ASTM_D_6299_-_18_rus.pdf

:D:D62996299-1818 STANDARD PRACTICE FOR APPLYING STATISTICAL QUALITY ASSURANCE AND CONTROL CHARTING TECHNIQUES TO EVALUATE ANALYTICAL MEASUREMENT SYSTEM PERFORMANCE 2012018 8 ():16.10.2018:3557-18/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D6299-18 1 :D6299:D6299-1818 1 D6299;,.().1.1.*1.1 ,(SQC).1 ,.,:(1),(2),(3)1 ASTM D02 ,D02.94 .1 2018.2018.1998.2017.D6299-17b.DOI:10.1520/D6299-18.ASTM D6299-18 2 ,(4),(5),.1.2 ,.1.3 .1.4 .1.5 ,D6708 .2 .D3764.3 1.5 .1.6 ,(),.4 .1.7 -,(TBT).ASTM D6299-18 3 2.2.2.1 ASTM:2 D3764 D4175 ,D5191 (-)D6300 D6708 ,D6792 ,D7372 E177 ASTM E178 E456,E691 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D6299-18 4 3.3.3.1:3.1.1 D4175,D6300,E456.3.1.2 ,.D6300 3.1.3 (R),5%(,20).D6300 3.1.4 ,.3.1.4.1 ,.D6300 3.2 ,:3.2.1 D4175,D6300,E456.3.2.2 ,ASTM D6299-18 5 ,(1),(2),(NIST),(3),.3.2.3 .3.2.4 ,.3.2.4.1 (,ASTM,ISO).3.2.4.2 ,.3.2.5 ,.3.2.6 ,.3.2.7 (QC)ASTM D6299-18 6 .3.2.8 QC,.3.2.8.1 ,.,.,.3.2.9 (,),.3.2.10 ,.3.2.11 QC ,QC .3.2.12 ,ASTM D6299-18 7 ,.3.2.13 ,.3.2.14 ,.3.2.14.1 ,.3.2.15 ,.3.2.16 .3.2.16.1 ASTM D02 ,.3.2.17 (QC),.ASTM D6299-18 8 .3.2.18 (SEV)QC,.3.2.18.1 SEV ;,SEV,QC.3.2.19 (R),0,95(95%),.2,77 R,.3.2.20 ,15.3.2.20.1 ,.,ASTM D6299-18 9,.,QC 24-,4 8,/,.3.2.21 ,.3.2.22 QC ,.3.3:3.3.1 ARV .3.3.2 EWMA .3.3.3 I (I-).3.3.4 MR .3.3.5 MR .3.3.6 QC .3.3.7 R .3.3.8 SEV .3.3.9 R .3.3.10 VA .3.3.11 2 -.3.3.12 .ASTM D6299-18 10 4 4 4.1 QC .,.4.2 .4.3 ,QC ,.5 5 5.1 ,.5.2,.5.3 ,.ASTM D6299-18 11 6.6.6.1 QC .6.1.1 ,.5 QC ,QC.6.1.2 ,QC,(1),(,)(2)QC .6.1.3 .6.1.4 .6.1.5 ,QC ,.6.1.6 QC,.,6.1.3,.(ASTM D6299-18 12 ,.,.,.,.)6.2 .6.2.1 ,.6 .6.2.2 ,.(ARV).3 6.2.2.1 ,.,3 ,.RR:D02-1007,E178 E691,ASTM ,ASTM International,1997.ASTM D6299-18 13 .F-.7 (ARV).,16 ARV ARV 4 .,ARV .16,.8 ,ASTM D02.CS92 ILCP;ASTM D02.01 N.E.G;ASTM D02.01.A;,Alberta Research Council.6.2.3 ,.,2,2-D5191.,.6.3 (VA)QC ,.ASTM D6299-18 14 7.(QA)7.1 (1)4 (QA):(1)QC,(2),(3),(4),(5)(VA),.QA ,(.7.1.1).7.1.1 ,.,QC.9 ,.D6792.10 (PT),.D7372.7.2 QC QC,.7.3 :4 .ASTM D6299-18 15 7.3.1 .7.4/:7.4.1 QC .11 ,.,.7.4.2 QC ,.,(1),(2),(3),(4),(5),.12 QC.,(.7.2),(.7.3).,QC.(.7.3),QC(.7.2).7.4.3 QC .7.4.4 ,ASTM D6299-18 16 .7.4.5 QC ,.7.4.6 ,QC ,.13 QC,.7.5 :7.5.1 ,QC .7.5.2 ,.7.6 :7.6.1 ,(ASTM),.,ASTM D6299-18 17 .7.6.2 (),.7.7 (VA).,VA,QA.14 ,(QC ),.,QA VA.7.7.1 (VA),.7.7.1.1 QC ,ASTM D6299-18 18 .7.7.1.2 QC ,.,.7.7.1.3 .,ARV.,.8.,8.1 ,QC,.,:8.1.1 ().8.1.2 ,(,).8.1.3,.8.1.4 ASTM D6299-18 19 .15 ,9,.8.2 ,QC ,.8.2.1 QC ,QC .8.2.2 ,.8.2.2.1 1 (1),ARV,(2),ARV:=(ARV)()(1)8.2.2.2 2 ,ARV,=ARV /(ARV)2+(ARV)2 (2)ARV ,ARV,;ASTM D6299-18 20 ARV ARV.,ARV ,ARV .(.16.)8.2.2.3 ARV ,ARV .16 ARV .8.2.3 VA ,8.2.1 8.2.2.8.3 (1,2)(I),(MR),1()(3),2(EWMA)(4,5,6)(.A1)()QC ,(b)(7),.I ,QC.1()2(EWMA).MR .17 ,ASTM D6299-18 21 ,.,.8.3.1 :1 (QC),QC,QC .2 (QC),1;,1,.1 8.4 ,(.19).20 .,(1.4).18 ,.19 1,8.7.2.3 8.7.3(Q-),.ASTM D6299-18 22 8.4.1 ,.,.15,.8.4.2 ,.(.1.3).,.8.4.3 ,.-(Anderson-Darling)(.1.4).(.A1.4),ASTM D6299-18 23 1.3.2.6,2.20 ,.8.4.4 ,.8.4.4.1 MR .MR ,MR MR.8.4.4.2 I I.8.4.4.3 EWMA EWMA I.EWMA I.2 8.4.5 .8.5 :8.5.1 (.1.5),().8.5.2 ,ASTM D6299-18 24 .21 ,.8.6 1 :8.6.1 1 (1)QC,;(2).8.6.2 20 F-(.1.8),.F-,100 ,.8.6.3 F-,100 ,.8.6.4 F-,.,.8.7 2 :ASTM D6299-18 25 8.7.1 2 QC,QC,QC.QC .I ,QC ,.8.7.2 1,:8.7.2.1 QC,20.8.7.2.2 QC.,QC .8.7.2.3 ,QC,MR .,I ,MR .MR,.ASTM D6299-18 26 8.7.2.4 20 ,F-,.F-,100 ,.8.7.2.5 F-,100 ,.8.7.2.6 F-,.,.8.7.2.7 I MR (EWMA 2),8,MR.8.7.2.8 I MR QC.8.7.3 2,Q-(.1.9)(8):8.7.3.1 .,QC .ASTM D6299-18 27 22 ,50 .8.7.3.2 Q-(),MR,QA .8.7.3.3 Q-I,20 (Q-),8.7.2,20 ,QC,Q-MR ,QC.8.7.3.4 Q-QC,.8.7.3.5 Q-MR-1 2 8.2.1 ;2 1,2 .8.8 Q-(8.7.3),QC (20)QC,ASTM D6299-18 28 .QC ,Q-MR,.8.9 Q-(8.7.3),.,Q-MR,.,.,.Q-,.ASTM D6299-18 29 9.9.1 ,QC:9.1.1 ,QC,(rms)(R).RiinIIn()=211 (3)R=2,77R (4)9.1.1.1 ,(.A1.4)R 2,46 (MR)MR .R=2,46 MR (5)23 (R)MR R/2,77=(MR)/1,128.9.1.1.2 (R),.,.,(2R),.1,414 ASTM D6299-18 30 (R).=(6)()-2 R=()1,414 (7)9.1.2 R ,.,R .2 1.7.9.2 15 ,I.t-(.1.6).9.2.1 t-,.9.2.2 t-,.,.9.3 ,.ASTM D6299-18 31 9.3.1 8 ARV.,.9.3.2 ,t-9.2 ,I,.9.3.2.1 t-,.9.3.2.2 t-,./.9.3.3 9.3.1 ,./.9.3.4 9.3.2.2 ,9.3.3 ,.9.3.4.1 ,D6708 .ASTM D6299-18 32 10.VA 10.1 VA QA,VA.,9,.10.2 VA ,.,.10.3 ,VA,.10.4 F-t-,(.1.8 1.6),VA,.10.5 ,.9 .AS