ASTM_D_7372_-_12_rus.pdf

D737212 ()STANDARD GUIDE FOR ANALYSIS AND INTERPRETATION OF PROFICIENCY TEST PROGRAM RESULTS 2017 ():07.11.2017:3310-17/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D7372-12 1 D737212 ()1 D7372;,.()1.1.1 (-).()(,.),.,1 ASTM D02 D02.94 .15 2012.2012.2007.2007.D7372-07.DOI:10.1520/D7372-12.ASTM D7372-12 2 ,.1.2 ,.,.2.2.1 ASTM:2 D1266 ()D2622 D4294 D4951 -D5185 ,-2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D7372-12 3 D5453 ,-D6259 D6299 D6617 D6792 ,D7039 E177 ASTM E456,E2655 ASTM 3.3.1:3.1.1 .E177,E456 3.1.2 ,ASTM D7372-12 4 .E456 3.1.3 ,.E177,E456 3.1.4 ,.E456 3.1.5 ,.D6299 3.1.6 ()ASTM,D02 (.ASTM).3.1.7 D6299 3.1.8 ,.E2655 3.1.9 Z-,().D6299 3.1.10 Z-,Z-,ASTM D7372-12 5,.Z ,()1().:Z-Z-,Xi-,X-,s-,s -.3.2 ,:3.2.1 (),-.D6299 3.2.2 (R),0,95(95%).,2,77 ,.D6299 3.2.3 ,ASTM D7372-12 6 ,15.D6299 3.2.4 ,ASTM International D02 ,.3.3 :3.3.1 I (I-).3.3.2 QC .3.3.3 R .4.4.1 ,.,.5.5.1 ,(),.ASTM D7372-12 7 5.2 ,.,.,:5.2.1 .()Z-()5.2.2 ,.C (Box and Whisker)5.3 ASTM .,ASTM D7372-12 8 .X2,X3,.6.6.1 ,.,.6.1.1 ,.,.6.1.2 ,.,.6.1.3 ,.,.6.2 :6.2.1 ASTM D7372-12 9,.X1 D6299.6.2.2/ASTM (1 3 ),:1 3-2 3-ASTM 3 Z-2 2 ,.:1 2 3.1 ,(),.2.3 ,.1 ,2,-.,.,-1,3,2 .ASTM D7372-12 10 6.2.3 ,.X1.6.3 :6.3.1 ,.-(),.D6299 .6.3.1.1 D6299 ,.1.0 ;1 -(-)6.3.2 .,ASTM D7372-12 11 q-q(,).D6299 .,.,().X3.1.6.4:6.4.1 .,n 20,99-n 30.2,33 ,2,33 99-.6.4.2 ,.,.,.,Z-,()ASTM D7372-12 12 ().X3.1.6.5 ():6.5.1 D6299,7.6,.D6299 ()().(),.(I-)(EWMA),.X3.2.6.5.2 (Box and Whisker).,.-,.,.7.2.6.5.3 D6617.,ASTM D7372-12 13 .6.6 Z-Z-,:6.6.1 Z-(+-).Z-,0 1,1 2,2 3 3,1-,1 2-,2 3-3-.,68%-1 +1,95%-2 +2 99%-3 +3.Z-,.-.6.6.2 Z-Z-().-,D6299.()(Z-Z-)Z-.ASTM D7372-12 14 =0,8 .0,8,.6.6.3 Z-Z-.-.6.6.4 Z-Z-,6.6.3 Z-.6.7 (),(),Z-,(),().,ASTM,.6.7.1 1 ():6.7.2 ()Z-(),Z-(.D6792).()3(-3),ASTM D7372-12 15 .()1,0.7.7.1 ,.,.ASTM D7372-12 16 1 ()1,2 ASTM.0,8 1,2 (),.3),.8.8.1 .,.ASTM D7372-12 19 9.9.1 ;Z-.ASTM D7372-12 20 ()X1.X1.1 ,().X1.1.1 ,.X1.1.2 ;,.X1.1.3 ,ASTM.X1.1.4 .X1.1.5 ,.X1.1.6 ,.X1.1.7 ,.X1.1.8 .X1.1.9 ,ASTM D7372-12 21 ,.X1.1.10 -,.X1.1.11 ,.X1.1.12 ,.X2.,.X2.1 -()X2.1.1 D6299 ,.(1,0,.X2.2 X2.2.1 (),.ASTM D7372-12 22 (X2.1):s-(),n-,.X2.2.2 95%-,.X2.2.1,96 (.E2655).X2.2 ,X3.95%-=X(1,96 )(X2.2)X2.3 X2.3.1 .X2.3,.,(),).(X2.3):n1-,(),s1-,N-.ASTM D7372-12 23 X2.4 F X2.4.1 F .X2.4 ,.F ,()(X Y),(,).(X2.4)X2.4.2 nY-1 nX-1.Excel3 p():(X2.5)X2.4.3 p 0,05,X Y 95%-.p 0,10 p 0,01,sX sY 90%99%-.X2.5 X2.5.1 .X2.6 ,X Y.,.3 Microsoft.ASTM D7372-12 24 Excel TDIST .3 (X2.6)X2.5.2 :(X2.7)X2.5.3 Excel3 p()p=TDIST(t,df,2).p 0,05,95%-,.X2.6 X2.6.1 ,.X2.8.(X2.8):df=nX+nY 2,p=TDIST(t,df,2).X2.6.2 p 3 ,.X3.1.5 .,.X3.9 Excel3 DF20910#2.,ASTM D7372-12 27 7/,D2622,D5453 D7039 .D4294 .,D4294,.Excel3 ,.X3.2 ()X3.2.1.X3.10 (ULSD)D5453.,().,(EWMA),.,Z-,.X3.3 Z-X3.3.1 .X3.11 Z-,ULSD D7039.ASTM D7372-12 28 (Excel3),EWMA,.Z-.Z-.F,Z-.,.F ,12 .,2 ,1.X3.3.2.X3.12 Z-ULSD D5453.,Z-,.,(s=0,71)(s=1,06).,F ,.,Z-,.,Z-,.X3.3.3.X3.13 Z-,D4951.ASTM D7372-12 29 (Excel3).().,Z-1 -2 0 -1.0,8,.B 1,0,.().X3.5 X3.5.1 .X3.15 .,.X3.12 2009.ASTM D7372-12 30 1240/(0,1240.%).()()(D2622,D4294 D5453).D1266 ,.,.X3.15,.F ,D2622 D5453,.,.X3.6 (X)X3.6.1 ,.,.-.X3.16 ,(RFG)./.,ASTM D7372-12 31 D4294 ,.D2622,D5453 D7039 ,.-.,-.X3.6.2 .,(X 1,96 ).X3.17 .X3.18 ,.D4294 D2622 .X3.17 ,(D4294,-D2622).,95%-,F ,D4294,.X3.6.3 .,.X3.18 ,ASTM D7372-12 32 D5453 D2622.,.,D5453 D2622.X3.6.4 .X3.19,D4294 ,D2622.F ,D4294 D2622.,D4294 D2622 95%-;90%-.,.X3.7 ()X3.7.1.X3.20 .X3.21 (),RFG,.()D5453 ,.,ASTM D7372-12 33 ()1,0,.()D4294 ,.,.D4294 (),RFG ,.X3.7.2.X3.21 (),ULSD.(),()D5453 0,6 1,0.D4294 .,D4294,RFG 100/.X3.8 ()X3.8.1.X3.22 ,D2622.,(),ASTM D7372-12 34#2,Mogas RFG.D2622 ()ULSD 5 15/.X3.8.2 D4294 .X3.23,100/.,.,-.X3.8.3.X3.24 D5453 .D2622(.X3.22),D5453 ULSD.D2622 .,.X3.9 -X3.9.1 .X3.25 D5453 0 15/,.D5453 ULSD,-.ULSD 10 ASTM D7372-12 35 20 0 10 .X3.25 ,.X3.24.,.:DF21006 -D7039(/).X3.1#2 D7039 ASTM D7372-12 36 S#2 D7039(DF21006;=0,73).X3.2#2 D7039 :DF20906 -D5453(/).X3.3#2 D5453 ASTM D7372-12 37 S#2 D5453(DF20906:=0,93).X3.4#2 D5453 :LUD905 -05185(/).X3.5 D5185 ASTM D7372-12 38 Ca D5185(LU0905;=1,07).X3.6 D5185 :DF20906-D2622(.%).X3.7#2 D2622 ASTM D7372-12 39 S#2 D2622(DF20906;=2,04).X3.8#2 D2622 .X3.9#