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TM_E_1421_ _99_rus_scan
CT PK ACTM E 1421-2011IpenncnoBne1OITOTOB,JEH K BHECEHpecnyoJnkaHcKnM rocyapcTBeHHbIMnpeanpnsTnem H TexHHqecKHMKOMHTeTOM no cTaHnapTH3aun No 33 Ha 6a3e TOO(CAIIA HHTEPCHCTEM2 yTBEPXKIEH M BBEIIEH B IIENCTBME IIpuka3oM Ipencenarens KoMHTeraTexHHyeckoro peryJInpoBaHH H MeTpOJIOrHH MHHHCTepCTBa HHIYCTPHH H HOBbIX TeXHOJIOTHHPecny6JHKn Ka3axcTaH OT 20 Hoaopa 2011r.No 636-on.3 HacTosi cTaHnapT HneHTnyeH AmepnkaHcKoMy HaunoHabHoMy cTaHnapTy-ASTM E 1421-99 Standard practice for describing and measuring performance of fouriertransform mid-infrared(ft-mir)spectrometers:level zero and level one tests(CraHnapTHbIiMeTon onncaHns H H3MepeHns 9KcnJyaralHoHHbIX napametpoB ypbe-cnektpoMetpoBcpehei HHopakpacHo oonactn cnektpa:HcnbltaHna ypoBHa HOnb H ypoBHa OHH),aBtopckoenpaBo npHHaniexKnT ACTM MHTepHemHen,100 Bapp Xapoop IIpaiB,BecT KoHekteH,IIITaTITeHCHbBaHHs,19428,CIIIA.Iepen3naerca c pa3pemeHns ACTM HHTepHemHen.OoHunaJbHoi Bepcnei aBJserca TeKcT Ha rocynapcTBeHHOM n pyccKom 93bIKe.IepeBonc aHrmniickoro 3bIka(en).OoHunabHbli 9K3emnsp AmepHkaHckoro HauHoHabHoro cTaHnapta-ASTM E 1421-99,Ha ocHoBe KoToporo nonroToBJeH HacToani rocynapcTBeHHbIn cTaHnapT,n cTaHnapToB,Ha KoTopble aHbI CCbIIKH,HMeeTca B locynapcTBeHHOM oHne TexHHyecKHX peraMeHTOB HcTaHnapToB.CTeneHb COOTBeTCTBHA HIeHTHYHas(IDT)4 B HacToseM cTaHnapre oTpakeHbI TpeooBaHna H HopMbI 3aKoHa PecnyoJkn Ka3axcTaHO TexHHyecKoM peryuupoBaHHn OT 09.11.2004 rona No 603-II,3aKoHa Pecny6JHKnKa3 axcTaH O npOMbILIeHHO6e3 onacHoCTH Ha onacHbIXpoH3 BOICTBeHHbIX O6 bekTaxOT03.04.2002roa314.5 CPOK IIEPBONPOBEPKN201704nEPHOIMYHOCTb IPOBEPKM5 neT6 BBEEH BEPBbIEMHoopMayua o6 u3MeHeHuax k Hacmoaueny cmaHdapmy nyonukyemca 6 ykasameneHopMamusHbie ookvMeHmbl no cmaHdapmusauuuy,a mekcm u3MeHeHuu-6 eoiceMecauHbixuncopMayuonnbix ykasamensx Tocyoapcmeennble cmandapmbly.B cnyuae nepecmompa(omMeHbl)wu 3aMeHbl Hacmoawe2o cmaHoapma coomeemcmeyiowaa uHobopMauua oyoemonvonuKoBaHa 6 uHoopMauuoHHoM yKa3amene(l ocyoapcmeeHHble cmaHoapmblyHacTosuni cTaHnapT He MOxeT 6bITb HOJHOCTBIO HIH yaCTHHO BOcnpOH3BeneH,THpaxKHpoBaH H pacnpocTpaHeH B KayecTBe ooHunabHoro H3naHHa 6e3 pa3peweHna KoMHTeraTexHHyeckoro peryJHpoBaHHa H MeTpOJOrHH MHHHCTepCTBa HHyCTPHH H HOBbIX TexHOJIOrHPecny6JKn Ka3axcTaHCT PK ACTM E 1421-20111.2.5 Ina upoBeneHni ucrraHni Ha cneKTpoMerpax FT-IR B pexnMe maroBorocKaHHpoBaH,cenyeT HCHOIL3OBaTb H3MeHeHMA Ho HacTomeMy MeTony H HHQOpManHIo,npenocTaBIeHHyIo opraHn3aunei-nocTaBImnKoM npn6opa.2 HopMaTHBHLIe CCLLIKHIna pHMeHeHA HacTomero cTaHnapTa Heo6XonuMLI CHenyomne cCLLIOqHbIenOKyMeHTLI.a HenaTHPOBaHHLIX CCLIOK pHMeHgeTCa nocAenHne u3naHue CCLIO4HoroIOKyMeHTa(BKIouaa Bce ero H3MeHeH).2.1 CTaHapTI ASTMASTM E 131-10*Standard Terminology Relating to Molecular Spectroscopy(CTaHnapTHa TepMHonor MoneKynpHo cneKrpocKonun).ASTM E 932-89(2007)*Standard Practice for Describing and Measuring Performance ofDispersive Infrared Spectrometers.(Meron na onucaHua n onpeneneHu 3KeHnyaTaunoHHLIxxapaKTepucTHK AncepcHOHHLIX HHQpaKpacHLIX cHeKTPOMeTPOB).ASTM E 1866-97(2007)*Standard Guide for Establishing SpectrophotometerPerformance Tests(PyKoBoncTBo no ctITaHnAM A onpeneneHn 3KCHIyaTauMOHHLIXnapaMeTpoB cneKTpoMeTpoB).ASTM E 1944-98(2007)*Standard Practice for Describing and Measuring Performanceof Laboratory Fourier Transform Near Infrared(FT NIR)Spectrometers:Level Zero and LevelOne Tests.(Meton wwis hna6opaTopHLIX ypLe-cneKTpoMerpoB An 6nn*Hei HHpaKpacHoi o6nacTH(FT-NIR):HCbITaHH ypOBH HO.IL H ypOBH IHH).3 TepMHHLI H onpeeIeHHB HacTogmeM cTaHapTe pHMeHIoTCA cIenyoHe TepMHHLI c COOTBeTCTByIOIHMHonpeneeHMH:3.1 OnpeneneHua:na onpeneneHi TepMHHOB,HCHOL3yeMLIX B HaCToeM MeTone,cCLLnaTcA Ha TepMHHOnorHO E 131.Bce onpeneneHHg cHeKTpaNLHLIX o6nacTei HMecTopacHooKeHni nonoc nornomeHHi naHLI B BOTHOBLIX qHCIax(cM),a cHeKTpaLHa3HeprHA,nponyckaoma cHocO6HOCTL H nornomaTeLHa cHoCO6HOCTL O603Ha4eHI BypaBHeHHAx 6yKBaMn E,T H A cooTBeTcTBeHHO.OTHomeHHe Byx BeHqHH nponycKaHnA(nponyckatomei cnoco6HocTn)n nornomeHna(nornomarenLHoi cnoco6HocTn),a TaKkeOTHomeHHe ypoBHei 3HeprHn npH Byx pa3HHLIX BOHOBLIX qHcIax 0603Ha4eHI 6yKBo R.loncTPouHLi HHneKc o603Haaer cHeKTpaLHoe nOnoKeHHe Ha BOTHOBLIX qHCIaX(HanPHMeP,A3082,nornomeHne npn 3082 cM).3.1.1 HcutIraHne ypoBH o1nn(1)(level one(1)test):IIpocraa cepua 3MepeHni,pa3pa6oTaHHag Ig o6ecneqeHHg KOHeCTBeHHLIX aHHLIX Ho Pa3JH4HLIM acHeKTaM9KcHTyaTauHOHHLIX HapaMeTpoB(XapaKTepHcTHK)pH6opOB H HHOpMauHH,Ha KoTopoiHyKHO OCHOBLIBaTL yCTaHOBIeHHe npO6JeM(3aTpyIHeHui).lo noBony HHopMauH o ccIoqHLIx craHnaprax ASTM,nocerurs calir ASTM www.astm.org nMcBa3arca co cHyx6o ASTM no o6cnyxHBaHuo norpeourene no neKTpoHHoMy anpecy serviceastm.org.ro6s nonyrs nopo6Hy1o HHopMao u3 ecezoonoi Knuzu cmandapmo6 ASTM cHIaTcA Ha crpaHnyKpaTKoro H3oeH cTaHIapTa Ha caire ASTM.*IpHMeHeTc B cooTBeTCTBHH c CT PK 1.92CT PK ACTME 1421-20113.1.2 McnbrraHHe ypoBHa HoJ(0)(level zero(0)test):CTaHnapTHas(Tekymas)npoBepka oKcnyaTaLnoHHbIX xaparrepHcTHK npHoopa,KoTopax MoxKeT ObITb ocymecTBJeHa 3aHecKoJbKO 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cBeToneJnTeJa Toro,YTO6bI OOHTbCa ynoBneTBopHTeJbHorOyHKIHOHHpOBaHn npHoopa.PaooyHe yCJoBHa OTHeJbHbIX npHoopoB Jyyie BceroHOJIYYHTb H3 JIHTepaTypbI H3TOTOBHTeJI B CB43H C H3MeHeHHAMH KOHCTPyKIIHH npHoopa.CneayeT OTMeTHTb,YTO MHoTHe npHoopbI FT-IR cnpoeKTHpoBaHbI IIa Hanyumnei pa6oTbI,Kora Hx ocTaBJISFOT B pexKHMe OxKHaHHS.CJenyeT OTMeTHTb,YTo cnekTpoMeTpbInpeHa3HayeHbI II HCIbITaHHH TOJIEKO B npeneJax CBOHX paooyHX IHana30HOB BOJHOBbIXqHceJI.IIPIMEYAHHE 1:Hacrosui Meron pa3paooraH ws HcnoJb3oBaHHa B cHryaunsx,korna erekrop HeHacbImeH.B HekoropbIx npHoopax,c coyeraHHeM onTHeckoi cucTeMbI H ereKTopoB,3JeKTpoHHas yacTbeTekropa HacblneHa nycTbIM JIyoM.Takne npnoopbI CKOHCTpyHpoBaHbI I ocJaoJeHn(aTTeHyauH)HHopakpacHoro Jyua B cnekTpoMeTpe HH B oTHeneHHH IIS oopa3na c neJbro ycTpaHeHna HacbrmeHna ereKropa.CJeayer oopaTHrbca K HMeromeMyca pyKoBOuCTBy K npHoopy HIH 0OCYIHTb COOTBercTByrouHe TexHHKHarreHyauHH c nocTaBIHKOM npHoopa.5.2 BHeIHHe yCJoBHA,B KOTOPbIX yHKUHOHHpyeT npnoop,BJIHAFOT Ha 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