ASTM_D_6730_-_01_2016_rus.pdf

D 6730-01(2016.)100-()STANDARD TEST METHOD FOR DETERMINATION OF INDIVIDUAL COMPONENTS IN SPARK IGNITION ENGINE FUELS BY 100METRE CAPILLARY(WITH PRECOLUMN)HIGH-RESOLUTION GAS CHROMATOGRAPHY ():2930-16/ASTM :30.06.2016 2016 (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.-,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/ASTM D 6730-01(2016)D 6730-01(2016.)100-()1 D 6730,.().1.1.1 ,(MTBE,ETBE,.)225C.,(,.),.1 ASTM D02 ,D02.04.0L .1 2016.2016.2001.2011.D 6730-01(2011).DOI:10.1520/D6730-01R16.1ASTM D 6730-01(2016)1.2 ,0,01%30%.,.1.3 ,t-,-(MTBE),-(ETBE)-(TAME)1%30%.1.4 ,.(PONA),-.,(,)n-,PONA.,25%.C7,-(FCC),.1 2ASTM D 6730-01(2016),.,.1.4.1 D 1319(),PONA.1.5 ,D 1744 .,.,.,D 4815 D 5599 D 5623 .1.6,.1.7 ,.,.3ASTM D 6730-01(2016)2.2.1 ASTM:2 D 1319 D 1744 (2016.)3 D 3700 D 4057 D 4177 D 4307 D 4626 D 4815 ,TAME,DIPE,1 4 D 5580 ,/-,o-,C9 ,D 5599 -2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3 .www.astm.org.4ASTM D 6730-01(2016)D 5623 E 355 E 594 -,E 1510 3.3.1 ,.E 355.4.4.1 ,(),.-,-,./.,.5ASTM D 6730-01(2016).5.5.1 ().5.2 4,5,6,7.,.,(,).5.3 ,4 Johansen,N.G.Ettre,L.S.,“Retention Index Values of Hydrocarbons on Open Tubular Columns Coated with Methyl Silicone Liquid Phases,”Chromatographia,5,.10,1982.5 Johansen,N.G.,Ettre,L.S.Miller,R.L.,“Quantitative Analysis of Hydrocarbons by Structural Group Type in Gasolines and Distillates.Part 1,”Journal of Chromatography,256,1983,.393-417.6 Kopp,V.R.,Bones,C.J.,Doerr,D.G.,Ho,S.P.Schubert,A.J.,“Heavy Hydrocarbon/Volatility Study:Fuel Blending and Analysis for the Auto/Oil Air Quality Improvement Research Program,”SAE Paper 930143,1993.7 Schubert,A.J.Johansen,N.J.,“Cooperative Study to Evaluate a Standard Test Method for the Speciation of Gasolines by Capillary Gas Chromatography,”SAE Paper 930144,1993.6ASTM D 6730-01(2016).(PONA),-.,/,PONA.5.4 ,D 1744.,.,.,.,D 4815 D 5599 ,D 5580 D 5623 .6.6.1 ,(5C)200C 0,1C/.,.,(200:1).-,7ASTM D 6730-01(2016),.-,594,250C.6.2 .,0,1 0,5.,.10.6.3 ,:6.3.1 400 .6.3.2 .6.3.3 .6.3.4 (1 2)(10).6.3.5 .6.3.6 .8ASTM D 6730-01(2016)6.3.7 .6.3.8 .6.4 ,(100).,.,.,.11,1,.6.4.1 ,.100 0,25 0,50 ,n,35C -400 000 500 000 ,k,35C 0,45 0,50 ,R,t-2-2 35C 3,25 5,25 ,t-35C 1,0 5,0 6.4.2 (0,25)(1 4),5%95%,()(100),1.9ASTM D 6730-01(2016)7.7.1-,99,999%.(,.)7.2 ,99,999%.(.7.1.)7.3 ,99,999%.(.7.1.)7.4-,99,999%.(,.)7.5:7.5.1 .,8.,.7.5.2 ().7.5.3 99,5%.(.7.5.2.)7.5.4 8 ,.,.,BDH Ltd.,Poole,Dorset,U.K.,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.10ASTM D 6730-01(2016).(.7.5.2.)7.5.5 ,D 4307,(.1).(.7.5.2.).1 ,.1.1.%8,00 n-2,00 t-0,50 2-2 2,50 2,3-0,50-10,00 n-2,00 1-0,50 1,00 28,90 3-0,20 1,2 t-0,50 n-2,00 2,3,3-0,50 7,00 n-2,00 25,00 p-1,00 2,3-0,20 n-2,00 5-0,20 1-2-0,50 n-1,00 n-0,50 1,2,3,5-0,25 0,50 n-0,25 1-0,25 n-0,25 11ASTM D 6730-01(2016).1 DHA()(7.5.5)12ASTM D 6730-01(2016)8.8.1 110 (16 .),(D 4057 D 4177).1.1 ,.8.1.1 D 3700.,350 (45 .).8.1.2 D 4057.8.2 ,4C .8.3 .8.4 .9.9.1 100-,A1.13ASTM D 6730-01(2016)E 1510/8.9.2 A1.,.2 12 1.2.5C 10 5,0/50C (50)1,5/200C 5 250C 150:1 0,1 0,2 -250C :30/300/,20/-277 (40 .)24/35C 9.3 ,35C.-.,.9.4 -,.7,00 0,02 35C,24/,14ASTM D 6730-01(2016)1.6,53 5C.-.277 (40 .),332 (48 .).:uave(/)=()/tM()(1)9.5 -,-.,.,9.5.1,9.5.2.9.5.1 -():9.5.1.1 P=(.)+)/.9.5.1.2 j=3/2(P2 1)/(P3 1).9.5.1.3 uo=uave/j=.9.5.1.4 Ac=pi(r)2=(2).r=().9.5.1.5 (3/)=u0 Ac 60.9.5.2 (+)/.9.5.3 100 0,25:9.5.3.1 Uave=100 100/6,98 60=23,88/.9.5.3.2 P=40 .+12,0/12,0=4,33.9.5.3.3 j=3/2(18,778-1)/(81,370-1)=0,33 9.5.3.4 uo=23,88/0,33=71,96/.9.5.3.5 Ac=pi(0,025/2)2=4,9 10-4 2.9.5.3.6 =71,96 4,9 10-4 60=2,12 3/.15ASTM D 6730-01(2016)9.5.3.7 =(192+2,12)/2,12=91,6:1.9.6 (),.,5%.9.7 9.4,9.5 9.6 -.10.10.1 .(),().,.,.16ASTM D 6730-01(2016),.10.2 ,(7.5.5),.2 12.:250C:0,2,0,5,1,0 :300C:0,2,0,5,1,0 10.3 ,13.2 .1.1.(%)=100 ()/(2)10.4 10.2,3%.11.11.1 ,.,.1 .1.1.,9 10,(7.5.5)35C,17ASTM D 6730-01(2016),.,.220C 20.11.2 (k)35C:k=(tR tM)/tM(3):tM-(),tR-,.11.2.1 0,45 0,50 11.3 ,:n=5,545(tR/w1/2h)2(4):n-(),tR-,w1/2h-.11.3.1 400 000.11.4 -.,(.1,.1.4).100-t-2-2 35C.:18ASTM D 6730-01(2016)R=2(tR2-M-2 tRTBA)/1,699(w1/2h2-M-2+w1/2hTBA)(5)11.4.1 35C 3,25 5,25.11.5 ,.,.,.,5%.1 .1.3.=B/A(6)11.5.1 t-(0,5%)(7.5.5)35C.1,0 5,0.12.12.1 .2 100-,1.,12.3.,19ASTM D 6730-01(2016),.12.2 .,.,.,.,.12.2.1 :RIi=100 (n+(lo