ASTM_D_6481_-_14_2019_rus.pdf

D6481-14(2019.),STANDARD TEST METHOD FOR DETERMINATION OF PHOSPHORUS,SULPHUR,CALCIUM,AND ZINC IN LUBRICATION OILS BY ENERGY DISPERSIVE X-RAY FLUORESCENCE SPECTROSCOPY 2019 ():08.08.2019:3728-19/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D6481-14(2019)1 D6481-14(2019.),1 D6481;,.().1.1.1 ,.1.1.0,02%0,3%0,05%1,0%0,02%1,0%0,01%0,3%1 ASTM D02 ,D02.03 .1 2019.2019.1999.2014.D 6481-14.DOI:10.1520/D6481-14R19.ASTM D6481-14(2019)2 1.2 (EDXRF),.1.3 ,.1.4 ,.1.5 ,.1.6 .1.7 ,.,.1.8 -,(TT).2.2.1 ,.,.ASTM D6481-14(2019)3 ,.,.2.2 EDXRF ,.,.3.3.1 -,.:,.,.3.2 ,(.2).3.3 ,.ASTM D6481-14(2019)4 2.,4 4.1 ,.,(),.,(,).,0,03%,1%.,.,ASTM D6481-14(2019)5 .4.2 ,0,03%,.4.3 ,0,03%,.4.4 ,.5.5.1 ,:5.1.1 ,4 25 ,.(,).5.1.2 ,1300 5,9.ASTM D6481-14(2019)6 1 ,.5.1.3 ,.5.1.4 ,.5.1.5 ,.5.1.6 ,.5.2 ,6 ,.3,5 8.5.3 (),.,().5.4 ,.,.,ASTM D6481-14(2019)7 XRF .,5.3.6 6.1 .,.2 ,.6.2,99,5%,.6.3 ,10 ppm (,).6.4 :6.4.1 3 ,.,.,:6.4.1.1 2-,12,3%.2 ,DC.,.Analar Standards for Laboratory Chemicals,BDH Ltd.,Poole,Dorset,United States Pharmacopeia and National Formulary,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.3 .ASTM D6481-14(2019)8 6.4.1.2 ,16,2%.6.4.2(2-),97%(9,62%).6.4.3-,97%(21,9%).6.4.4,2-,2-./.,.2 ,6.4.1 6.4.3,(,),%.3.(%)1 0 0 0 0 2 0,005 0,005 0,050 0,05 3 0,600 0 0 0 4 0 0,300 0 0 5 1,00 0 1,00 0 6 0 0 0 0,300 7 0,005 0,250 0,800 0,300 8 0,500 0,150 0,500 0,150 9 0,010 0,200 0,100 0,250 10 0,050 0,010 0,400 0,075 11 0,100 0,150 0,200 0,200 12 0,200 0,200 0,800 0,100 13 0,400 0,005 0,800 0,300 14 0,600 0,100 0,500 0,050 15 0,800 0,010 0,050 0,100 16 1,00 0,300 1,00 0,150 17 0,400 0,050 0,600 0,250 ASTM D6481-14(2019)9 7.7.1 ,.3 .3.8.8.1 (,),.8.2 .,.,.,.8.3 ,8.1.,.8.4 ,.ASTM D6481-14(2019)10 .8.5 .3 ,8.4,8.5,.8.6 ,.4.(,).,.(,).,.4 ,-.4.-ASTM D6481-14(2019)11 9.9.1 .,.,.,.9.2 ,8.1.10.10.1 .11.11.1 :11.1.1 ,.11.1.2,D6481.12.(QC)12.1 QC,.,QC .ASTM D6481-14(2019)12 12.2 QC ,.12.3 QC ,.13.4 13.1 ,:13.1.1 ,.5 .5.,%0,0060 0,01648(+0,0141)0,8 0,008795(+0,0120)0,5 0,0032740,25%.13.1.2 ,4 -ASTM International RR:D02-1460.ASTM :serviceastm.org.ASTM D6481-14(2019)13,.6 .6.,%0,0199 0,1024(+0,0141)0,8 0,1492(+0,0120)0,5 0,021650,25%.5 .5 6,.7.7.%(X)0,02 0,006 0,020 0,05 0,006 0,020 0,15 0,006 0,020 0,3 0,006 0,020 0,05 0,002 0,011 0,10 0,003 0,018 0,50 0,010 0,060 1,0 0,017 0,104 0,02 0,002 0,027 0,05 0,002 0,037 0,10 0,003 0,050 0,50 0,006 0,107 1,0 0,009 0,150 0,01 0,001 0,007 0,05 0,002 0,10 0,10 0,002 0,012 0,15 0,002 0,014 0,3 0,002 0,016 13.2 D6481 ASTM D6481-14(2019)14 ,.14.14.1 ;()1.1.1 ,.,.1.2 ,.,.1.3 .1.4 ,.1.5 ,QC.1.6 ,QC .1.7 QC,.ASTM D6481-14(2019)15 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.