ASTM_D_6591_-_18_rus.pdf

D6591-18 548/06 STANDARD TEST METHOD FOR DETERMINATION OF AROMATIC HYDROCARBON TYPES IN MIDDLE DISTILLATES HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD WITH REFRACTIVE INDEX DETECTION 2019 ():13.05.2019:3661-19/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D6591-18 1 D6591-18 548/06 1 D6591;,.().,IP 548-06,.ASTM-IP ISO.1 ASTM D02 ,D02.04.0 .,(IP)2000,(,61 New Cavendish Street,London W1M 8AR.1 2018.2018.2000.2017.D591-11(2017).DOI:10.1520/D6591-18.ASTM D6591-18 2 ,.1.1.1 ,+-,150C 400C,.,%/,.1 ,50C-300C,D6379 .1.2 ,4%40%(/),0%20%(/),0%6%(/)+-,0%26%(/)4%65%(/).1.3 ,.,.ASTM D6591-18 3 1.4 .,.-.1.5 (FAME),+-.,FAME,+-.1.6 ,.,.1.7 -,().ASTM D6591-18 4 2.2.1 ASTM:2 D1319 D2425 -D4057 D4177 D5186 D6379 2.2 :3 IP 548 3.3.1 ,:3.1.1 (DAHs),2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3 ,61 New Cavendish St.,London,WIG 7AR,U.K.,http:/www.energyinst.org.ASTM D6591-18 5 ,+-.3.1.2 (MAHs),(DAHs).3.1.3 ,.3.1.4 (POLY-AHs),+-.3.1.5 ,MAHs,DAHs +AHs.3.1.6+-(T+AHs),DAHs.3.1.6.1 .:(1):(),(),(2)MAHs:,(3)DAHs:,(4)+AHs:,ASTM D6591-18 6 .4.4.1 ,.,MAHs,DAHs +AHs.DAHs +AHs .4.2 ,.,(),/MAHs,DAHs +AHs .DAHs +AHs /POLY-AH.MAHs,DAHs +AHs (%/).5.5.1 ,.5.2 (US EPA)ASTM D6591-18 7 .(CARB),.5.3 ,.D1319,US EPA ,315C(600F).D2425 ,.D5186,(CARB),.2 D5186 CARB ,D1319.6.6.1 (HPLC)HPLC-,0,5/1,5/,0,5%99%.7 .7.2,HPLC.HPLC-.(,).8 ,.9 HPLC-;,.7.3 o-(1,2-),98%.7.4 1-,98%.7.5,98%.7.6,95%.7.7 9-,95%.(,).10 ASTM D6591-18 11 .8.8.1 ,D4057 D4177,.9.9.1 ,-.HPLC-,(.1).,;.1 .ASTM D6591-18 12 11 ,(.6.5).(.)./,.12 .,.9.2 1,0 0,2/.().9.2.1 ,(1)(),(2).,.,.13 (0,8/1,2/),9.4.3.9.3 ASTM D6591-18 13(SPS)(1,0 0,1),o-(0,5 0,05),(0,05 0,005)9-(0,05 0,005)100 .,9-o-(,).14 SPS-,5C 25C.9.4 ,10 SPS(.9.3).,HPLC-0,5%.15 /,.1 ,.9.4.1 ,SPS-(.2).9.4.2 ,9-.16 /(S/N)9-3:1.9.4.3 ,o-.9.4.3.1 o-:()()2112699,12yytt+=(1)ASTM D6591-18 14:t1-,t2-o-,y1-,y2-o-.5,0,.,.,.2 9.5 9-.9.6 B,:,ASTM D6591-18 15 B=tA+0,4(tB-tA)(2):tA-(),tB-9-().17 ,+AHs ,.9.7 ,10 SPS-(.9.3).(.9.6)+AHs,(.3).(.).,.3 ,ASTM D6591-18 16 9.8 9.7 ,o-,9-.18 ,().10.10.1:10.1.1 (,D),.1,0,0001 ,100 .19 .1 ,.,(.,).20 (,10),5C 25C.1.,/100 o-,/100 1-,/100 ,/100 A 5,0 4,0 4,0 0,4 2,0 1,0 1,0 0,2 0,5 0,25 0,25 0,05 D 0,1 0,05 0,02 0,01 ASTM D6591-18 17 10.1.2 (.9.4)10 .(.3).(.9.6)+AH-,.(.).10.1.3 10.1.2 ,D.10.1.4 D ,D (,0,02/100),10.1.1.10.1.5 ,%/(/100),.o-,1-.0,999 0,01/100.21 .22 .23 ,.10.2 :10.2.1 0,9 1,1 0,001 10 .ASTM D6591-18 18 10 (.6.3).10.2.1.1 ,()(,2/10),(,0,5/10).24 ,.,.4 10.2.2 (.9.4),(.10.1)10 (.10.2.1).(.9.6)+AHs,(.4).,ASTM D6591-18 19 (.).10.2.3 .5,MAHs,DAHs +AHs.10.2.4 ,(.5)(D .5).,.5 ,ASTM D6591-18 20 10.2.5 (.5)MAHs .10.2.6 (C .5)MAHs DAHs .10.2.7 ,+AH(E .5)+AH(F .5).,.10.2.8 MAHs (.5).10.2.9 DAHs D(.5).10.2.10 +AHs E F(.5).25 ,.11.11.1 /(/)MAHs,DAHs +AHs,:()MVISA+=+AHs DAHs MAHHs,/%(3):A-MAH,DAH +AH,ASTM D6591-18 21 S-(%/)MAH,DAH +AH,I-MAH,DAH +AH(%/),M-()(.10.2.1),V-()(.10.2.1).26 .11.2 /(/)POLY-AH :%/POLY-AH=%/DAHs+%/T+As(4)11.3 (%/)(.MAHs+DAHs+AHs).12.12.1 MAH,DAH,+AH,POLY-AH,0,1%/.12.2 :12.2.1 D6591;12.2.2 ;12.2.3 (.11);12.2.4 (),12.2.5 .ASTM D6591-18 22 13.4 13.1 (95%-):13.1.1 ,.2,.13.1.2 ,.2,.2.%(/)(MAH)4-40 0,026(+14,7)0,063(X+17,3)(DAH)0-20 0,10(X+2,6)0,32(X+1,8)+-(T+AH)0-6 0,12(X+0,6)0,64(X+0,3)(POLY-AH)0-26 0,13(+2,5)0,29(+2,5)4-65 0,036(X+1,5)0,116(X+6,3)AX=,4 -ASTM International RR:D02-1503.ASTM Customer Service serviceastm.org.ASTM D6591-18 23 13.1.3 D6591 -.14.14.1 ;()X1.X1.1 ,150 300 4 5 .(,30 4,6,).X1.2 ,.,.X1.3 ,ASTM D6591-18 24 ,().1/,.,(,0,25/)12 (,).X1.4 ,.,./.X1.5 ,(,1/2).,/,.X1.6 ASTM D6591-18 25 ,/:X1.6.1 Waters Spherisorb 3 NH2.X1.6.2 Waters Spherisorb 5 NH2.X1.6.3 UBondapak 10 NH2.X1.6.4 Whatman 5 PAC.X1.6.5 Lichrosphere 100 NH2,5.D02.04 (D6591),.(1 2018.)(1)9.7.ASTM D6591-18 26 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 :serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.