ASTM_D_5453_-_19a_rus.pdf

D5453-19a ,-STANDARD TEST METHOD FOR DETERMINATION OF TOTAL SULFUR IN LIGHT HYDROCARBONS,SPARK IGNITION ENGINE FUEL,DIESEL ENGINE FUEL,AND ENGINE OIL BY ULTRAVIOLET FLUORESCENCE 2020 ():31.01.2020:3826-20/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D5453-19a 1 D5453-19a ,-1 D5453;,.().1.*1.1 25 C 400 C 0,2 c 20 c(2/).1.2 (ILS),ASTM,1 ASTM D02 ,D02.03 .1 2019.2019.1993.2019.D5453-19.DOI:10.1520/D5453-19.*ASTM D5453-19a 2 ,(FAME),(,-85,M-85,RFG),/.,1,0/8000/(.1).1 (PLOQ).,1,0/5,0/(.9 16.1).1.3,.1.4 ,.,.3.1,7.3,7.4,8 9.1.1.5 -,(TT).ASTM D5453-19a 3 2.2.1 ASTM:2 D1250 D1298 ,API D4052 ,API()D4057 D4177 D6299 3.3.1 ,(SO2).,(UV).SO2 (SO2*).,SO2*SO2,.(UV).2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM ASTM D5453-19a 4 ,).4.4.1 ,.,.5.5.1 0,35%().5.2 (NO),.A1 ,.6.6.1 ,(1050 C 1150 C),SO2.6.2 ASTM D5453-19a 5 ,.-.(.1).1 .,.1 6.3 ,-.6.4 -ASTM D5453-19a 6 .,.,.6.5 ,.6.6 5 90 .6.7 .6.7.1 ,.,1/.,.2.6.7.2 -.().ASTM D5453-19a 7 ,.,.3.2 6.8 ,4 C .6.9 ,().6.10,0,01 ().-ASTM D5453-19a 8 .3 7.7.1 .,.3 ,.7.2-.3 ,DC.,.Analar Standards for Laboratory Chemicals,BDH Ltd.,Poole,Dorset,United States Pharmacopeia and National Formulary,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.-ASTM D5453-19a 9 .7.2.1 ,(.),99,998%,5/.7.2.2 (.,),99,99%,5/.7.3 ()(.,),99,75%,5 ,.().7.4,(,).,(),.,.().7.5,FW184.26,17,399%(/)S(.2).7.6 ,FW146.29,21,92%(/)S(.2).7.7 (),FW134.20,23,90%(/)S(.2).2 ,.7.8 ,(.3)3 7.8 ASTM D5453-19a 10 .7.9 ,1000 S/0,5748 0,4562 0,4184 100.(.4 7).4 .5 ,.3.6 ,.7 ,.7.10 (QC),.QC ,15.7.11 ()(WO3),(2,0),99,75%.ASTM D5453-19a 11 8.8.1 ,.9.9.1 D4057 D4177.,.,.(,.,).9.2 ,.10.10.1 ,.10.2 ,.1.ASTM D5453-19a 12 1.()(700 750)1/()(700 750)140 160/1075C 25C (3,8 4,1)450 500/(0,4 0,8)10 30/-(3,4 3,6)130 160/10.3 ,.11.11.1 ,.2.,.,.,.,.11.2 .11.3 ,.2 (.8-10).ASTM D5453-19a 13 2.I ,/II ,/III ,/0,50 5,00 100,00 1,00 25,00 500,00 2,50 50,00 1000,00 5,00 100,00 10,00 10 20 5 10 5 8 ,.9 10 100/1000 1,0.10 ,/.11.3.1 .,10%,.,10%,.(.11).11 .11.3.2 11.3.1.,ASTM D5453-19a 14 0,01.11.4 .:11.4.1 .().11.4.2 ,(.7.8),.(.12).1 (.12).12 .,.11.4.3 .ASTM D5453-19a 15 ,.11.5 :11.5.1 ,11.2 11.4.,(.7.4).(y),().(.13).,(.15).13 ,.11.5.2 ,11.2 11.4.(,.7.4 11.5.1),(.13).,(.15).11.6 ,.2,().,ASTM D5453-19a 16 ().12.12.1 ,9.,.12.1.1 (/).12.1.2 (/).12.2 ,11.2 11.4.12.3 .12.3.1 ,.12.3.2 .,.12.3.3 ,.ASTM D5453-19a 17 12.4 .12.5 ,(/)D1298,D4052 ,.14 13.1.14 (.16.1)(/),:.12.5.1 ,D1298 D4052,(.15).15 D1250 ,.13.13.1 /:(/)=MdVd(1):Md-(0,01),Vd-(A).13.2 ,(ppm):ASTM D5453-19a 18 =/)(ppm,gKMSYI)(2)=/)(ppm,vKVSYI)1000)(3):D-,/,I-,Kg-,/,/,Kv-,/,/,M-,V D,S-,/S,V-,M/D,Y-y,1000-.13.3 ,(ppm):=/)(ppm,gKMG1000(4)ASTM D5453-19a 19 =/)(ppm,DVG1000(5):D-,/(),/(),Kg-,/,/,M-,V D,V-,M/D,G-,1000-.14.14.1 ,10/,1/.,10/,0,1/.,(.5.2).,D5453.15.15.1 (QC)(7.10)(.11.5).ASTM D5453-19a 20 15.1.1 /(QC/QA),.15.1.2 /(QC/QA),1.16.16.1 4.(1)RR:D02-1307(1992.),(2)RR:D02-1456(1992.),(3)RR:D02-1465(1997.)RFG,(4)RR:D02-1475(1998.),(5)RR:D02-1547(2000-2001.)39 16,(1/S 100/S)(5/S 40/S),(PLOQ),(6)RR:D02-1633(2008.).16.1.1 ,(.16):4 -ASTM International ,16.1.ASTM :serviceastm.org.ASTM D5453-19a 21 16 (.9 11.4).16.1.2 ,20,x=.400/:r=0,1788 X(0,75)(6)400/:r=0,02902 X(7)16.1.3 ,20,x=.400/:R=0,5797 X(0,75)(8)400/:R=0,1267 X(9)16.2 (RR:D02-1307)4 1992.(SRMs),.16.2.1 (SRMs),(NIST).:SRMs 2298(4,7/1,3/S)SRMs 2299(13,6/1,5/S),ASTM D5453-19a 22 SRM 2723a(11,0/1,1/S).,ILS ARV()NIST 95%.4.RR:D02-1547(2000-2001.).4 16.3 400/.3.3.(r)(R)(/)r R 1 0,2 0,6 5 0,6 1,9 10 1,0 3,3 50 3,4 10,9 100 5,7 18,3 400 16,0 51,9 4.NIST ASTM(RR)SRM NIST /NIST /ASTM ILS ,/(95%)?NIST 2298 4,7(1,3)3,6(0,19)1,1 NIST 2299 13,6(1,5)11,6(0,52)2,0 NIST 2723a 11,0(1,1)10,2(0,44)0,8 17.17.1;-85;M-85;RFG;.ASTM D5453-19a 23 ()A1.(S),(N),(S),.(NO)()/,.(N),.,.,.N S .,10/,300/,.A1.1 ,A1.1 .ASTM D5453-19a 24 A1.1.1,/D5453.A1.2 (STM)1 5(,10/).A1.1(),/1 10 2 10 10 3 100 10 4 200 10 5 300 10 A1.2.1 D5453 /1 16;(,10/,r=1.0/).A1.2 r,13/=1,2/D5453 12,6 13 10 13,3 13 100 13,0 13 200 13,3 13 300 13,0 13 A1.3 r,10/=1,0/D5453 10,1 10 10 10,3 10 100 11,0 11 200 11,9 12 300 12,5 13 ASTM D5453-19a 25 A1.3 ,A1.2.1 1(1/1).A1.4 A1.2 ,A1.3 ()=10/,100/.A1.5 .,(),14.ASTM D5453-19a 26 ()X1.X1.1 (QC).X1.2 QC(.D6299 MNL 7).5 X1.3