.ASTM D5185-18 15 0,0500%,.D4307.,.,0,0500%,.(,.)1 ,.,.8.5 ,D1552.,NIST SRM 1622c8 .8.6 ,.,.9.9.1 ,.8 (NIST),100 Bureau Dr.,Stop 1070,Gaithersburg,MD 20899-1070,http:/www.nist.gov.ASTM D5185-18 16,D4057 D4177.10.10.1 ,.10.2 ,.10.3 ,30.,.2 ,.10.4 -,.10.5 ASTM D5185-18 17 ,.,:,(),(),().,10.11.11.1 .,.11.2 ,.,.,5%,.,.11.3 ,11.2.:ASTM D5185-18 18 I(Re)=(I(e)I(Be)/I(is)(9):I(Re)-e,I(e)-e,I(Be)-e,I(is)-.11.3.1 .,.12.12.1 ,(),.,.12.2 20 0,500%,(-)1-1 .,.,100/;100-.ASTM D5185-18 19 13.13.1 ,.13.2 ().60C.13.3 ,.60C.14.14.1 .14.2 ,10/0,0500%-,(.7.1),45 .,.,.,.ASTM D5185-18 20 3 ,:2 0,0500%-4,8 90 .14.3 ,.14.4 .,10%.14.5 ,.,10%.,.15.15.1 ,(.,.).60.,.15.2 ,5%,ASTM D5185-18 21 .4 ,SRM 1085,.15.3 ,9,11.3.16.16.1 /,./,.17.9 17.1 .,.:,;,;,;SRM 10858,SRM 10838()40/(9 -ASTM International RR:D02-1282.ASTM Customer Service serviceastm.org.ASTM D5185-18 22 8%,),SRM 1085,SRM 1083 40/,SRM 1085,SRM 1083 2/12 .5 ,.D5185,.5.(/)(/)1 10 100 1000 1,8 2,6 1 32 0,2 1,0 1,0 8 0,8 5 3,3 7 1,2 8 61 0,2 4 1,5 7 1,6 4,9 19 71 17 37 2,4 0,2 1,0 2,2 130 3,5 1,3 0,1 0,6 8 65 17.1.1 ,ASTM D5185-18 23 ,.2 .5,.17.1.2 ,.3 .6,.6.(/)(/)1 10 100 1000 6,8 0,6 13 6 120 0,8 3,3 2,4 24 3,3 21 6,9 16 4,2 25 150 2,1 33 3,3 17 4,7 14 43 140 25 49 7,1 0,4 3,5 5,6