ASTM_D_7573_-_09_rus.pdf

D 757309 STANDARD TEST METHOD FOR TOTAL CARBON AND ORGANIC CARBON IN WATER BY HIGH TEMPERATURE CATALYTIC COMBUSTION AND INFRARED DETECTION 2014 ():2521-14/ASTM :09.12.2014 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 7573-09 1 D 757309 1 D 7573;,.()1.1.1 (TC),(I),(TOC),(DOC)(NPOC),0,5 4000/.,680 C,1 D19 ASTM ,D19.06 .01 2009.2009.DOI:10.1520/D7573-09.ASTM D 7573-09 2 CO2,-(NDIR).1.2 TOC-DOC-TC-DC-,I-.TIC-DIC-.TOC-DOC-,.TOC=TC I.1.3 NPOC-I-,NPOC-.1.4 ,-,.1.5 ,.1.6 .1.7,.1.8 ,.ASTM D 7573-09 3 ,.2.2.1 ASTM:2 D 1129,D 1192 (2003.)3 D 1193 D 2777 ,D19 D 3370 D 4129 D 5847 3.3.1 ,.D 1129.3.2 ,:2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3 www.astm.org.ASTM D 7573-09 4 3.2.1 (I-),.3.2.2 (TOC-).3.2.3 (NPOC-),.3.2.4 (-)I-TOC-.3.2.5 (DOC-),.3.2.6 (-),(VOC).3.2.7 ,.4.4.1 .I-,NPOC-TC-,-(TC I).DOC-,0,45.4.2 TOC-DOC-I-.,I-,TOC-(CO2).I-ASTM D 7573-09 5.1.1 TIC-5.5.1 ,.5.2 TOC-,(COD)(TOD),.4 6.6.1 CO2 4 ,5.3,1973.,.512.ASTM D 7573-09 6 (680 C),.-(NDIR).6.2 (,),.6.3 (),TOC-(NPOC-).NPOC-TOC-()-.6.4 -,TOC-(.TOC=TC TIC).6.5,.,I-TOC-,(TC I)TOC,NPOC-.6.6 (1)-TOC-.6.7 680 C,ASTM D 7573-09 7 .6.8 ,.(),.,.6.9 ,.TOC-(1,0/),.6.10 ,.CO2,TIC-.,40 TIC-,1 TIC-160/.6.11 ,.,(5%NPOC-.1 5 ,OI Analytical Aurora 1030C 1020.,-ASTM International.1,.ASTM D 7573-09 9 TIC-.7.2.1.2 ,.7.2.2 ,.7.2.3 CO2 CO2-NDIR.7.2.4 ,CO2 CO2.,-,.7.2.5 NDIR-/.7.3 TOC-TOC-10 ,TOC-,TOC-TOC-1.ASTM D 7573-09 10 IC NPOC TC 2 -8.8.1 .,6,.,6 ,DC.,.,BDH Ltd.,Poole,Dorset,U.K.,U.S.Pharmacopeial Convention,Inc.(USPC),MD.2 ASTM D 7573-09 11 .8.2 ,I II,D 1193.,NPOC-0,05/.,.,CO2 =2,CO2 ().,.,.CO2 ,.8.3 TIC-.,TIC-.8.4 (1000/)1000,500 ,2,128 (KHC8H4O4),ASTM D 7573-09 12 120 C.,1 (HCl),.().8.5 (1000/)1000,500 ,2,377 (C12H22O11),1 (HCl),.().8.6 (1000/)1000,500 ,8,826 (Na2CO3),120 C.Na2CO3,.8.7 (834 CaCO/)10 (.8.6)100 I-8.8 TC,I 8.8.1 4 (CB-).ASTM D 7573-09 13 .pH 2 (HC1).TC-NPOC-.NPOC-I-.(CB)0,0 C/,.CB-,30.CB-,.1.8.8.2 4 (CB-).(NPOC-).1.8.9 ,CO2 .,.ASTM D 7573-09 14 1 (/)()()(/)(CB).0,0 1000 0,0 1 1000 0,5 1000 0,5 2 1000 1,0 1000 1,0 3 1000 10,0 1000 10,0 4 1000 25,0 1000 25,0 5 1000 50,0 1000 50,0 6 1000 100 1000 100 7 1000 250 1000 250 9.9.1 D 1192 D 3370.9.2 6 C TOC-,pH 2 HCl ,.,.,().28 .9.3 DOC-48 /.2 2 6 C.48 .ASTM D 7573-09 15 9.4 ,.(.6.3).2 ,DOC-.9.5 ,.10.10.1 ,.11.11.1 30 (,).,.,20%.11.2 ,ASTM D 7573-09 16 (CCV-)(QC).CB-,.,25 250/,4-7.(MRL).I-NPOC-(TC-).,.5%.,.11.3 r2 0,993(-0,9995).(ICV-),.ICV-10%.11.4 .,.,QC-,(SOP-),.ASTM D 7573-09 17 12.12.1 .,.(-),.,:12.1.1 .12.1.2 pH 2 pH 5 7 10N NaOH .12.1.3 .12.1.4 TIC-TC-()TOC-.12.1.4.1 I-,TOC-,I-,CO2 10N NaOH pH 5 7 TC-.12.2 ASTM D 7573-09 18 (,I-).TIC-.12.3 ,pH 2(),I-.().CO2 I-,.(70C).12.4 TOC-NPOC-.I-,NPOC-(.6.4).12.5 TC-.13.13.2 ().13.3 ,.ASTM D 7573-09 19 14./(QC/Q)14.1 ,QC-.14.2 .11.14.3 ,.,.14.3.1 ,0,5 4000/.,.14.3.2 ,15.,.,D 5847 F-t-ASTM D 7573-09 20 .14.4 (LCS),LCS-.,LCS-20.LCS-,.,LCS-,15%;,.14.5 (I-),NPOC-()I-,.NPOC-(MRL).TIC-TIC-TOC-.14.6 .,QC-.ASTM D 7573-09 21 14.7 (MS)-().14.7.1 .,25-,1050-(,).14.7.2 (P):(1):A-(/),-(/),-(/),Vs-(),V-().14.7.3 ,80 120%();,-.:(1)(2),(3),.ASTM D 7573-09 22 14.8 :14.8.1 .14.8.2 ,F-.F-.6.4.4 D 5847.14.8.3 ,.14.9 ,(IRM),.IRM-,-,.15.7 15.1 ,(.D 2777-06).15.2 2,3.7 -ASTM International RR:D19-1180.ASTM D 7573-09 23 16.16.1;2 (MDL)0,519 0,484 0,505 0,502 0,494 0,443 0,542 STDDEV()0,030762 MDL()0,096592 ML()0,307162 3 10 1 100%NPOC 101%NPOC 98%NPOC 101%NPOC(RSD=0,73%)101%NPOC(RSD=1,85%)79%NPOC/96%TC 108%NPOC/99%TC 97%NPOC 98%NPOC 62%NPOC/98%TC 97%NPOC 100%NPOC (100)70103%NPOC 9395%NPOC(RSD=1,55%)(5 2)ASTM D 7573-09 24 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).ASTM(www.astm.org/COPYRIGHT/).