ASTM_D_5917_-_12_rus.pdf

56343 2015 2015 563432015 II 1 -(),4 2 160 3 10 2015.70-4 591712 -(ASTM D 591712 Standard test method for trace impurities in monocyclic aro-matic hydrocarbons by gas chromatography and external calibration).-1.52012(3.5).-,5 1.02012(8).(1 ),-.()-.,(gost.ru),2015 ,-563432015 1 Monocyclic aromatic hydrocarbons.Determination of trace Impurities by gas chromatography test method using the external calibration 20160101 1 1.1 :,-(-).,-.2360 -.1.2 -,1 10 (),0,001%.2,500%.1.2.1 -(.6.1).1.3 -,6 10 (-10),0,001%.1,000%.1.4 E29.1.5 .1.6 -,.-.9.2 :2.1 1)841 (ASTM D 841,Specification for nitration grade toluene)2360 -(ASTM D 2360,Test method for trace impurities in monocyclic aromatic hydrocarbons by gas chromatography)3437 (ASTM D 3437,Practice for sampling and handling liquid cyclic products)4052 ,AP I (ASTM D 4052,Test method for density,relative density,and API gravity of liquids by digital density meter)1)ACTM ATM,www.astm.org -ATM:serviceastm.org.(Annual Book of ASTM Standards).563432015 2 4307 -(ASTM D 4307,Practice for preparation of liquid blends for use as analytical stan-dards)4790 -(ASTM D 4790,Terminology of aromatic hydrocarbons and related chemicals)5136 -(ASTM D 5136,Specification for high-purity p-xylene)5211 -(ASTM D 5211,Spe-cification for xylenes for p-xylene feedstock)6526 (ASTM D 6526,Test method for analysis of toluene by capillary column gas chromatography)6563 ,(BTX)(ASTM D 6563,Test method for benzene,toluene,xylene(BTX)concentrates analysis by gas chromatography)6809 -(ASTM D 6809,Guide for quality control and quality assurance procedures for aromatic hydrocarbons and related materials)E29 (ASTM E 29,Practice for using significant digits in test data to determine conformance with specifications)E260 (ASTM E260,Practice for-packed column gas chromatography)E355 (ASTM E355,Practice for gas chromatography terms and relationships)E691 -(ASTM E691,Practice for conducting an interlaboratory study to determine the precision of a test method)E1510 (ASTM E1510,Practice for installing fused silica open tubular capillary columns in gas chromatographs)2.2 OSHA,29 (),1910.1000 1910.1200(OSHA Regulations,29 CFR paragraphs 1910.1000 and 1910.12001).3 3.1 4790.3.2 C8,-,-.-,.4 ,-(FID).-.(GC),100,00 .5 5.1 ,-,-.-,.,1 10 ,.1),732 N.Capitol St.,NW,Mail Stop:SDE,Washington,DC 20401,http:/www.access.gpo.gov.563432015 3 5.2 100,00.,.5.3 2360,-.6 6.1 -.-6526.6.2 -,50%.7 7.1 ,-,-,1.-0,001%.-.1 ,C 270:,:,C ,/,C ,-:,/,145 ,:,C 60 0,32 0,25 60 10 5 150 10 20 45 100:1 1,0-300 30 7.2 .-,.-,1,.7.3 .7.4 .-,-12.7.563432015 4 7.5 100 3.7.6 100.8 8.1 .,-1).8.2-99,999%.-,.-.8.3 0,1 p pm.8.4-99,999%.8.4.1 -99,9%,-.1,9 3-3,8 3-(105)C ,1/2 3/4 -.5.-.-.8.5 :-,-,-.-(PDEB).99%.99%.,-.9 9.1 ,.10 10.1 3437.11 11.1 ,-,1,-.-E260,E355 E1510.12 12.1 -,.1;-.2 .-,-,-1)Reagent Chemicals,American Chemical Society Specificatios,American Chemical Society,Washigton,D.C.(.,).,.Analar Snandards for Laboratory Chemicals,BDHL td.,Poole,Dorset,U.K.(),the United States Pharma copeia and National Formulary,U.S.Pharma copeial Convention,Inc.(USPC),Rockville,MD.().563432015 5 (PDEB).PDEB ,PDEB.2 ),(PDEB)(PDEB)%.%.%.%.-PDEB 0,861 0,879 0,867 0,867 0,880 0,862 0,718 0,864 0,866 99,6099,62 20 20 100 100 20 20 100 20 99,60 0,020 0,020 0,100 0,100 0,020 0,020 0,100 0,020 99,60 0,020 0,020 0,100 0,102 0,020 0,017 0,101 0,020 99,62 0,020 0,020 0,100 0,100 0,020 0,020 0,100 99,62 0,020 0,020 0,100 0,102 0,020 0,017 0,101 )20 C.ASTM D S4A 110.,1971.12.1.1 -,-20.12.2 Ci ,2,Ci=100DiVi/VtDp,(1)Di i-2;Vi i-,;Vt ,;Dp-2.12.2.1 ,4307.12.3 ,12.1,.1.563432015 6 1 ;2 ;3 ;4 ;5 -;6 -;7 ();8 -;9-1 12.4 i-RFi=Ci/Ai,(2)Ci i-;12.2,%.;Ai i-.12.5 -RF.12.6 RF .CVi RF CVi=100SDi/Agi,(3)SDi RFi;Agi RF i-.12.7 ,-,-10%.13 13.1 -,20.,12.13.2 ,-.12.3 -12.7.563432015 7 14 14.1 ,().-,-,-,-(-1).C9+,-,.-C9+,-(.-1),.C9+,C9+C9+,.14.2 ,-,-.14.3 2 841,3 -5211,4-5136.1 ;2 ;3 ;4 ;5 -;6 -;7 ();8 -;9-2 841 563432015 8 1 ;2 ;3 ;4 ;5 -;6 -;7 ();8 -;9 C9+;10 -3 5211 1 ,2 ,3 ,4 ,5 -,6 -,7 (),8 -,9 C9-,10 -4 -5136 14.4 Ci ,.-,-,-,-,563432015 9 ,-(PDEB).PDEB ,PDEB,Ci=AiRFiDc/Ds,(4)Ai i-;RFi i-12.4;Dc (-)2;Ds 2 4052.14.5 ,%,=100,00 Ct,(5)Ct ,%.14.5.1 ,-,.-100().-6563.15 15.1 ,C9+0,001%.15.2 0,001.,0,001.0,000.15.3 0,01%.15.4 -GC 0,01%.16 1)16.1 95%,-,.-,6.2 -.-51.-691.-,.16.1.1 3 ,-.3 (0,017)(0,017)-(0,009)-(0,013)-(0,001)(99,94)0,0040 0,0014 0,0025 0,0013 0,0003 0,0160 0,0083 0,0030 0,0027 0,0025 0,0005 0,0210 1)-ASTM International RR:D16-1020.563432015 10 3 (2,286)(0,675)(0,010)(96,93)0,1039 0,0244 0,0006 0,1280 0,3688 0,1580 0,0020 0,3690-(0,014)(0,006)(0,076)-(99,694)-(0,142)-(0,055)-(0,004)0,0052 0,0014 0,0024 0,0100 0,0038 0,0016 0,0008 16.2 ,-,3.16.3 ,3.16.4 -,.17 17.1 6809 QA/QC,-.-QA/QC,6809.563432015 11 ()().1 -84113 *236011 *343711 *405211 *430799(2010)*479011 *513609(2013)*521112 *652612 *656312 *680902(2012)*E 2913 *E26096(2011)*E35596(2007)*E 6913 *E 151095(2013)*.563432015 547.53:543.064:543.544.32:006.354 71.080 2409 :,-,02.03.2015.60 x841/8.1,86.31.1113.,123995,.,4.www.gostinfo.ru infogosti