ASTM_D_7029_-_09_rus_scan.pdf

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ncnonb3oBaHbI HOpMaTNBHble ccbinkn Ha chegyiowne cTaHAaptbl:OCT14888 BeH3ouna nepekucb mexHu4ecka.TexHu4eckue ychoeuaOCTP 55134-2012(MCO 11357-1:2009)nacmMaccbi.DuppepeHuuanbHaR ckaHupyow,a kano-puMempu(ACK).4acmb 1.06wue npuHuunbip u Me 4 a H ne-p nonb3oBaH HacTOuM cTaHAapToM enecoo6pa3Ho npoBepTL gecTBe ccbino-HbIX cTaHAapToB B MHPopMaMOHHo ccTeMe o6wero nonb3oBaHMA-Ha opManbHoM cante PeAepanbHoroareHTcTBa no TexHM4ecKoMy perynpoBaHnio n MeTponornM B ceTH VHTepHeT nn no exeroAHoMy nHPOpMauOHHOMyyKa3atenio HanoHanbHbe cTaHAaptb,KoTopbiony6nnKoBaH no cOcToHI Ha 1 HBap Tekyuero roga,n no Bbinyc-Kam exeMec4Horo HpopMayoHHoro yka3ateng 3a Teky roA.EcnM 3aMeHeH cCbINO4HLIM cTaHAapT,Ha KOTOpbiNgaHa HegatpoBaHHa ccbinka,To peKoMeHAyeTcncnonb3oBaTb geMcTByiouyio Bepcnio aToro cTaHgapTa cyeToM BcexBHeceHHbIX B aHHyIo Bepcn n3MeHeHn.Ecnn3aMeHeH ccbno4HbiNcTaHapt,Ha KoTopbin gaHa gaTnpoBaHHa ccbinKa,To peKoMeHAyeTc cnonb3oBaTb BepCio 3Toro cTaHAapTa c yKa3aHHbIM Bbiwe rogoM yTBepxAeH(npHAT).Ecnnnocne ytBepxgeHng Hactoguero ctaHgapta B ccbino4hbin cTaHgapt,Ha KoTopbin gaHa gaTnpoBaHha ccbinKa,BheceHOn3MeHeHMe,3aTparnBaiouee nonokeHe,Ha koTopoe AaHa ccbunKa,To 3To nonoeHne peKoMeHAyeTCA npMeHATb 6e3yueta gaHHoro 3MeHeHn.Ecnn ccbinohbi cTaHAapt oTMeHeH 6e3 3aMeHbi,To nonoxeHne,B KoTopoM gaHa ccbinKa HaHero,peKoMeHAyeTca npMeHaTb B act,He 3aTparnBaiowen 3Ty ccbinky.3 TepMHb n onpegeneHB HacToAeM cTaHgapte npnMeHeHbI cneAyiow,ne TepMHbI c cOoTBeTCTByowMn onpeAeneHnAMn:3.1 Bpem reneo6pa3oBaHnA:epnog BpeMeHn,BbipaxeHHbI B MnHytax n cekyHAax,3a KoTopbiMTeMnepatypa,n3MepgeMag npoMeTpoM,noBbiwaeTcA oT TeMnepatypbi Hnke(06bi4HO Ha 5,5 C-16 C)TeMnepaTypbI TepMocTatpoBaHnA go TeMnepaTypbiBbiWe TeMnepatypbi TepMocTatnpoBaHnA Ha 5,55 C;kaKnpaBuno,Ang temnepatypbi tepMoctatupoBaHng,paBHo 82,2 C,-3to guana3oH teMnepatyp oT 65,5 CAo 87,8C.3.2 BpeM oTBepxAeHng:epnog BpemeHn,BbipaxeHHbinB MHytax n cekyHAax,3a KoTopLi TeMne-patypa,3MepgeMag nnpoMeTpoM,noBbiwaetcA oT TeMnepatypbi He(o6bi4Ho Ha 5,5 C-16)TeMnepa-TypbI TepMOcTaTpoBaHn go MaKcManbHo TeMnepaTypbi,Kak npaBno 3To Auana3oH TeMnepaTyp oT65,5，o 82,8C.M3AaHne opnunanbHoe0CTP57565-20173.3 BpeMa npoxoxneHn HTepBana:nepnon BpeMeHn,BblpakeHHbin B MWHyTax n cekyHAax,3aKOTopbIN TeMnepaTypa,W3MepaeMaa nmpoMeTpoM,CHNKaeTCA OT TeMnepaTypbl Bblwe TeMnepaTypbl TepMo-CTaTnpoBaHna Ha 5,5C Ao MakcnManbHon TeMnepaTypbl.Bpema npoxoxneHna MHTepBana-3To pa3HMuaMexkny BpeMeHeM OTBepkneHna N BpeMeHeM reneoopa3oBaHna.3.4 3K3oTepMwyecknn nnk:MaKcnManbHa TeMnepaTypa,AocTnraeMa npn npoBeneHnn ncnblTa-HMM.3.5 nmpoMeTp:Lnpoknn Knacc ycTpoNcTB n N3MepeHna TeMnepaTypbl,BKnoya TepMonapbl,cBO3MOXKHOCTbHO HenpepblBHoN percTpauln TeMnepatypbl.3.6 WHnuNaTop:BewecTBo,nalowee CBo6O Hble pannkanbl,Heo6xoAMble n Hauana pannkanbHoNnonnMepn3aunn HeHacblweHHblx nonn3npHblx n BNHnn3npHblX CMon.Kak npaBnno,ncnonb3yIoT nepekncbwnN coyeTaHne HeckonbKNX NHNuMaTopoB.4 CywHocTb MeTonaCMony cMewNBaoT c HWuMaTopoM B nabopaTopHOM cTakaHe.npn noMown TepMonapbl perncTpnpyOT3K3OTepMNyeckyio kpnByo,dopMnpyeMylo CMonon no Mepe ee oTBepneHNa.CTpoaT KpNByio,onpenenaloTBpeMa DOCTNKeHNa pa3HbIX TeMnepaTyp,a Takke nonyueHHoro 3K3OTepMNyeckoro nwka.B KayecTBe NHNUMa-Topa Ncnonb3yIOT nepekncb 6eH3owna,nonyckaeTca npwMeHATb apyrne WHNuNaTopbl.HacTogwnn MeTog ncnblTaHnn naeT NHcopMaunio o BbinengeMoM npn OTBepxneHnn CMonbl Tenne nnpononKNTenbHOCTn BpeMeHn,korna cMona N3 KnAKoro COCTOAHNA nepexonT B TBepnoe.AaHHbin MeTon aHanornyeH MeTony ucnblTaHnn no OCTP55134.5 Annaparypa5.1冂poMeTp camonnwy山MN co cKopoCTblo perncTpaunn rpa中MKa1,5M/4.5.2 TepMoMeTp c ueHon neneHna 0,05C n AMana3oHOM 3MepeHnN,COoTBeTCTByIOUNM TeMnepaTypeOTBepxneHNA WcnblTyeMON CMonbl.5.3 TepMocTaT,3anonHeHHbin BonoN wnM apyroN NKOCTblO,C BO3MOXKHOCTbo perynwpoBaHna TeMne-patypblc norpewHocTblO He 6onee 0,2C,co cKopoCTblO CMeHbI KNAKOCTN 1-206wero o6beMa TepMoCTaTa BMWHyTy.O6beM TepMocTaTa-He MeHee 8,8 AM3.TepMocTaT nomkeH 6bITb OCHaweH KpblWKoN C OTBepCTn9-MM n BCTaBKn HarpeBalowero 3neMeHta,TepMoMeTpa n npo6npoK,4To6bl cBecTn K MNHNMyMy ncnapeHneBOAbl.5.4 npo6upkn n3 6opocunnkaTHoro cTekna anameTpoM 19 MM W AnNHoN 150 MM c rnaAKnM KOHUOM WHOCNKOM.5.5 Mrna TepMonapbl Thna J,W3roToBneHHag N3 HepxaBelowen cTann,AnNHon 152 MM C HapyKHbIMMaMeTpoM 3,2 MM,coe NHeHHa c 3axKNMOM B coope Twna Jwnn aHanoryHbIM.5.6 ABoNHon npoBon Thna J c nonnBNHnnxnopnaHon n3onaunen n uBeTHon MapknpoBKoN(6enbinUBeT-nonoxKnTenbHbin,KpacHbin-OTpMuatenbHbin)n npncoenHeHna wrnbl TepMonapbl Twna J KcaMonnwyweMy nnpoMeTpy wnw aHanor4HbIN.5.7 Becbl c norpewHoCTblo B3BewnBaHna He 6onee 0,01 r,C MMHNManbHbIM npenenoM B3BewnBaHna200r.5.8 LeHTpnpyrowee ycTponcTBo Ana ueHTpoBKn nrnbl TepMonapbl BHyTpn npo6bl CMonbl.3To ycTpon-CTBO MoXKeT 6bITb W3roToBneHo N3 apMnpoBaHHbix nnacTMacc,MWKapTbl wnn Apyroro nonxonwero MaTepna-na(CM.pvcyHOK 1).5.9 CTakaH na6opaTopHbln BMecTNMOCTbO 150 CM3 N3 CTekna wnw nnacTMaccbl.2FOCT P57565-201726,9238,123,0216,51-16,6623,0216.51-16.663,253,06166,68PcyHOK 1-LeHTppyioee ycTpOcTBO An LeHTPOBK nb6 PeaKTBbI n MaTepnanbl6.1 MoHoMep cTupona,c Ao6aBneHneM(155)ppm Tpetu4Horo 6ytun-katexnHa(TBC),B kayecTBeMHr6Topa.6.2 MHnaTop:6.2.1 nHnynatop tuna l,nepekncb 6eH3onna,1-copm no FOCT 14888;6.2.2 nHnLnatop Tuna II,3MynLcna nepekncn 6eH3onna c cogepxaHnem 6eH3onna He 6onee 1,5%ncogepaHeM BoAbi He 6onee 18%.lpumep 40%nepekucu 6eH3ouna e duana3oHe KoHyeHmpayu om 38,5%do 41,5%.6.2.3 nHnynatop tuna lll,cornacoBaHHbinc 3anHTepecoBaHHbiMn cTopOHaMn;6.2.4 HeHacbieHHa nonn3pHa n BHnupHa cMona;6.2.5 cnKoHoBaA KoHccTeHTHaA cMa3ka.peAynpexAeHne!HnunaTopbi,takne kak nepeKncb 6eH3onna,cnegyet XpaHnTb B cOOTBeTCTBnn cycTaHoBneHHbIM Tpe6oBaHnAMn 6e3onacHocT.Heco6nogeHne Tpe6oBaHn 6e3onacHoctn Moxet npnBec-T K Hecta6nnbHoctn MatepnanoB,kotopag MoxeT cTatb npnynHo noxapa n B3pbiBOB.HenocpeAcTBeHHoe cMenBaHe nHNLnaTopoB c HeKoTOpbIMN XnMn4ecKnMN peaKTnBaMn,HanpnMep cKo6anbToM,MokeT co3Aatb B3pbBoonacHble ycnoB.7 ogroToBka k npoBegeHnio cnbiTaH7.1 logroToBKa annapaTypbiYcTaHaBnMBalot B TepMocTate TeMnepatypy(82,2 0,25)C,n3MepAloT TeMnepatypy npu noMowMTepMoMeTpa u xAyt yctaHoBneHng paBHoBecng no teMnepatype np unpkyngunn BoAbi B Te4eHne He MeHee60 MMH.7.2 KoHAnuoHpoBaHne7.2.1 An Hactowero Metoga ncnbitaHn KoHgnnoHnpoBaHne He tpe6yetcA.7.2.2 lepeA go6asneHnem nHnynatopa k cmone,cMona gonxHa 6bItb Bbigepxaha npu temnepatype,yka3aHHON B HOpMaTnBHom AokyMeHte nu TexHn4eckon gokyMeHTaynn ha npogykunio.8 poBegeHne ncnbiTaHn8.1 B3BewnBaloT(1,00 0,02)r nepeKncn 6eH3onna n noMewaoT B cTaKaH BMeCTNMOCTbIo 150 CM3.Ao6aBnAioT 1,00 r MoHoMepa ctupona K nHnnaTopy n TaTenbHo nepeMewaoT.3