ASTM_D_6376_-_10_2017e1_rus.pdf

:D6376-10(2017.)1 STANDARD TEST METHOD FOR DETERMINATION OF TRACE METALS IN PETROLEUM COKE BY WAVELENGTH DISPERSIVE X-RAY FLUORESCENCE SPECTROSCOPY 2018 ():28.03.2018:3388-18/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D6376-10(2017)1 1 :D6376-10(2017.)1 1 D6376;,.().1 2017.1.1.1 .1.1.2 ,1 ASTM D02 ,D02.05 ,.1 2017.2017.1999.2010.D6376-10.DOI:10.1520/D6376-10R17E01.ASTM D6376-10(2017)1 2 .1.3 (.1).,.1.4,.1.5 ,.,.2.2.1 ASTM:2 D346 D1552 (IR)(TCD)D4057 D5056 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D6376-10(2017)1 3 D5600 -(ICP-AES)D6969 D6970 E11 3.3.1:3.1.1 ,.3.1.2 ,.3.1.3 ,-,.3.1.4 ,().3.2 ,:3.2.1 ,.3.2.2 ,75 (200).3.2.3 (),ASTM D6376-10(2017)1 4.3.2.4 ,.1 ,(/)Na 50-500 Al 50-500 Si 20-500 S,%0,10-7,0 Ca 20-500 Ti 10-200 V 20-2000 Mn 10-200 Fe 20-1000 Ni 20-500 4.4.1 110 10 ,75 (200).,.,.,.,ASTM D6376-10(2017)1 5.4.2 .5.5.1 ,.5.2 (),.5.3 (SOx),.6.6.1 .2.-,.6.2 ,.6.3 ,ASTM D6376-10(2017)1 6 .2.2Q-,.A ,.A 25,05 26,75,24,35,2d 50A 145,13 143,13 PET 144,95 147,05,142,85 InSb 110,68 113,18 Ge 113,08 116,00 LiF(200)86,13 84,13 LiF(200)76,93 78,93 LiF(200)62,97 60,97 LiF(200)57,52 59,02 LiF(200)48,66 49,92,47,40 LiF(200)A .,.,.7.7.1,50 0,01.7.2 ,276 (40 000 .).7.3 ,20 ,75 (200)10,.7.4/,.7.5 ,(),.7.6 ,.7.7,75 (200),ASTM D6376-10(2017)1 7 E11.7.8 ,110 10.7.9 ,.:7.9.1 .,.2.7.9.2,.,.7.9.3 ,.7.9.4 ,.7.9.5 ,.8.8.1 .,ASTM D6376-10(2017)1 8.3,4 ,.8.2 P-10(90%,10%).8.3 ,.8.4 ,.9.9.1 ,.D4057,D346,D6969 D6970.75 (200),.50.1 ,3 ,DC.,.Analar Standards for Laboratory Chemicals,BDH Ltd.,Poole,Dorset,United States Pharmacopeia and National Formulary,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.4 ,.Reagent Chemicals and Standards,by Joseph Rosin,D.VanNostrand Co.,Inc.,New York,NY.ASTM D6376-10(2017)1 9.,.9.2 :9.2.1 .,.,.9.2.2 ,.9.3 :9.3.1 110 10 5.9.3.2 5 0,01 .9.3.3 1 0,01 20.9.3.3.1 ,75 (200),.2 ,ASTM D6376-10(2017)1 10(,.),.,0,01.9.3.4 ,.,.9.3.5 .276 (40 000 .)5.9.3.6 -.().9.3.7 .3 7.9.3.8 ,9.3.2 9.3.7,20%.9.3.9 .,.9.3.10 ,.ASTM D6376-10(2017)1 11 3%(10%).,.10.10.1 ,XRF-.10.2 10.3 .,:10.3.1 :,%=100/(Tt)1/2 l/(Rp)1/2 (Rb)1/2)(1):Tt-.Tt ,Rp-,Rb-10.3.2 ,:Tp/Tb=(Rp/Rb)1/2(2):Tp-,Tb-,ASTM D6376-10(2017)1 12 Rp Rb-,.11.11.1,:11.1.1 .3 D1552(),D5600 D 5056(),.11.1.2 .:=3(2+N)(3):N-,.11.1.2.1 ,.11.2:11.2.1 ,12.11.2.2 ,:Ci=(Di+Ei Ri)(l+isCs)(4)ASTM D6376-10(2017)1 13:Ci-i-,Di-i-,Ei-i-,Ri-i-,is-,i-,Cs-.11.2.3 ,.11.2.4 (is).11.2.5 ().10%(),.d :d=R1/Rn(5):R1-,Rn-.12.12.1 (),-.12.2 .ASTM D6376-10(2017)1 14 12.3 ,.2 .12.4 .12.5 ,11 .13.13.1 ,:13.1.1 ,.3 .13.1.2 ,.3 .13.2 .ASTM D6376-10(2017)1 15 14.14.1 ;,;,;3.26/36/8/11/45/66/0,12%0,22%9/11/2/2/24/32/2/3/19/28/10/14/ASTM D6376-10(2017)1 16 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.