ASTM_D_5985_-_08_rus_scan.pdf

MEXTOCyAAPCTBEHHbM COBET No CTAHAAPTN3ALN,METPONOrnN CEPTONKALN(MrC)INTERSTATE COUNCIL FOR STANDARDIZATION,METROLOGY AND CERTIFICATION(ISC)FOCTMEKOCYAAPCTBEHH bICTAHAAPT32393-2013HETENPOAKTbIOnpegeneHne TeMnepatypbi 3acTbIBaHg MeToAOMBpaweHgM3aHne onunanbHOeMocKBaGKCTaHAapTMHOPM2014FOCT 32393-2013npencnoBneLenn,ocHoBHbie npHynti n nopaAok npoBeAeHn paoT no MexrocyAapcTBeHHo cTaHAapTn3a-MM ycTaHoBneHbi OCT 1.0-92 MexrocyAapCTBeHHaR cucTeMa cTaHAapTn3aunn.OCHOBHble nonoxe-H OCT 1.2-2009 MexrocyAapcTBeHHa cncTeMa cTaHAapTn3ayn.CTaHAapTbi MexrocyAapcTBeH-Hble,npaBnna n peomeHgaynn no mexrocygapcTBeHHon cTaHAaprn3ayn.paBnna pa3pa6orkn,npnH-T,nMeHeH,HoBneH OTMeHbICBeeHnA o cTaHAapTe1 NOATOTOBNEH 中eAepanLHbiM rocyAapCTBeHHLIM yHNTapHbIm npeAnpnATnem BcepoccncKnHayHO-nccneAoBaTenbcKn eHTP cTaHAapTn3au,nHopMau n cepTOnKaun cbipbA,MaTepnanoB nBe山(eCTB(中Y门 BHIL(CMB)Ha ocHOBe co6CTBeHHorO ayTeHT4Horo nepeBoga Ha pyccKn A3bIK cTaH-AapTa,yka3aHHoro B nyHkTe 42 BHECEH 中egepanbHbiM areHTCTBoM no TexHn4eckoMy perynnpoBaHnIo n MeTponornn3 NPNHAT MexrocyAapcTBeHHLIM coBeToM no cTaHgaptn3aynn,MeTponornn n cepru中nKaynn(npoTokon Ne 44-2013 oT 14 Ho6p 2013 r.)3a npHATe nporonocoBan:KpaTkoe HanMeHoBaHne cTpaHbI noKoA cTpaHbI noCokpaeHHoe HanMeHoBaHne HauoHanb-MK(MCO 3166)004-97MK(MCO3166)004-97Horo opraHa no cTaHAapT3anApMeHAAMMH3KOHOMKn Pecny6nKn ApMeHAKnpr3KGKbiprbi3cTaHAapTPOCCHARUPoccTaHAapTTaAnKcTaHTJTaAnKCTaHAapTy36eKncTaHUZy3cTaHAapT4 HacTou craHAapt nAeHTn4eH craHAapry ASTM D 5985-08 Standard test method for pourpoint of petroleum products(rotational method)CTaHAapTHLI MeToA onpegeneHnA TeMnepaTypbI 3acTbi-BaHA HeTenpoyKTOB(MeToA BpaweH)CTaHAapT pa3pa6oTaH KOMMTeToM ASTM DO2 HepTenpoAyKTbI CMa304Hble MaTepnanbI Haxogutca nog KoHTponem nogKomnTeTa D02.06 AMepnkaHckoro o6wecTBa no CnbITaHnAM n MaTepna-naM.epeBo c aHrnckoro 3bika(en).HanmeHoBaHne HacToq山ero MexrocyAapcTBeHHoro cTaHAapTa 3MeHeHO OTHOCTeNbHO HanMeHO-BaHn yKa3aHHoro cTaHgapTa n npBegeHn B cooTBeTcTBe c OCT 1.5-2001(nopa3en 3.6).OOnyManbHble 3K3emnnpb cTaHAapTa ASTM,Ha ocHoBe KoToporo nogroToBneH HacToq山n Mex-rocyAapcTBeHHbi cTaHAapt,cTaHAapToB ASTM,Ha KoTopbie gaHbi ccbinKn,MeoTcA B eAepanbHOM H-中opMaLMOHHOM 中oHAe TexHnecKnX pernaMeHTOB n cTaHAapTOB.CBegeHuA o cooTBeTcTBn MexrocyAapcTBeHHbix cTaHAapTOB cCbino4HbiM cTaHAapTam npBeAeHbIB AononHTenbHoM npnoeH A.A.CTeneHb COoTBeTCtBn-AeHT4Ha(IDT)5 puKa3om 中egepanbHoro areHTcTBa no TexHn4eckoMy perynpoBaHnio n MeTponornn oT 22HoR6pA 2013 r.Ne 691-cT MexrocyAapcTBeHHbi cTaHAapT FOCT 32393-2013 BBeAeH B AecTBMe BkayecTBe HauoHanbhoro cTaHAapTa PoccncKon 中egepayn c 01 AHBapa 2015 r.6 BBEAEH BNEPBbIEFOCT32393-2013MHpopMayuA 06 u3MeHeHuAx K HacmogeMy cmaHdapmy ny6nukyemcA e exe2odHOM uHpopMa-quOHHOM yka3amene HaquoHanLHbe cmaHdapmbi,a meKcm u3MeHeHuu u nonpaeok-e exeMeCR4HOMuHcpopMaquoHHOM yka3amene HayuoHanLHbie cmaHapmbi.B cnyuae nepecMompa(3aMeHbi)unu om-MeHbI Hacmogue2o cmaHdapma coomeemcmeyiouee yeedomneHue 6ydem ony6nukoeaHo e exeMec4-HOM uHpopMauOHHOM yKa3amene HayuoHanbHbIe cmaHdapmbi.Coomeemcmeyiowa uHpopMauus,yeedomneHue u mekcmbi pa3Mewaiomcs makke e uHpopMayuoHHo cucmeMe o6山e2o nonb3oBaHu-HaopuquanLHoM came PedepanLHo2o a2eHmcmea no mexHu4eckomy pezynupoeaHuio u mempono2uu ecemu HmepHemCTaHAapTHopM,2014B Poccnckon 中egepaynn HacToAyn craHgapt He MOxeT ObITb NONHOCTbIo n yacT4HOBOcnpon3BeAeH,TpaxMpoBaH n pacnpocTpaHeH B ka4ecTBe ouManbHoro n3AaHnA 6e3 pa3peweHA中egepanbHoro areHTcTBa no TexHn4eckoMy perynnpoBaHnIo n MeTponornnFOCT 32393-2013ME KOC YAAPC TBEHHbIMCTAHAAPTHE中TENPOAyKTbIOnpegeneHne TeMnepatypbi 3actbiBaHug MeTogOM BPaweHAPetroleum products.Determination of pour point by rotational methodAaTa BBeAeH-2015-01-011 06nacTb npMeHeH1.1 HacToAwni craHgapt ycTaHaBnMBaet MeTog onpegeneHnA Temnepatypbi 3acTbIBaHnA HeTe-npogyKToB c cnonb3oBaHMeM aBToMaT4eckoro npopa,HenpepbiBHO Bpauaiouero oxnaqaeMyio nc-nbiTyeMyo npo6y.1.2 HacToA MeTog npumeHAiot npn teMnepatype or MnHyc 57 C go nnoc 51 C,oAHako npo-rpaMMa Mexna6opaTopHbix ncnbiTaH 1992 r.,6bina npoBegeHa np Temnepatype oT MHyc 39 C Aonnioc 6 C(cM.13.4).1.3 HacToqu meTog onpegenget oTcyTcTBe Te4eHnA HeptenpogykToB npn kpucTannn3aunno6pa3ua n/n yBenneH ero BA3KOCT.1.4 Hactou metoA he npeAHa3HayeH An cbitaHA cbipo Hetn.p u m e 4 a H u e 1-Bo3MoxHoctb npnMeHeHng Hactoqw(ero metoga Ag cnbitaHnA Ma3yTa He ycTaHoB-neHa.onee nopo6Ha HopMau npBeAeHa B 13.4.1.4 3Ha4eHna B eAnHnyax cnCTeMbI C paccMaTpnBaoT KaK cTaHgapTHble.Apyrne eAnHnUbI n3Me-peHn B HacTon cTaHAapT He BKno4eHbI.1.5 B HacTouem cTaHAapte He npeAycMoTpeHO paccMoTpeHne Bcex BonpocoB 06ecne4eHA 6e3-onacHOCTM,cBA3aHHbix c ero npnMeHeHeM.onb3oBaTenb HacTouero cTaHgapTa HeceT OTBeTCTBeH-HOCTb 3a ycTaHoBneHne cooTBeTcTByox npaBnn no TexHnke be3onacHocTn n oxpaHe 3opoBba,a Takkeonpegenget yenecooopa3HocTL npMeHeHnA 3aKoHOgaTenLHbIx orpaHeHnn nepe ero ncnonL3oBaH-eM.2 HopMaTBHble ccbIJIKnAng npMeHeHnA HacTowero cTaHgapTa Heooxognmbi cneAyioue ccbino4Hble goKyMeHTbi.AnHeAaTpoBaHHbIX ccbinoK npMeHAoT nocneqHee n3AaHne ccbino4Horo gokyMeHTa(Bkno4a Bce ero n3-MeHeHMA)ASTM D 97 Standard test method for pour point of petroleum products(CTaHAapTHLI MeToA onpe-AeneHn TeMnepatypbi Tekyuect HeTenpoAyKToB)ASTM D 4057 Standard practice for manual sampling of petroleum and petroleum products(CraH-AaptHag npaktuka pyHoro oToopa npo6 HeT n HeTenpoAyKToB)ASTM D 4177 Standard practice for automatic sampling of petroleum and petroleum products(CTaHAaptHag npaktnka aBtoMatneckoro or6opa npo6 HeTn n HeTenpoAyKToB)IP 15*Test method for pour point of petroleum products(MeTog onpegeneHnA TemnepaTypbi 3a-CTbIBaHg HeTenpoAyKTOB)门p u M e 4 a H ue-p nonb3oBaHnn HacTOAuM cTaHAaptom yenecoo6pa3Ho npoBepntb AenctBneccbIno4HbIX cTaHAapToB B HopMaLnOHHo CncTeMe oowero nonb3oBaHnA-Ha onanbHoM cante egepanbHoroareHTcTBa no TexHMueckoMy perynnpoBaHMio n MeTponorM B ceT VHTepHeT n no exeroAHoMy HOopMaMOHHOMyyka3atenio HaynoHanbHble cTaHgapTbi,KoTopbi onyonnKoBaH no cocTOAHMo Ha 1 gHBap tekywero roga,n no CcbInKn Ha cTaHAapTb ASTM MokHO yTo4HNTb Ha calite ASTM website,www.astm.org un B cnyx6e noAepxknKnMeHToB ASTM serviceastm.org,a Takke B nHpopMayNOHHOM ToMe exeroAHoro c6opHnKa cTaHAapToB ASTM(Website standards Document Summary).AocTyneH B HcTTyTe 3HepreTukn,61 New Cavendish St.,London,WIG 7AR,U.K.,http:/www.energyinst.org.uk.M3aHne ouanbHoeOCT 32393-2013BbinycKam exeMecq4Horo HpopMayMoHHoro yKa3ateng HayoHanbHble cTaHgapTbi 3a tekyun rog.EcnMccbIno4HbI cTaHAapT 3aMeHeH(3MeHeH),To np noNb3OBaHMN HaCTOALMM CTaHAapToM cheAyeT pyKoBOACTBOBaTbCA3aMeHAHOWM(3MeHeHHbIM)CTaHAapTOM.ECnM cCbInO4HbI cTaHAapT oTMeHeH 6e3 3aMeHbi,To nonoeHMe,BKoTopoM AaHa ccbinka Ha Hero,npnMeHgeTcA B uact,He 3aTparnBaouwen 3Ty ccbinky.3 TepMHbI onpegeneHB HacToAuem cTaHAapTe npnMeHeHbi cneAyowe TepMMHbI c cOOTBeTCTByIoMn onpegeneHnA-M:3.1 TeMnepaTypa 3acTLIBaHA HepTenpoAyKToB(pour point of petroleum products):CaMa Hn3-ka Temnepatypa,npn KoTopo Ha6niogaetcA ABneHne cnbITyeMo npo6bi npn ycTaHoBNeHHbIX ycnoBn-AX CnbITaHA.3.2 TeMneparypa npekpaueHn TeeHn HeTenpoAyKToB(no-flow point of petroleum products):TeMnepaTypa cnLiTyeMo npooLi,np KoTopon KpcTann3yeTcA napaOH/Mn nOBbIaeTCA BA3KOCTb,npenTcTByowne ABnxeHio noBepxHOcT npoobi B ycnoBAx cnbiTaHng.3.2.1 ocHeHneTeyeHne npekpawaeTc,ecnn npn oxnaxgeHnn 中opMnpyercA KpucTannn4ecka cTpyKTypa napa-OHa/nn noBbwaeTCA BA3KOCTb go 3Ha4eHn,np KOTOpOM yCTpOMCTBO OOHapyeHnA He perncTppyeTABnxeHne B ycnoBgx ucnbiTaHn.Temnepatypa npeAbiyuero ha6nogeH,npn koTopon ewe Ha6noAa-OT Te4eHne cnbityeMo npoobl,aBngetca Temnepatypo 3acTbiBaH.3.3 TeMnepatypa 3acTLIBaHnA HeptenpogyKToB c HTepBanoM CnbITaHnA 3 C(pour point at3 C testing intervals in petroleum products):TeMnepaTypa,BbI4cneHHa okpyrneHneM 3Ha4eHnA TeMne-patypbi,npu koTopon npexpawaetcA teyeHne ucnbiTyemon npo6bi,go 6nnxanwero yenoro uncna,kpaTho-ro 3C.3.3.1ocHeHneB HacToem MeToge cnbiTaHn TeMnepatypa npekpaeHnA TeyeHnA MOkeT ObITb 3MepeHa cTOHOCtbio go 0,1 C.B ASTM D 97 Ha6nogeHna npekpaueHng teyeHng npoBoAAt c HtepBanom 3 C.AaHHble BbI4ncneHnA npoBogAT np opopMneH pe3ynbTaToB no ASTM D 97.HexoTopble annapatbiMOryT BbinonHATb 3TM Bb4CneH aBToMateckn.3.4 BpawaTenLHLi(rotational):MeTog spaweHnA cocyga c nCnbiTyemo npo6o B BepTnKanLHOMnonokeHn Ha noBopoTHoM Ancke,cHa6xeHHOM cTayMOHapHbiM gaTynKoM TeMnepaTypbi n MaATHKOM,norpykeHHbIM B npo6y.3.4.1 ocHeHneO6pa3yoweca np oxnaxgeHnn npo6bi kpncTannbi nn noBbiweHne BA3KoCT npb oKa3biBaOTBnHe Ha MagTHnK,oTknoHgg ero oT cTaynoHapHoro nonokeHng,4To perncTpupyeTcA KaK TeMnepaTypanpekpaueHg TeyeH.4 CyHOCTb MeToa4.1 门omewaiot npo6y B aBToMatueckn annapat onpeAeneHnA Temnepatypbi 3acTbiBaHnA,BKn-aoT nporpaMMy,HarpeBaoT o6pa3ey,3aTem oxnaxgaoT 3a ceT noggepaHA nOcTOAHHOM pa3HOCTTeMnepatyp MexAy 6nokom oxnaxgeHng n npo6on.locToAHHo npoBepAoT xapakTepncTnkn TeyeHng npo-6bi,spawa cocyA c npo6o co ckopoctbio np6nn3nTenbHo 0,1 06/MnH Bokpyr cTaynOHapHoro,ypaBHO-BeweHHoro wapoo6pa3Horo MagTHnKa.TemnepaTypy npo6bi,np KoTopon Kpncrannn4eckaA crpyKTypa/unn yBenn4eHne BA3Koct npo6bi Bbi3biBaeT CMeweHne MatHnKa,perncTpnpyioT c TO4HOCTbi gO 0,1 C.3aTem HarpeBaiot npo6y go nepBoHaanbHo TeMnepatypb.5 Ha3HaeHe n npMeHeHe5.1 TemnepaTypa 3acTbiBaHnA HeTenpoAyKToB BngeTcA noka3aTeneM caMoM Hn3Ko TeMnepay-pbi 3KcnnyaTaun.XapaKTepncTnKn TeyeHn,TaKne KaK TeMnepaTypa 3acTbiBaHnA,MOryT MeTb BaKHOe3Ha4eHne gn Ka4ecTBeHHon paoTbI CMa304Hon cnCTeMb,TONnMBHON CCTeMbI n 3KcnnyaTaunn TpyOo-npoBoAoB.5.2 An cMewnBaHn HeT Tpe6yeTcA TO4HO 3MepeHHOe 3Ha4eHne TeMnepatypbI 3acTbIBaHA.5.3 Hacoqwu metog no3Bonget onpegenutb temnepatypy npo6bi c TO4HOCtbio go 0,1 C.,npuKOTOpo 中OpMpyOTcA KpcTannbi nM B3KOCTb nOBbiaeTcA HacTonbKo,4to npengTcTByet te4eHOHeTenpoAyKTOB.5.4 TemnepaTypa 3acTbiBaHn,nony4eHHa no HacTogeMy MeTogy aHanorn4Ha 3Ha4eHIo no Me-TogaM ASTM D 97 u IP 15,B KoTOpbix pe3ynbTaTbI perncTppyoT c nHTepBanoM 3 C.2