ASTM_D_6584_-_13_rus_scan.pdf

MEXTOCyAAPCTBEHHbIM COBET No CTAHAAPTM3ALN,METPONorN CEPTONKALM(MrC)INTERSTATE COUNCIL FOR STANDARDIZATION,METROLOGY AND CERTIFICATION(ISC)FOCTMEXTOCYAAPCTBEHHbI33018-CTAHAAPT2014TONBO A3OBOE O3EHOE B100OnpegeneHne o6wero cogepaHuA MoHornnuepuAoB,AurnnuepuAoB,tpurnnuepnAoB,cBo6oAHoro n o6werornnuepnHa ra3oBon xpoMaTorpanenM3aHe onunanbHoeMocKBaGnCTaHAapTHPopM2015FOCT33018-2014MHpopMauuA o6 u3MeHeHuAX k HacmoweMy cmaHoapmy ny6nukyemca e exe2oHOM uHopMauuoH-HoM yKa3amene HauuoHanLHbie cmaHdapmbi,a meKcm u3MeHeHuuu nonpaeok eexeMecA4HoM uHpop-MaquOHHOM yKa3amene HaquoHanLHbie cmaHdapmbi.B cnyuae nepecMompa(3aMeHbi)unu omMeHbIHacmoue2o cmaHdapma coomeemcmeyiowee yeedoMneHue 6ydem ony6nukoeaHo e exeMecA4HOMuHpopMaLuOHHOM yKa3amene HayuoHanLHbIe cmaHapmbi.Coomeemcmeyioa uHpopMauuA,yee-domneHue u mekcmbi pa3Meuwaiomca makke e uHpopMayuOHHou cucmeMe owe2o nonL3oaHuR Ha opu-quanLHoM caume PedepanLHo2o a2eHmcmea no mexHu4eckoMy pe2ynupoeaHuio u Memponozuu e cemuHmepHemCTaHAapTHopM,2015B Poccnickon Pegepaynn hactown ctaHgapt he Moxet 6bItb nonHoctbio nn yactu4ho Bocnpon3-BegeH,TpaxnpoBaH n pacnpocTpaHeH B ka4ecTBe opnynanbHoro n3gaHn 6e3 pa3peweHng egepanbHoroareHTcTBa no TexHeckoMy perynpoBaHo n MeTponorn0CT33018-2014M E X r O C yA P C T B E HH bI NC T A HA P TTOnnNBO BA3OBOE BNON3EnbHOE B100OnpeneneHne o6wero conepxkaHna MoHornnuepnnoB,nnrnnuepnnoB,TpwrnnuepnnoB,CBOOOAHoro N o6wero rnNuepNHa ra3oBon xpoMatorpadnenBiodiesel B100 blend stock.Determination of total monoglycerides,total diglycerides,total triglycerides,free and totalglycerin by gas chromatographyAaTa BBeneHna-2016-07-011 06nacTb npnMeHeHNA1.1 HacToawnn cTaHnapT ycTaHaBnMBaeT MeTon KonwyecTBeHHoro onpeneneHna o6wero conepxaHnsMOHornMuepnnoB,nnrnwuepnnoB,TpnrnwuepnnoB,CBO6O Horo N o6wero rnwuepHa B 6a3oBOM 6non3enb-HOM TonnNBe B100 Ha oCHoBe MeTnnoBbix 3npoB xnpHbIX KNCnoT MeToAoM ra3oBoM xpoMaTorpacwn.Anana-30H onpeneneHna conepxaHna MOHornMuepngoB cocTaBnaeT 0,009 Macc.-0,77860 Macc.,ArnnuepngoB 0,092353%Macc.-0,54475%Macc.n TpnrnnuepngoB 0,00092857%Macc.-1,3881%Macc.Anana3oH onpeneneHna conepxkaHna CBO6O Horo rnMuepnHa cocTaBnaeT 0,0005714 Macc.-0,019533 Macc.,o6wero rnMuepMHa-0,0090714 Macc.-0,42767 Macc.MeTon He wcnonb3yOT ana onpeneneHna MeTwnoBbIx 3npoB KoKocoBoro w nanbMoBoro Macen,nony-yeHHbIX N3 naypNHOBoro Macna.1.2 3HayeHna B eAMHMuax CncTeMbl CM CYNTalOTC CTaHAapTHbIMN.1.3 B HacToaweM CTaHnapTe He npeaycMoTpeHo paccMoTpeHne Bcex BonpocoB obecneyeHnabe3onac-HOCTM,CB93aHHbIX c ero wcnonb3oBaHneM.nonb3oBaTenb HacToawero cTaHnapTa HeceT OTBeTCTBeHHOCTb 3aycTaHoBneHne CooTBeTCTByHOwNX npaBnn no TexHNke be3onacHOCTN NoxpaHe 3nopoBba,a Takke onpenenaeTenecooopa3HOCTb npNMeHeHna 3aKoHonaTenbHbIx orpaHnyeHwN nepen ero ncnonb3oBaHneM.2 HopMaTnBHble ccblnKnna npwMeHeHNA HacToawero cTaHnapTa Heo6xonMbl cnenylowne ccbinoyHble nokyMeHTbl.na Hena-TNpoBaHHbIX cCblnoknpNMeHAHOT nocne Hee n3naHne CCblnoyHoro nokyMeHTa(BKnoYa9 Bce ero N3MeHeHNA).2.1 CTaHAapTbI ASTM1)ASTMD4307 Standard practice for preparation of liquid blends for use as analytical standards(CTaHnap-THaa npaKTnka npnroToBneHNA KNOKNX cMecen cnonb3oBaHNa B KayecTBe aHanNTNyeCKNX CTaHnapToB)ASTME 355 Standard practice for gas chromatography terms and relationships(CTaHAapTHaa npakrnkano TepMNHaM N COOTHO山eHM9MBa3 oBoN xpoMaTorpa中MMASTM E 594 Standard practice for testing flame ionization detectors used in gas or supercritical fluidchromatography(CTaHnapTHa npaKTnka npoBepkn nnaMeHHO-NoHn3auNoHHbIX AeTeKTopoB,ncnonb3yeMbIxB ra3oBoN Mnn CBepxkpNTNyeCKoN KNAKOCTHON XpoMatorpadnn).3 TepMNHbI n onpeneneHnaB HacToaweM cTaHnapTe npnMeHeHbl cnenylowne TepMNHbI C COOTBeTCTByHOWNMN onpeneneHWAMN:3.1 OnpeneneHna3.1.1 6a3oBoe 6nonn3enbHoe TonnNBo B100(biodiesel B100):TonnNBo N3 MOHoanknnoBblx 30n-poB HHOLenoyeyHbIX KNpHbIX KNCNOT,nonyyeHHbIX N3 pacTnTenbHbIX Macen NnM XKNBOTHbIX XKMpoB,0603HayaeMoe B100.1)yTOuHMTb cCbinKn Ha CTaHgapTbl ASTM MOXHO Ha canTe ASTM www.astm.org wnn B cnyx6e nopgepxkn knneH-TOB ASTM serviceastm.org.B wHoopMauMoHHOM TOMe exeroAHoro c6opHnKa cTaHgapToB ASTM(Annual Book of ASTMStandards)cnenyeT o6pawaTbca K cBonke cTaHnapToB exeronHoro coopHnka cTaHnapToB Ha cTpaHnue canta.M3 naHne o中nunanbHoe