ASTM_D_5708_-_15_rus.pdf

D 5708-15 ,-()STANDARD TEST METHODS FOR DETERMINATION OF NICKEL,VANADIUM AND IRON IN CRUDE OILS AND RESIDUAL FUELS BY INDUCTIVELY COUPLED PLASMA(ICP)ATOMIC EMISSION SPECTROMETRY ():2820-16/ASTM :25.01.2016 2016.(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.-,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/ASTM D 5708-15 D 5708-15 ,-()1 D 5708;,.().1 *1.1 ,-.1.2 A(7-11 18-22)-,.1 ASTM D02 ,D02.03 .1 2015.2015.1995.2012.D5708-12?1.DOI:10.1520/D5708-15.1ASTM D 5708-15 .1.3 (12 22)-,.1.4 ,.15.2.21.1.5,.1.5.1 .1.6 ,.,.2.2.1 ASTM:2 D 1193 D 1548 1(1997.)3 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM 3 .www.astm.org.2ASTM D 5708-15 D 4057 D 4177 D 5185 -(ICP-AES)D 6299 D 7260 ,-(ICP-AES)3.3.1 A 10 (,.)10%(/).,.3.2 1 20 (.).,.3ASTM D 5708-15 525C .(.),.-.4.4.1 Ni,V Fe ,D 1548,.4.2 .,.,.,.5.5.1 .,4ASTM D 5708-15 ,.4 ,.5.2 1/.5.3 ,II D 1193.6.6.1 .D 4057 D 4177.6.2 ,.,80C().A -7.7.1-4 ,DC.,.,BDH Ltd.,Poole,Dorset,U.K.,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.5ASTM D 5708-15 ,.7.2 (),.7.3 .0,5 3/,6.,5.7.4 ,.100.8.8.1 ,o-,-.().8.2 ,U.S.P.8.3 5 Viton,E.I.duPont de Nemours.6ASTM D 5708-15 100/.8.4 (QC),.QC ,19.9.9.1 .10%(/).9.2 ,.10%(/).9.3 10%(/).9.4 ,10/,.,(),10%(/).9.5 (QC)QC 7ASTM D 5708-15 10%(/).10.10.1 D 7260,ICP-AES.10.2 .10.3 ,(1),(2),(3)(),(4)(.10.4),(5)1 10,(6).1.1.,.A ,259,94;238,20 231,60;216,56 292,40;310,22 A Winge,R.K.,Fassel,V.A.,Peterson,V.J.,Floyd,M.A.,-:,Elsevier,NY,1985.10.4 ,.8ASTM D 5708-15 10.4.1 .,D 5185.10.5 .10.6 .10.6.1 ,.11.11.1 ,.11.2 .,5%,.11.3 ,.,.,.9ASTM D 5708-15 ().11.4 ,.11.5 .5%,.11.6 ,(1/).,.,.12.12.1.7.1 7.4.12.2 ().1.400,/,10ASTM D 5708-15 (.2),-250,1 .-.-().1.12.3 ,/400,.,.12.4 ,525C 25C 400.12.5 ().12.6 ().11ASTM D 5708-15 13.13.1 ,1000/.13.2 ,HNO3.16(0,060 1,5).1 25,4 37/8 98,4 11/2 38,1 5 127 2 50,8 61/2 165,1 31/16 77,8 .2.12ASTM D 5708-15 13.3 ,(1+1).13.4 ,(19+1)19 .13.5 ,H2SO4.14.(QC)14.1 (19+1).14.2 ,100/,.14.3 .14.4 ,.14.5 (QC).15 QC .15.15.1 ,0,0025 0,12 .10.0,5 H2SO4 .1 ,100.13ASTM D 5708-15 .,.15.2 ,.,.(1/.,.,20 10 ,).15.3 (.2).,().-(.1).()-.,-,.15.4 ,.15.3,.(,14ASTM D 5708-15 ).15.5 ,525C 25C.,.,.15.6 19 1+1 .15 30.15.7 10 .,.16.16.1.10.2 10.4.17.17.1.11.17.2 (.15.2),.18.18.1 15ASTM D 5708-15 :(/)=C F(1):-,/,F-.18.2 :(/)=(C V F)/W(2):-(,),/V-,F-,W-,.19.19.1 (QC)(9.5 14.5 ).19.1.1 QC/QA ,.19.1.2 QC/QA 1.20.20.1 16ASTM D 5708-15 .21.6 21.1 .,o-.,.,.().2.X=,/.,/,/50-500 A 0,07X0,88 0,02X1,1 10-100 A 0,01X1,3 0,02X1,2 1-10 A 0,22X0,30 0,23X0,67 6 -ASTM International RR:D02-1351.17ASTM D 5708-15 NIST SRM 1618,7 NIST RM 8505.7 21.1.1 ,.2 3 .3.(/)(/)1 10 50 100 500 A 2,2 4,0 17 1,5 3,2 19 A 0,20 1,6 4,0 0,32 2,2 5,0 A 0,22 0,44 0,23 1,08 21.1.2 ,.4 5 .21.2 ,NIST.V Ni 7 (NIST),100 Bureau Dr.,Stop 3460,Gaithersburg,MD 20899-3460.18ASTM D 5708-15 .Fe ,.4.X=,/.,/,/50-500 A 0,12X1,1 0,10X1,1 10-100 A 0,41X0,78 0,05X1,3 1-10 A 0,68X0,35 0,91X0,51 5.(/)(/)1 10 50 100 500 A 8,9 19 112 7,4 16 93 A 2,5 8,7 15 1,0 8,1 20 A 0,68 1,5 0,91 2,9 22.22.1 ;-,19ASTM D 5708-15 ()X1.X1.1 (QC).X1.2 QC(.D 6299 ASTM MNL 7).8 X1.3 ,QC ().(.D 6299 ASTM MNL 7).,().X1.4 ,QC ,.QC ,QC ,.QC ASTM .X1.5 ,QC,8 ASTM MNL 7,6-.,ASTM International,W.Conshohocken.20ASTM D 5708-15 .QC,.X1.6 QC .D 6299 ASTM NL 7.X2.D 5708 X2.1 ,.X2.2 ,.X2.3 ,ICP-AES,.,.X2.4 ,-.X2.5 .X2.6 .(21ASTM D 5708-15 ).X2.7 ().X2.8 .X2.9 ,.X2.10 .X2.11 30 .X2.12 ,.X2.13 (30 ).,5%,.X2.14 (60),.X2.15 ,.,100-1000 .,22ASTM D 5708-15 .X2.16 ,.,(.,).X2.17 ,.X2.18 ,.X2.19 ,.,10%.X2.20 ,%,.(),.X2.21 ,:X2.21.1 .23ASTM D 5708-15 X2.21.2 .X2.21.3 .X2.21.4 .X2.21.5 ,.X2.22 ,.,.,.D02.03 (D 5708-121),.(1 2015.)(1)12.3,.24ASTM D 5708-15 25ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.