ASTM_D_5600_-_17_rus.pdf

D5600-17 -(-)STANDARD TEST METHOD FOR TRACE METALS IN PETROLEUM COKE BY INDUCTIVELY COUPLED PLASMA ATOMIC EMISSION SPECTROMETRY(ICP-AES)2017 ():21.08.2017:3257-17/ASTM -,.9,-49,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D5600-17 1 D5600-17 -(-)1 D5600;,.().1.*1.1 -.1.2,.1.,.1.3 ,1 ASTM D02 ,D02.03 .1 2017.2017.1994.2014.D5600-14.DOI:10.1520/D5600-17.*ASTM D5600-17 2%.1.4,.1.5,.1.6 ,.,.1.7 -,(TBT).2.2.1 ASTM:2 D346 D1193 D6299 2 ASTM,-ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D5600-17 3 D7260 ,-(ICP-AES)E11 1.,A,/C 237,313;256,799;308,216;396,152 15-110 455,403;493,410 1-65 317,933;393,367;396,847 10-140 259,940 40-700 279,079;279,553 5-50 257,610;294,920 1-7 231,604;241,476;352,454 3-220 212,412;251,611;288,159 60-290 588,995;589,3;589,592 30-160 334,941;337,280 1-7 292,402 2-480 202,548;206,200;213,856 1-20 A -.,(.6.1).B ,-(Inductively Coupled Plasma Atomic Emission Spectroscopy,Winge,R.K.,Fassel,V.A.,Peterson,V.J.,and Floyd,M.A.,Elsevier,1985).,.3.3.1 :3.1.1 ,.3.1.2-/ICP-AES -.3.1.3 ,ASTM D5600-17 4 -.4.4.1 700C.(HCl)-(-),.,.5.5.1 .5.2 ,.6.6.1 ,ASTM D5600-17 5 .6.2 :(1);(2);(3)(4).6.3 ,.,.,.,.,.6.4 -.D 7260.ASTM D5600-17 6 7.7.1,0,0001 150.7.2 ,.7.3 ,.7.4,700C 10C 1000C 10C .7.5-,.7.6 (),(PTFE),12 (1/2).7.7 .7.8 .7.9 .7.10 .7.11 ,50 58.7.12 ,100 200.7.13 .7.14 .7.15,0,250 (60)0,075 (200),E11.ASTM D5600-17 7 7.16 ,.7.17 .7.18 ,2,5.8.8.1 .,3.,.8.2 ,II,D1193.8.3 ,.8.4 ,.8.4.1 (LiBO2),().8.4.2 (Li2B4O7),().8.5 1,20%(400 HCl,2000).8.6 2,.20,0 0,1 100 200.3 ,.,Analar Standards for Laboratory Chemicals,BDH Ltd.,Poole,Dorset,U.K.United States Pharmacopeia and National Formulary,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD().ASTM D5600-17 8 1000C 5 .,2.1000 1(20%HCl).2.1800.,.1 2 0,5 25 1.8.7 (99,9%),.1,0 50/()1000/().2 ,HCl(5%HCl+95%).,.,.3 .8.8 NIST ASTM D5600-17 9 SRM 2718A 2719 QC.4 9.9.1 ,.(60)0,250,D346.9.2 ,30 ,(60)0,250 (60,9.1,(200)0,075.110C 115C ,.9.2.1 0,075 0,250 -,-.10.10.1 -.10.2 ,.10.3 ,4 (NIST),100 Bureau Dr.,Stop 2300,Gaithersburg,MD 20899-2300,http:/www.nist.gov.ASTM D5600-17 10 ,30 .10.4 ,.10.5 ,.,(),(),().10.6 ,.(.11.6).10.7 .,.11.11.1 5 (0,1),9,50 58.11.2 700C 10C .ASTM D5600-17 11 11.3 ,0,5 (0,0005).1000C 10C .,.-,.11.3.1 .,.11.3.2 1000C 10C,.,30.,.-,.11.4 5-10 ,25 1 .30,ASTM D5600-17 12.11.4.1 ,-.,.11.5 ,100,.11.6 ,2,.11.7 ,50 2 100,.4 ,-.11.8 -,11.7,.11.9 .12.12.1 :,/()/(DCWVA(1)/10000/,%,MM(2):M-,A-/()M ,ASTM D5600-17 13 V-,W-,(C/D)-,(C ,D ).13.13.1 /()%(1000/()=0,1%).14.14.1 (QC)(.8.8).14.2 /(QC/QA),.14.3 QC/QA,.D6299.15.15.1 .2,ASTM RR:D02-1007.15.1.1 ,.2.15.1.2 ,ASTM D5600-17 14 ,.2,.2.1 X /.,/0,32 X0,66 0,92 X0,66 0,19 X0,66 0,71 X0,66 7,2 20,8 1,66 X0,5 3,77 X0,5 0,21 X0,66 0,61 X0,66 0,042(X+2,55)0,34(X+2,55)0,52 X0,66 0,96 X0,66 0,09(X+4,80)0,20(X+4,80)1,04 X0,5 3,52 X0,5 0,75 1,16 0,20 X0,75 0,35 X0,75 1,07 X0,33 2,20 X0,33 15.1.3 ,.2,.15.1.4 D5600 ,.16.16.1;e;-;ASTM D5600-17 15;,;D02.03 (D5600-14),.(1 2017.)(1)2.1,8.8,14 4.ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.()ASTM 610-832-9585,610-832-9555 serviceastm.org (www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.