ASTM_D_4530_-_11_rus_scan.pdf

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cTaHAapToBCCbIN04HbIM CTaHAapTaM.11IV0CT32392-2013M E X rO C yA P C T B E HH bIC T A HA P THETEnPOnyKTbIOnpeneneHne KokcoBoro ocTaTka MWkpoMeToDOMPetroleum products.Determination of carbon residue by micro methodAaTa BBeneHna-2015-01-011 06nacTb npnMeHeHnA1.1 HacTogwnn CTaHnapT ycTaHaBnnBaeT MeTon onpeneneHna conepxaHn KoKcoBoro ocTaTka(MWK-poMeTo),o6pa3oBaBweroca nocne BbinapnBaHna N nwponv3a HedTenponyKToB npn ycTaHoBneHHbIX ycno-BNAX,wnpe Ha3HayeH nn onpeneneHnA CKnOHHOCTN TaKnx nponyKToB Ko6pa3oBaHnlo KoKca(npnMeyaHne 1).1.2 Pe3ynbTaTbl ncnblTaHwa no HacTogweMy CTaHAapTy 3KBMBaneHTHbl pe3ynbTaTaM NcnblTaHNA Cncnonb3oBaHneM MeTona KoHpancoHa no ASTM D 189n p n M e 4 a H M e 1-MeTog npencTaBnaeT co6on Mognonkauwio nepBoHauanbHoro TepMorpaBnMeTpnueckoroMeTopa M annapara a onpepeneHn KOKCoBoro ocTaTka B HedTenpopyKTax).na nonyueHn 3KBMBaneHTHblx pe3ynbTa-TOB npn Ncnonb3oBaHNn TepMorpaBnMeTpnueckoro MeTona ycnoBna NcnbITaHnA nonxkeH onpenenATb aHanNTNK.1.3 HacToawnn MeTon ncnblTaHa MOXHo ncnonb3oBaTb n ncnblTaHna HedTenpoAyKTOB,KoTopbleHacTNYHo pa3naraloTca npn neperoHke npn aTMocoepHoM naBneHwn N KOTopbIX 3HayeHNA KOKCOBOrOOCTaTKa HaxoAaTca BAMana3oHe oT0,10%Macc.Ao 30%Macc.O6pa3ubl,Ana KoTopblx npennonaraeMoe 3Ha-eHNe KoKcoBoro ocTaTka MeHee 0,10%Macc.,npenBapNTenbHoneperoHAOT nA OTroHa 90%06beMa npo6bl(CM.pa3nen 9).3aTeM 10%-HbIn oCTaToK B Kon6e aHanv3npyloT ana onpeneneHna KoKcoBoro OcTaTka noHacToAweMy MeTony WcnbITaHNA.1.4 3ona,onpeneneHHa no ASTM D 482,n TpyAHo ncnaparowneca npncankn MoryT 6bITb BKnoyeHbl Bobwee conepxkaHve KokcoBoro ocTaTka.1.5 n An3enbHoro TonnnBa,conepkawero anknnHnTpaTbl(aMnnHNTpaT,reKcnnHNTpaT wnn oKTMn-HNTpaT),3HayeHN KOKcoBoro ocTaTKa 6onbwe,yeM y TonnnBa 6e3 npncanKn,4To MoXKeT npnBecTn K own604-HOMy 3aknioyeHNIO o CKnOHHOCTN TonnNBa K o6pa3oBaHniO KoKca.ConepxaHne anknnHNTpaToB B TonnNBeonpenenaioT no ASTM D 4046.1.6 3HayeHNa B CNCTeMe ennHny CM paccMaTpnBaloT Kak cTaHAapTHble.1.6.1 VcknioyeHne-B 6.4 n6.5 ncnonb3yioT eAHnubl 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