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ASTM_D_7041_-_04_2010_rus_scan.pdf
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TM_D_7041_ _04_2010_rus_scan
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BHVM Hn)2 BHECEH enepanbHbIM areHTCTBOM no TexHnueCKoMy perynnpoBaHnlo MeTponorn(PoCCTaHAapT)3 nPMHAT MexrocynapcTBeHHbIM coBeTOM no cTaHgapTn3aynn,MeTponornn n cepTnonkaynn(npo-T0K0n0T18MoH92015r.N947)3a npnHaTne nporonocoBann:KpaTkoe HanMeHoBaHne CTpa-KoA CTpaHblCokpaweHHoe HaNMeHoBaHNeHblnoMK(MC03166)00497HauMoHanbHoro opraHan0MK(MC03166)004-97no cTaHgapTn3aylnApMeHNAAMMNH3KOHOMNKN Pecny6nNKn ApMeHNAKnprN3N9KGKblprbl3cTaHnapTMonAoBaMDMonAoBa-CTaHAapTPoccnaRUPoccTaHnapTy36eKncTaHUZy3cTaHnapT4 npnka3oM enepanbHoro areHTCTBa no TexHnyeCKoMy perynupoBaHnlo n MeTponornn OT 31 aBrycTa2015 r.Ne 1261-CT MexkrocynapcTBeHHbin CTaHaapT TOCT 33253-2015 BBeaeH B eNCTBMe B KayecTBeHayMoHanbHoro CTaHAapTa Poccnnckon enepaynn c 1 AHBapa 2017 r.5 HacToaunn cTaHnapT MAeHTw4eH cTaHAapTy ASTM D7041-04(2010)Standard test method fordetermination of total sulfur in light hydrocarbons,motor fuels,and oils by online gas chromatography withflame photometric detection(CTaHnapTHbIn MeTon onpeneneHna oowen cepbl B nerknx yrneBonoponax,MOTOPHbIX TonnNBax N Macnax noTOYHON ra30BoN xpoMatorpaonen c nnaMeHHO-OOTOMeTpNyeCKNM neTeK-TNpoBaHNeM).CTaHAapT pa3pa6oTaH noAKOMMTeTOM D02.03 3neMeHTHbIi aHann3TexHnueckoro KOMNTeTa ASTMDO2He中TenpoayKTbl M CMa3 OuHble Matepnanbly.nepeBon c aHrnwnckoro 93bika(en).HaNMeHOBaHne HacTogwero CTaHnapta N3MeHeHO OTHOCNTenbHO HanMeHOBaHNA yKa3aHHoro CTaH-AapTa ana npuBeneHMa B CooTBeTCTBMe c rOCT 1.5-2001(nyHKT 3.6).OoMuNanbHble 3K3eMnnapbl CTaHnapta ASTM,Ha OCHOBe KOToporo nonroToBneH HacToAwNn MexKro-cynapcTBeHHbIn CTaHnapT,CTaHnapToB,Ha KoTopble naHbl cCbinkn,WMelOTCA B enepanbHOM NHopMaun-OHHOM OHne TexHNyecKnx pernameHTOB N CTaHnapToB.CBeneHNA O COOTBeTCTBNN MexkrocynapcTBeHHbIX CTaHnapToB cCblnoyHbIM CTaHnaptaM npnBeneHbl BononHNTenbHOM npwnoxkeHnN A.CTeneHb COoTBeTCTBNA-MaeHTNYHaA(IDT)6 BBENEH BNEPBbIE4FOCT 33253-2015M E K T O C YA A P C T B E H H bIMC T A HA A PTHETENPOAYKTbIOnpegeneHne o6wero cogepxaHA cepbi MeTogoM ra3oBonXpoMaTorpa中nn c nnaMeHHO-中oToMeTpnyecKnM AeTeKTuPOBaHeMPetroleum products.Determination of total sulfur content by gas chromatography method with flame photometricdetectionAaTa BBeAeH-2017-01-011 06nacTb npMeHeHA1.1 HacTown cTaHAapT ycTaHaBnnBaet onpegeneHne o6wero cogepxaHn cepbi B nAKnx yrneBo-gopogax c Temnepatypom KoHua KnneHnA go 450 C MeTogom ra3oBon xpoMatorpann c ncnonL3oBaHneMnnaMeHHo-oToMeTpeckoro AeTekTopa.1.2 HacTouu meTog moxho npnmeHAtb npn 06wem cogepxaHnn cepbi oT 0,5 go 100 mr/kr.p n M e 4 a H e 1-Ha ocHoBaHnn pe3ynbTaToB nporpaMMLI Mexna6opaTopHbIX o6beAHeHHbIX C-nbtahn 2002 r.6biN yctaHoBneH o6begnHeHhbi npegen konnuectBeHHoro onpegeneHnA(PLOQ),paBHbi 1 Mr/kr.p n M e 4 a H n e 2-MokHo npoBoAnTb aHann3 o6pa3yoB c pyrnMn ypoBHAMn oowero cogepxaHngcepbi,Ho Ana taknx o6pa3uoB He cneAyet npMeHATb npe3nOHHOcTb,ycTaHoBneHHyio B HacTOeM cTaHAapTe.1.3 3HaeHng,ycTaHoBneHHble B eAnHnyax C,cunTaoT cTaHAapTHbIM.1.4 B HacToueM cTaHAapTe He npeAycmoTpeHO paccMoTpeHMe Bcex BonpocoB 06ecne4eHA Ge30-nacHOCTM,cBA3aHHbIX c ero cnonb3oBaHeM.onb3oBaTenb cTaHgapTa HeceT OTBeTCTBeHHOCTb 3a o6eC-ne4eHMe cOOTBeTCTByOLX Mep 6e3onacHOCT OxpaHbI 3AOpoBbA n onpegengeT yenecoopa3HOCTbnpMeHeHA 3aKoHogaTenbHbix orpaH4eH nepeg ero mcnonb3oBaHeM.CneyanbHbie yKa3aHnA noTexHKe 6e3onacHocT npBeAeHbI B pa3gene 7.2 HopMaTBHble cCbInKnAng npMeHeHnA HacToero cTaHAapTa Heo6xoAnMbi cneAyioue ccbino4hble AokyMeHTbi.An HeAa-TPoBaHHbIX cCbInoK npnMeHioT nocneAHee n3aHne ccbino4Horo goKyMeHTa(Bkno4a Bce ero n3MeHeH).2.1 CTaHAapTbI ASTM1:ASTM D 1298 Test method for density,relative density,or API gravity of crude petroleum and liquidpetroleum products by hydrometer method(MeTog onpegeneHA nnoTHOCT,OTHOCTeNLHO nnOTHOCTunu nnoTHoctn B rpagycax API cbipo HeTn n xnAKnx HeTenpoAyKTax apeoMeTpoM)ASTM D 4052 Test method for density,relative density,and API gravity of liquids by digital densitymeter(Merog onpegeneHn nnoTHoctn,oTHocutenLHou nnoTHoct u nnoTHocTn xnAKocTen B rpaycaxAPI POBbIM nnoTHOMePoM)ASTM D 4057 Practice for manual sampling of petroleum and petroleum products(门lpakrnka pyqHoroOTopa npo6 HedT n HeTenpoyKTOB)ASTM D 4177 Practice for automatic sampling of petroleum and petroleum products(lpaKruka aBTo-MaTneckoro oToopa npo6 HeT n HeTenpoAyKTOB)ASTM E 840 Practice for using flame photometric detectors in gas chromatography(lpakruka ncnonL-30BaHn nnameHHo-oTomeTpecknx geTekTopoB B ra3oBon xpoMaTorpaonn)3 CyuHOCTb MeTogaO6pa3ey aHann3npyoT MeToAoM ra3oBo xpomaTorpann c nnaMeHHo-oToMeTpn4ecKnM geTeKTo-poM.中nKcpoBaHHoe KonMecTBo o6pa3ya BBoAAt B ra3oBb xpomaTorpa,B KoTopom 06pa3ey ncnap-eTcA.loToK Bo3Ayxa nepeHocuT napbi o6pa3ya B BbicoKoTemnepaTypHyo 30Hy(900 C),B KoTopo npn-cyTCTByoune B oopa3ye coegnHeHn oKncnoTcA.Cepa,cogepxaac B coeHeHx,oKncneTcA OAnoKcnga cepbi(SO2).loTok nepeHocut oKncneHHble KOMNOHeHTbi B XpoMaTorpapnueckyio KonOHKy,B Ko-)YTo4HNTb ccbInKn Ha cTaHAapTbi ACTM MoxHo Ha cavite ACTM www.astm.org unu B cnyx6e nogepxkn knn-eHToB ACTM:serviceastm.org.B nHpopMauMOHHOM 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