ASTM_D_6443_-_04_2010_rus.pdf

:D 6443-04(2010.),()Standard Test Method for Determination of Calcium,Chlorine,Copper,Magnesium,Phosphorus,Sulfur,and Zinc in Unused Lubricating Oils and Additives by Wavelength Dispersive X-ray Fluorescence Spectrometry(Mathematical Correction Procedure)-2011.ASTM International:D6443-04(2010)/11061:07.09.2011 (ASTM)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM ,ASTM,.ASTM.Translation of this standard has been made by Normdocs OOO.under the official permission from the American Society for Testing and Materials(ASTM),100 Barr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM does not confirm or approve this translation,and only the English version as published and copyrighted by ASTM can be considered as the original version.Reproduction of this translation is possible by authority of ASTM only.197376,-,.,5,.1,1237.:+7(812)438-16-88+7(495)223-46-76:+7(812)438-16-88E-mail:informnormdocs.ru http:/www.normdocs.ru:D 6443-04(2010.),()1 D6443;,.().1.1.1 ,.1.2 ,1.,.1.3 ,(LOD)2(.40 CFR 136,B)(LOQ),2 Sr,.LOD LOQ,2.1.3.1 LOD LOQ .LOD LOQ ,.1.4 ,()(E1361),.1.5 ,.1.6,_1 ASTM D02 ;D02.03 .1 2010.2010.1999.2004 .D6443-04.DOI:10.1520/D6443-04R10.2,55,.2210-2218.1 ,.1.7 ,.,.2.2.1 ASTM:3D 1552 ()D 4057 D 4177 D 4307 D 4628 ,D 4927 ,D 4951 -D5185 ,_3 ASTM -ASTM,www.astm.org,ASTM serviceastm.org.ASTM -ASTM.1.2 LOD LOQ,-(ICP-AES)D6299 E29 E1361 2.2:440 CFR,136 B,1.11,.265-2673.3.1 .,.,.,.,.3.2 .,.,-.,(),.4.4.1 ,.,.,.4.2 ,_4 ,732 N.Capitol St.,NW,Mail Stop:SDE,Washington,DC 20401.4.3 ,.4.4 ,D4628,D4927,D4951 D5185.5.5.1 .,.,.,.5.2 ,.,.5.3 -d,.,.6.6.1,1 10 .,:6.1.1 ,.,.,.6.1.2,.6.1.3-,(LiF200),(PE)50 .6.1.4 .6.1.5,.1 .6.2,30 1.2 3 (r)(R),6.3 ,.,.4 .,.7.7.1 .,.5 ,.7.2,(99.95%),.7.3 P-10,90%10%,.2 P-10 .7.4 ,-.U.S.P.7.5 :7.5.1 ,:,.7.5.1.1 ,.D1552 .7.5.1.2 ,.7.5.2-n-,.3 -n-._5,American Chemical Society,Washington,DC.,BDH Ltd.,Poole,Dorset,U.K.,U.S.Pharmaceutical Convention,Inc.(USPC),Rockville,MD.7.5.3,.7.5.4,.,-.8.8.1 D4057 D4177,.8.2 .9.9.1 .(D4307),1.9.1.1 ,1.9.1.2 ,(,2,6,8 10).9.2-(.)-.,.2 ,.-,0.25%,.-,.10.10.1 K-.5.;,5 .3.4 ,X=.10.2 ,(-),.10.3 -,.10.4 ,.,.,4-5 .,.10.4.1 ,.10.5 ,.,-,:Ci=i ,Di=,i,Ei=i,Ii=i,aij=j i ,Cj=j.10.5.1 ,(.1).,D,E,.10.5.1.1 ,.-,.10.5.1.2 ,0.05%.,-.10.5.2 ,(.1,2,6,8 10).,D E .10.5.3 ,(.1).,D E .10.6 ,.(-),.,.11.11.1 ,.11.2 ,.11.3 ,D E ,1.11.4 ,1,.12.()12.1 (QC),.,QC .X2 .12.2 QC ,/.12.3 QC .13.13.1 ,.13.2%,0.0100%,0.0010%0.0100%,0.0010%.13.3 .E29.4 5 ,Ca,0.70LiF(200).,0.70 113.16,116.16Cl,0.70Ge.,0.70 92.80,94.80Cu45,60LiF(200).,.,0.30 45.03,47.03,Mg40,7050.,0.70 23.05,25.80P40,70Ge.,0.70 141.00,137.00S,0.70Ge.,0.70 110.75,116.75Zn45,60LiF(200).,.,0.30 41.76,47.03 6 (r)(R),7 ,G J.?.?CaCuMgPZn0.00240.00230.01030.00260.00230.00250.00240.01100.0025 0.00250.0010.010.00070.00010.0020.13030.01430.11030.14870.13620.1320 0.0147 0.1094 0.1511 0.13470.00170.000430.1090.00240.001513.4 ,LOD.,LOD,2,2,.13.4.1 ,.14.614.1 .11 3 .2 Conostan.7,8 ,_6 -ASTM International RR:D02-1450.7 Conostan ConocoPhillips Inc.,CONOSTAN Division,1000 South Pine,Ponca City,OK 74602.8 ,-ASTM International.,1 .,.,.,.14.1.1 ,8-6,.14.1.2 ,8-6,.14.2 ,.(G)Conostan 5000 ppm(Ca,Zn,Cu,P),Conostan (Mg),2-,8,9 .8,9 :Ca,0.0024%;Zn,0.0023%;Cu,0.0023%;P,0.0026%;Mg,0.0103%;Cl,0.0035%._9 Aldrich Chemical Co.,1001 West Saint Paul Ave.,WI 53233.5 8 ,X=%.,(J)Conostan(Zn,P,Ca,Mg),Conostan 5000 ppm (Cu),2-.:Ca,0.1303%;P,0.1487%;Zn,0.1362%;Mg,0.1103%;Cu,0.0143%;Cl,0.0275%.7 ,.14.2.1 ,.14.2.2 ,.14.3 LOD LOQ,2.LOD Sn,LOQ-10 Sn,Sr-,()5 2(.40 CFR 136 B).14.3.1 LOD LOQ ,.15.15.1 ;()X1.X1.1 ,.X1.2 .X1.3 (),.X1.4,-(D -,.1).,.X1.5 ,.,.X1.6 .X1.7 ,.X1.8 .X1.9 .X1.10 .X1.11 (,.).(1 ).,.X1.12 .X1.13 ,.X1.14 (,.),.-,.X1.15 U.S.P,.,.6X2.(QC)X2.1 ().X2.2 (.D6299 MNL710).X2.3 QC .(.X2.1).,().,.X2.1 ,.X2.4 ,_10MNL7,6-,3,ASTM International,W.Conshohocken,PA 19428.,.,.,.(.D6299 MNL710).X2.5,QC,.QC .X2.6 .D6299 MNL710.ASTM International ,.,.;,.;-ASTM International.,.,ASTM .ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States .(),ASTM 610-832-9585(),610-832-9555 (),serviceastm.org (),-ASTM(www.astm.org).ASTM(www.astm.org/COPYRIGHT/).7