ASTM_D_5742_-_95_2010_rus_scan.pdf

MEXTOCyAAPCTBEHHbI COBET no CTAHAAPTM3AUMN,METPONOrN CEPTONKALM(MrC)INTERSTATE COUNCIL FOR STANDARDIZATION,METROLOGY AND CERTIFICATION(ISC)FOCTMEXTOCyAAPCTBEHHbI33585-CTAHAAPT2015yrOJb AKTBMPOBAHHbICTaHAapTHbI MeToA onpegeneHaKTMBHOCT no 6yTaHyM3paHne onunanbHoeMocKBaGGnCTaH,AapTHOpM2016FOCT 33585-2015npeAncnoBneLenn,ocHoBHble npnHyunbi n ocHoBHo nopagok npoBegeHnA pa6ot no MexrocyAapctBeHHO cTaH-AapTn3aun ycTaHoBneHbi OCT 1.0-92 MexrocyAapcTBeHHaA ccTeMa cTaHgapTn3aunn.OcHOBHblenonokeHnA OCT 1.2-2009 MexrocyAapcTBeHHaA ccTeMa cTaHAapTn3aunn.CTaHAapTbi Mexrocy-AapcTBeHHble,npaBnna n pekoMeHAaunn no MexrocyAapcTBeHHo cTaHAapTn3aunn.paBnna pa3pa6oTkn,npHt,npMeHeHg,6HoBneH OTMeHbICBeAeHA o cTaHAapTe1 NOAFOTOBNEH eAepanLHbiM rocyAapcTBeHHLIM yHnTapHbIM npeAnpnATneM BcepoccnickniHayqHo-nccnegoBatenbckn nHctNtyT cTaHAaptn3aynn MatepnanoB n texHonoru(中厂YN BHM CMT)Ha ocHoBe co6cTBeHHoro ayteHt4Horo nepeBoga Ha pycckn 3biK ctaHgapta,yka3aHHoro B nyHKTe 52 BHECEH egepanbHbIM areHTCTBoM no TexHn4eckoMy perynnpoBaHnio n MeTponornn(PoccTaH-AapT)3 7IPMHAT MexrocyAapcTBeHHbIM CoBeToM no cTaHAaptn3aunn,MeTponornn u ceptn中nKaunn(npoToKon oT 27 oKT6p 2015r.Ne 81-)3a npnHaTe nporonocoBann:KpaTKoe HanMeHoBaHMe cTpaHbIKoA cTpaHblCokpaueHHoe HanMeHoBaHe HauMoHanbHoro opraHano MK(MCO 3166)004-97no MK(MCO 3166)004-97no cTaHapT3auBenapycbFoccTaHAapT Pecny6nnkn BenapycbKa3axcTaHKpr3826%occTaHAapT Pecny6nnkn Ka3axcTaHKbiprb3cTaHAapTPOCCHARUPoccTaHAapTTaAKnKcTaHTJTaAKnKcTaHAapT4 puka3oM PegepanbHoro areHTcTBa no TexHn4eckoMy perynnpoBaHnio n MeTponornn oT 17 MapTa2016 r.Ne 172-cT MexrocyAapcTBeHHbi cTaHAapt FOCT 33585-2015 BBeAeH B AectBMe B ka4ecTBeHaoHanbHoro cTaHAapTa Poccnnckon egepauun c 1 anpena 2017 r.5 HacToAwM cTaHAapt nAeHtn4eH cTaHAapty ASTM D 5742-95(Reapproved 2010)Standard TestMethod for Determination of Butane Activity of Activated Carbon(CTaHAapTHLIM MeToA onpeAeneHnA aKTuB-HOcTn no 6yTaHy aKTBpoBaHHoro yrng).CTaHAapt pa3pa6oTaH KoMnTeToM ASTM D28 AKTBnpoBaHHbin yronb,HenocpeAcTBeHHyOOTBeTCTBeHHOCTb 3a pa3pa6otky MeToga Hecet noAKoMnTeT D28.04 MeTobi aHann3a ra3oBo pa3bi.epeBog c aHrnckoro 3bika(en).HanMeHoBaHne Hactowero cTaHAapTa 3MeHeHO OTHOCnTenbHO HanMeHoBaHnA yKa3aHHoro cTaH-Aapta An npuBeAeHn B cooTBeTctBue c OCT 1.5-2001(noApa3gen 3.6).OnynanbHble 3K3eMnngpbi cTaHgapta ASTM,Ha ocHoBe kotoporo nogrotoBneH hactogw Mexrocy-gapctBeHhbi ctaHgapt,u ctahgaptoB ASTM,Ha KoTopbie gaHbi ccbinkn,MelotcAB egepanbHoM nHPOpMa-LOHHOM oHAe TexHnecknx pernaMeHTOB cTaHAapToB.CBeAeHA o cooTBeTcTBnn MexrocygapcTBeHHbIX cTaHAapTOB cCbIno4HbIM cTaHgapTaM npnBeAeHbIB AononHTenbHoM nnoeH A.CTeneHb cooTBeTctBn-AeHtnHag(IDT)6 BBEAEHBNEPBbIEFOCT33585-2015MHpopMauu o6 u3MeHeHuAX K HacmouweMy cmaHdapmy ny6nukyemc e exe2odHOM uHopMauuoH-HoM yKa3amene HaquoHanLHbie cmaHdapmbi,a meKcm u3MeHeHuuu nonpaeok eexeMecAHoM uHpop-MaquOHHOM yKa3amene HaquoHanLHLie cmaHdapmbi.B cnyuae nepecMompa(3aMeHLi)unu omMeHbiHacmouwe2o cmaHdapma coomeemcmeyiowee yeedoMneHue 6ydem ony6nukoeaHo e exeMecA4HOMuHpopMayuOHHOM yKa3amene HauoHanLHbIe cmaHapmbi.CoomeemcmeyioaR uHpopMayuA,yee-domneHue u mekcmbi pa3Mewaiomca makke e uHpopMayuOHHou cucmeMe o6we2o non3oaHuR Ha opu-quanLHoM caume PedepanLHo2o a2eHmcmea no mexHu4eckoMy pe2ynupoeaHuio u Memponozuu e cemuHmepHemCTaHAapTHopM,2016B Poccnicko egepaynn hacto ctaHAapt he moxet 6bitb noNhoctbio unn yactn4ho Bocnpon3Be-AeH,TpaxnpoBaH n pacnpocTpaHeH B ka4ecTBe onnanbHoro n3gaHnA 6e3 pa3peweHnA eAepanbHoroareHTcTBa no TexHneckoMy perynupoBaHno n MeTponornFOCT 33585-2015ME KOC yAAPCTBEH HbIMC TAHAPTyrOnb AKTMBMPOBAHHbIMCTaHAapTHLI MetoA onpeAeneHA aKtBHoct no 6yTaHyActivated carbon.Standard test method for determination of butane activityAaTa BBeAeH-2017-04-011 06nacTb npMeHeHA1.1 Hactogwnn ctaHAapt yctaHaBnnBaet MeTog onpegeneHng ypoBHA aKtuBHOCt aKTBnpoBaHHoToyrng.AKtuBHoctb no 6yTaHy(BA)onpegengot kaK oTHoweHne(B npoLeHTax)Maccbi 6yTaHa,agcop6npoBaH-Horo npo6o aktnBnpoBaHHoro yrng,k Macce npo6bl yrng,HacbieHHoro 6yTaHoM,B ycnoBngx,ycTaHoB-neHHbIX HacToM cTaHAapTOM.1.2 B HacToAweM cTaHgapte Bce eAHLbI n3MepeHnA npBegeHbi B cncTeMe C.HnKakne ApyrneeAHbI 3MepeHn B HacTo cTaHAapT He BKno4eHbI.1.3 B HacTogeM cTaHgapTe He npeAycMoTpeHO paccMoTpeHMe Bcex BonpocoB o6ecne4eHng 6e30-nacHOCT,cBA3aHHbIX c ero cnonb3oBaHeM.onb3oBaTenb cTaHgapTa Hecet oTBeTCTBeHHOCTb 3a o6ecne-eHMe cOoTBeTCTByIouX Mep 6e3onacHOCT OXpaHbI 3AOpoBbA onpegengeT Lenecoo6pa3HOcTbnpMeHeHnA 3aKoHogaTenbHbiX orpaHn4eHn nepeA ero ucnonb3oBaHeM.Mepbi npeAocTopOxHOCTnpBegeHbi B 7.1.2 HopMaTBHble ccbInKnAng npuMeHeHng Hactogwero ctaHAapta Heo6xognMbi cnegyiowne ccbino4hble AokyMeHtbi.Ang HeAa-ThpoBaHHbIX ccbinoK npnMeHgioT nocneqHee n3aHne ccbino4Horo gokyMeHta(Bknio4ag Bce ero n3MeHeHng).2.1 CTaHAapTbI ASTM1)ASTM D 2652 Terminology Relating to Activated Carbon(TepMHonorng,oTHocwagcA K aKtnBn-poBaHHOMy yrno)ASTM D 2854 Test Method for Apparent Density of Activated Carbon(MeToA onpegeneHnA HacLinHoinnoTHocT aKTBpoBaHHoro yrng)ASTM D 2867 Test Methods for Moisture in Activated Carbon(MeToAbi onpegeneHnA Bnarn B akTn-BupoBaHHoM yrne)ASTM D 3195 Practice for Rotameter Calibration(ApaKTuka no kanu6poBke poTaMeTpoB)ASTM D 3467 Test Method for Carbon TetrachlorideActivity ofActivated Carbon(MeToAonpegeneHnaKTBHoCT aKTBpoBaHHoro yrng no yeTbipexxnopucToMy yrnepogy)ASTM E 177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods(pakrukaucnonb30Bahug tepMnHoB npeyn3nOHHoctn n otKnoHeHng B meTogax ucnbitahn no ASTM)ASTM E 300 Practice for Sampling Industrial Chemicals(ApaKTnKa oT6opa npo6 npoMbIneHHbIXXMeckX npoAyKTOB)ASTM E 691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a TestMethod(门paktuka npoBegeHng mexna6opaTopHbix cnbitaHun Ang onpegeneHnA npen3OHHOCT MeToAacnbitaH)1)YTo4HNTb cCInkn Ha cTaHAaptbi ASTM MoHo Ha caite ASTM:www.astm.org unn B cnyx6e noggepxkn knneH-ToB ASTM:serviceastm.org.B nHpopMauoHHoM ToMe exerogHoro c6opHnKa cTaHgapToB(Annual Book of ASTMStandards)cneAyer o6paw,aTbca k cBogke cTaHgapToB exeroAHoro c6opHnKa cTaHAapToB Ha cTpaHne cavTa.M3aHne onunanbHoeOCT 33585-20153 TepMHbI onpegeneH3.1 OnpegeneHna TepMnHoB,cnonb3yeMbIx B Hactowem ctaHgapte,npBeAeHbi B ASTM D 2652.4 CyHOCTb MeToga4.1 Cnon aKTBnpoBaHHoro yrnA n3BecTHoro o6beMa n Maccbi HacbiuaoT napaMn 6yTaHa.Maccyancop6npoBaHHoro 6yTaHa B cocTogHn HacbieHMg 3anncbiBaoT u npeAcTaBngioT kaK Maccy 6yTaHa HaeHuy Maccbl yrng.5 3HaeHne n npnMeHeHne5.1 AKTBHOCtb no 6yTaHy,3MepeHHag B cooTBeTCTBn c HacTouM cTaHAaptoM,ABngetcA noka-3aTeneM,xapaKTepn3youM cnoco6HOCTb aKTBMpoBaHHoro yrng agcoppoBaTb 6yTaH 3 cyxoro Bo3pyxaB onpegeneHHbIx ycnoBx.loka3aTen cnonb3yoT np KOHTpone Ka4ecTBa n oueHke rpaHynpoBaHHbIXaKTBpoBaHHbIx yrnen.AKTBHocTb no 6yTaHy-3To noka3aTenb o6beMa MKponop npo6bi aKTnBnpoBaHHO-To yrng.3HayeHe aktBHoct no 6yTaHy He Bcerga ABngeTcA a6conoTHbIM n oTHOCnTenbHbIM noka3aTe-neM 3peKTBHOcT McnbiTaHHoro yrng no OTHoweHMo K ApyrnM agcoponpyeMbIM BewecTBaM nnM npApyrnx ycnoBnx npoBeAeHng cnbiTaHn.5.2 HacToAn MeTog onpegeneHnA aKTuBHOCt no 6yTaHy MoeT 6bITL Cnonb3oBaH B KayecTBe3aMeHb MeToga onpegeneHng aKTBHOCtn no 4eTbipexxnopucToMy yrnepogy no ASTM D 3467,He npBog-山en k pa3pyweHno o3oHoBoro cnog.Ha pcyHke 1 noKa3aHa Koppenu 3Ha4eHn aKTBHOcT,nonyeHHbIX3KcnepMeHTanbHo c cnonb3oBaHeM 3Tx AByx acoponpyeMbix BeecTB.p u Me 4 a H ne 1-Hactoun MeToA He npeAHa3Ha4eH Ang ucnLITaHnA nopowkoo6pa3Horo aKTuBpoBaH-Horo yrng,ogHako oH MokeT 6bITb ycnewiHo npnMeHeH B cny4agx,Korga Ang coxpaHeHng nepena,pa gaBneHng Ha npeM-neMOM yPoBHe 3MeHgoT cKopoctb notoKa n BpeMg nn yMeHbwaot o6bem npo6bl.140-口120-口00回口口o0005201500500五6roEn5o1msLd口520110000505上四-OO308二回80口旦。一。二口口口回AKTBHOCTL no CCl4=a.AKTBHOCTL no 6yTaHy20-onHa oppenu a=2,55;R=0,935175 akcnepMeHTanbHbIX To4eK0-102030405060AKTMBHOCTb no 6yTaHy(r 6yTaHa/100 r aKTMBMpoBaHHoro yrng)PucyHoK 1-Koppengyu 3Ha4eHn aKTnBHoCTn aKTnBnpoBaHHoro yrn no 6yTaHy n eTLipexxnopncToMy yrnepopy2